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Home My WebLink About2015 Jul 31 - Bennett Environmental Assoc. Inspection & Alpha Lab Reports � ` BENNETT ENVIRONMENTAL ASSOCIATES, INC. LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS 1573 Main Street,P.O.Boa 1743 (508)896-1706 Brewster,MA 02631 fax(508)896-5109 LETTER OF TRANSMITTAL TO: DATE: JOB NUMBER: MassachusettsDepartmentofEnvironmentalProtec[ion 9/31/15 BEA13-10579 Attention:Title 5 Program 1 Winter Street-6th Floor Boston,MA 02108 REGARDING: Drinane Residence 12 Dove's Wing Road ��6�Q��Dp SHIPPING METHOD: South Yazmouth,MA 02664 AUG 21 2015 Regulaz Mail � Pick Up � PriorityMail ❑ HandDeliver ❑ HEALTHDEPT. �� Express Mail ❑ Other ❑ Certified Mail 0 Green Cazd/RR � COPIES DATE DESCRIPTION 1 DEP Approved Inspection and O&M Form for Title 5 UA Treatment and Disposal Systems(December 2014,June 2015) 1 Singulair Service Inspection Checklist(December 2014,June 2015) 1 12/12/14 Alpha Anatytical Labomtory Report 1 6/9/15 Alpha Malytical Laboratory Report For review and comment � For approval: � As requested: � For your use: � REMARKs: Please find enclosed the DEP Inspection and O&M Forms,Singulair Service Inspec[ion Checklists,and laboratory analytica]results for operation and maintenance conducted during the reporting period for the above referenced property. On February 6,2015 the Yarmouth Board of Health issued a letter approving the reduction in operation and maintenance of the alternative sepric system to semi-annvally. If you have any questions or require addiriona7 informafion,please contact us at your earliest convenience. Thank you. cc:Yarmouth Boazd of Health Lee Drinane,Property Owner � Robin Cassidy-Norweco[via email] FROM: DavidBennettWWTO#6243/SamanthaFarrenkopfWWTO#13265/JosephSmithWWTO#12529/GregBrehmWWTO#16149 If enclosures aze not as noted,kindty nodfy us at once ' Massachusetts Department of Environmental Protection ' � Bureau of Resource Protection - Title 5 DEP Approved Inspection and O�M Form for Title 5 I/A I Treatment and Disposal Systems A. Installation �mportanc:wnen Lee Drinane filling out fortns Owner on the computer, - useonlythetab 12 DOVe'S Wing Road key to move your Facility Street Address cursor-do not South Yarmouth 02664 use the retum City Zip key. �Il Mailing address of owner, if different: VI I� � StreetAddresslPOBox: xm City State Zip (508) 398 -3280 ext. Telephone Number B. Authorized Service Provider Bennett Environmental Associates, Inc. O&M Firtn 1573 Main Street/ PO Box 1743 Street Address Brewster MA 02631 City State Zip (508) 896- 1706 e�. 129 .Telephone Number Samantha Farrenkopf 13265 Certified Operator Name Certification Number C. Facility/System Information Singulair 960 NR DEP ID Manufacturer ID Model Number 7/2/08 7/8/08 Installation Date Start of Operation Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial Seasonal Residence—used less than 6 mo./year: ❑ Yes � No D. Operating Information 12/4/14 9/10/14 Inspedion Date Previous Inspection Date Sludge Depth(to be checked yeariy) Pumping Recommended ❑ Yes � No t5aiom.doc•rev.04-11-13 Page 1 of 3 1 i � ' Massachusetts Department of Environmental Protection ° � Bureau of Resource Protection -Title 5 , DEP Approved Inspection and O&M Form for Title 5 I/A ' Treatment and Disposal Systems E. Field Testing iField Inspection: Color: ❑ gray ❑ brown � clear ❑turbid ❑ Other(specify): Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid Effiuent Solids: ❑ no � some pH 7.0 SU D0 4.0 mg/L Turbidity 3.49 NTU 6 to 9 2 or greater 40 or less Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected per Standard Methods and analyzed for BOD and TSS. F. Sampling Information Samples Taken: ❑ Influent � Effluent Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use nitragen reducing systems: gpd Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS 0 TN � Other(list below) Nitrate Nitrite TKN Other 1 Other 2 Other 3 G. Inspection and Maintenance Description of any maintenance pertormed since previous inspection &during this inspection: Conduct an operation and maintenance event. Collect effluent samples for field testing and laboratory analysis. Notes and Comments: EfFluent quality passed field testing parameters. The recirculation pump is not functioning and requires replacement. t5aiom.doc•rev.04-11-13 Page 2 of 3 � Massachusetts Department of Environmental Protection � Bureau of Resource Protection - Title 5 DEP Approved Inspection and O&M Form for Title 5 1/A Treatment and Disposal Systems H. Certification I certify: I have inspected the sewage treatment and disposal system at the address above, have conducted the required Field Testing and/or sample collection in accordance with Standard Methods, have completed this report and the attached technology operation and maintenance checklist, and the information reported is true, accurate, and complete as of the time of the inspection. I am a Massachusetts certified operator in accordance with 257 CMR 2.00. �A�V19'��`�L�titi�:V��'�,4-, �lu1S Operator Signature �� Date System owner must submit this report, technology O&M checklist, and any required sampling results to the Iocal board of health as follows for each inspection performed: Remedial Use—by January 31�of each year for the previous calendar year Piloting Use-within 45 days of inspection date Provisional Use—by March 31'"of each year for the previous 12 months General Use—by September 30`"of each year for the previous 12 months Send to: Department of Environmental Protection Attention: Title 5 Pro�gram One Winter Street, 5 Floor Boston, MA 02108 t5aiom.doc•rev.04-11-13 Page 3 of 3 � Massachusetts Department of Environmental Protection � Bureau of Resource Protection -Title 5 DEP Approved Inspection and O&M Form for Title 5 I/A � Treatment and Disposal Systems A. Installation Important:When Lee Drinane fillingoutforms pkrner on the computer, use onrytnetab 12 Dove's Winq Road key to move your Facility Street Address cursor-donot SouthYarmouth 02664 use the retum C� Zip key. �Il Mailing address of owner, if different: VI�� StreetAddress/POBox: rertan City State Zip (508) 398-3280 e�. Telephone Number B. Authorized Service Provider , Bennett Environmental Associates, Inc. O&M Finn 1573 Main Street/ PO Box 1743 Street Address Brewster MA 02631 City State Zip (508) 896- 1706 e�h. 129 Telephone Number Samantha Farrenkopf 13265 Certified Operator Name Certfication Number C. Facility/System Information Singulair 960 NR DEP ID Manufacturer ID Model Number 7I2I08 7/8/OS Installation Date Start of Operation Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial Seasonal Residence—used less than 6 mo./year: ❑ Yes � No D. Operating Information 6l3/15 12/4/14 Inspedion Date Previous Inspection Date Sludge Depth(to be checked yearly) Pumping Recommended ❑ Yes � No t5aiom.doc•rev.04-11-13 . Page 1 of 3 � Massachusetts Department of Environmental Protection � Bureau of Resource Protection - Title 5 DEP Approved inspection and 08�M Form for Title 5 I/A ; Treatment and Disposal Systems � E. Field Testing Field Inspection: Color: ❑ gray ❑ brown � clear ❑turbid ❑ Other(specify): Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid Effluent Solids: � no ❑ some PH 7.0 SU p� 4.0 mg/L Turbidity 0.90 NTU 6 to 9 2 or greater 40 or less Should a Remedial or General Use system fail the Field Testing, effluent samples shali be collected per Standard Methods and analyzed for BOD and TSS. F. Sampling Information Samples Taken: ❑ Influent � Effluent Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use nitrogen reducing systems: gpd Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS � TN � Other(list below) Nitrate Nitrite TKN Other 1 Other 2 Other 3 G. Inspection and Maintenance Description of any maintenance performed since previous inspection &during this inspection: On 1/5/15 replace the recirculation pump under manufacturer's warrentee. On 6/3/15 conduct an operation and maintenance event. Collect effluent samples for field testing and laboratory analysis. Notes and Comments: All mechanical components of the system are operating correctly. Effluent quality passed field testing parameters. t5aiom.doc•rev.0411-13 Page 2 of 3 � Massachusetts Department of Environmental Protection � Bureau of Resource Protection - Title 5 DEP Approved Inspection and 08�M Form for Title 5 I/A Treatment and Disposal Systems H. Certification • I certify: I have inspected the sewage treatment and disposal system at the address above, have conducted the required Field Testing and/or sample collection in accordance with Standard Methods, have completed this report and the attached technology operation and maintenance checklist, and the information reported is true, accurate, and complete as of the time of the inspection. I am a Massachusetts certified operator in accordance with 257 CMR 2.00. �'�`��t�o�e�C�UN 'I��1�lS OperatorSignature �- D� System owner must submit this report, technology O&M checklist, and any required sampling results to the�ocal board of health as follows for each inspection performed: Remedial Use—by January 31�of each year for the previous calendar year Piloting Use-within 45 days of inspection date Provisional Use—by March 31�'of each year for the previous 12 months General Use—by September 30`h of each year for the previous 12 months Send to: Department of Environmental Protection Attention: Title 5 Pro�qram One Winter Street, 5t Floor Boston, MA 02108 t5aiom.doc•rev.0411-13 Page 3 of 3 � � SINGULA.I12 960 NR WASTEWATER TREATMENT SYSTEM SERVICE INSPECTION CHECKI,I5T Addirss: �Z �U�S .�'^� LGvv� Owner: L-22 (�r�n<tn� Operator. �� ✓1G �(�/f'�- (—��/M Date: �vZ�� 7—�/ This checklist summat•izes the service procedw�es to be perfonned dm�ing a rontine Singulair 960 NR inspection.Refer to tlie Singulair Manual for a detailed explanaflon of each service procedm•e and an O&M h•oubleshooting guide. � CONTROL CENTER SERVICP: NOTES/COM�IENTS �Check operation of conhol cemer c--L�.+F G��n 'vii J t��Y}� ('o:fQC`�l f ❑A,djust time clock when required , �Checkoperationofrecirculationcontrolpanel ;tF'+L' y��^'� y14}Z v�iF��Et�,n$ N FFLUENT RECI�CU] TION SYSTEM t Il heck operation of recirculation pump �[1eC�U��8 it �."7�s w� � �1r>�T,�h�n S pect recirculation well&fittings C�t�f PC �� Test Operation + ❑Set recirculation raYe rate(a)minlhr ABBATOR SERVICE heck0 aeratorop�ation I�2!"Cc�c�f i5 r�Az�� CC1tr�c��y �eck aerator power comumption eck aerator air delivery C�lean stainless steel aspirator shaft 1 vi ce ::. o �`i S �it f./� �rC�anaspiraWrtip �."�(�"�`� LYClean fi•esh air vent in concrete cova . � � Fd Inspect aeration cham6er contents C CATION CIiAMBER SERVICE f i emovetheBio-ICineticsystem ��:' 15 V_+DESt�+4�+�3 CGtft�=1'�y - I ❑Sciape the olarificatian chamber O IpSpect the Bio-Static sludge return �Inspect ouflet couplmg ❑Install a clean Bio-Kinedc system ❑Fill Blue Crystal feed iube(if installecn ❑Fi(1 Bio-Neutralizer feed tube("if installed) GE ERAL SERVICE _ / �pecteffiuentpiunpchamber 5 S��n . �5 Vtt�� 0 P�C,'{�n t<7f�tCT��/ Iuspect effluent qualify C�t ..� c. .o,� � c J Vto f ❑Inspeot outlet line �o n� � r i . Q Inspect ground water re[ief point(if installed) QInspecteftluentdisposalsystem ��Cc� r,,,,c, � „ pt.SSC�' '�•e�� ❑Compfete owner service record , S . nc �''� <S ❑Co�nplete health departme�noti5cation � ❑Complete distributor service iecatd P Upat U,y� � c.� rq�J Q Mail health depattmetct notification �¢t�ta � S� S� --� �� " � T•� . (v�74 3 t,,� �� Siegmund Environmental Services,Inc. � �;'iF+�' J� �^� � _ � L: Ff.0 vnvw�.siepmundLEARD OLnUTIONS. J � / f✓i�� 2. ,r ri� "7 ,L1�I �`J � � !�3' k� • a SINGULAIR 960 NR WASTEWATER TREATMENT SYSTEM SERVICE INSPECTION CHECKLIST Address: ��i �V2$ ��l-.�_ }'��' Owner: �Y��h�h�-- �J �, ( + Operator. J� � ��,' �� ' Date: �31 (� � 2�'� Tftis checklist summaiizes the service procedures m be pert'ormed during a ioutine Singulair 960 NR inspecfion.Refer to tlie Singulan-Mamial for a detailed explanation of each service procedure and an O&M hnubleshootivg guide. CONTROL CFNTF.R SERVICE NOTES/COMML�N'1'S �.Check operation of control center l�*�.� 5�v.5,v�a J� `� �'W'��✓�, ��. W'^�� ❑Adjusttimeclockwhenrequucd c��- -�y' a$ a{��•�a>-� w�.ra�v,� ❑Check operation of recu•cu(afion control pauel NR EFFLUENT RECIRCULATION SYST$M heckoperationofrecirculationpump Qxi.�. . ,P�� r�� o,��r�J��w��, O Inspect recircularion well&fittings �.Test Operation ❑Set recirculation rate rate @ min/lu ABRATOR SERVICE �heckaerntoroperation �x..r��r ;3 �,�a.r�,>-�..��v��c,��"(,- ❑Check aerator power consumptlon �Checkaeratorairdelivery \aok- 5�,- y� ��-S o.- � �u\�v� �Clean stainless steel aspirator shaft p��. v.S,a . i�Clean aspirator rip C�Clean fresh air vent in concrete cover ❑Inspect aeration chamber contetrts CLARII7ICATION CHAMBER SERVICE \ emovetheBio-Kineticsystem i�:A - \�'..�.2c. �:,�y�f � �o��"`a ❑Scrape the cla�ification chamber '�,o� c,�---, - Q�dnspect the Bio-Static sludge retum �InsPectoutletcoupling '"B..a ._ SJ�.:c, S�� e- f •>r"• Q��Install a clean BiaKinetic system "�� C�-��- . ❑Fill Blue Crystal feed tube(if installed) ❑Fill Bio-Neutralizer feed tube(if installed) ��a3 -o `6� GENERAL SERVICE �nspecteffiuentpumpchamber '�� ^ 1 `� ��'M�Q Ci`-*c'^�'"r �o S ,Q.S og{�� nspectetfluentquality �p -V��p cr�� ❑Inspect ouUei line D Inspect graund water relief pourt(if insta(Ied) vr-.p . � S , �J e � +v�S ut� ❑Inspect eff7uent cIisposal system --j'.at� -o.�iD c-�"`^• � w•-�`1 �w�ry.•t. ❑Complete owner service record ❑Complete health departmerrt notification ��3� � �g ;� t�Y--f'c. ;�ti� ' ❑Complete distributor service record �p Z El J` `w��i �L J ❑Mail health depaz�hnent notification C,V - , �`�'�-""� �y_ �.�a�g SS - Siegmund Envu�anmentel Sexvices,Inc. � � t \ � ,p c SSr�+� IT.UID TIIINI�NNG.CI,F,AR SOLUTIONS. ��(�j,�✓�-� v \�� vnv�v.sieemunrleroun.com � �� \ � v �i Serial No:12121412:47 r. 4 { ' �� / - '.'�.�1�N�'L�'Y�T 1 C A L � ANALYTICAL REPORT Lab Number. L1429300 Client: Bennett Environmental Associates 1573 Main Street Brewster, MA 02631 ATTN: David Bennett Phone: (508)896-1706 Project Name: DRINANE RESIDENCE Project Number: BEA13-10579 Report Date: 12/12/14 The original project report/data package is held by Alpha Analytical.This reportldata package is paginated and should be reproduced only in its entirety.Alpha Analyfical holds no responsibility for resutts and/or data that are not consistent with the original. Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086), PA(68-03671),USDA(Permit #P330-11-00240),NC(666),TX(f104704476),DOD(L2217),US Army Corps of Engineers. Eight Walkup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com Page 1 of 15 '�` "`.. r /� d w N r Q �j O 7 C) � M � � � I � N � •V � � � O � N J � � j I O Z I m � d o N 9 R � fn � � C Gf � t' � � V Z p '�•- � J 2� � � � UG � ' Q ' � 2 H � O � � Q c } m o = a�= r m � m o O tq J lA � X W � F � � W U Z W � � � � W o I- Q c'i 0 W � W d L�i. � m � LL U W i: . d d a E E m � � z z o � � � 0 0 0 m d d � M N . �Q � � O O a` a a� a a I'i ¢ e� � Serial No:12121412:47 � Project Name: DRINANE RESIDENCE Lab Number: L1429300 Project Number: BEA13-10579 Report Date: 12/12/14 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were enwuntered during the preparation ior analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. � Results contained within this report relate on�y to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC,for all NELAC accredited parameters.The data presented in ihis report is organized by parameter(i.e.VOC,SVOC,etc.).Sample specific Qualily Control data(i.e.Surrogate Spike Recovery)is reported at the end of the iarget analyte list for each individual sample, followed by the Laboretory Batch Quality Control at the end of each parameter.If a sample was re-analyzed nr re�xtracted due to a required quality control corrective adion and if both sets of data are reported,the Laboratory ID of the re-analysis or re-exh'action is designated with an`R"or"RE",respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific% recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.All spe�c QC information is also incorporeted in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability impiications.Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in ihe Glossary located at ihe back of the report. In reference to questions H(CAM)or 4(RCP)when'NO'is checked,the pertormance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any assoaated usabiliry implications. _ Please see the associated ADEx data file for a comparison of laboretory reporting limits that were achieved with the regulatory Numeriral -StandaMs requested on the Chain of Custody. HOLD POLICY � �� For samples submitted on hoid,Alpha's policy is to hold samples(with the exceptlon of Air canisters)free of charge for 21 calendar days � finm the date the projecl is completed.After21 calendar days,we will dispose of all samples submitted induding those put on hoM unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters wiil be disposed aRer 3 business days from the date the projec[is completed. Please contact Client Services at 800-624-9220 with any questions. I,the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analy[ical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. AuthorizedSignature: I'��•udhU�' LisaWesterlind Title: Technical Director/Representative Date: 12/12/14 Page 3 of 15 �� Serial No:12121412:47 ' � I INORGANICS & RIIISCELLANEOUS . ��. Page 4 of 15 Serial No:12121412:47 Project Name: DRINANE RESIDENCE Lab Number: L1429300 i Project Number: gEA13-10579 Report Date: 12/12/14 SAMPLE RESULTS Lab ID: L1429300-01 Date Collected: 12/04/14 15:10 I CII2f12 ID: EFFLUENT Date Received: 12/05114 i Sample Location: souTH vnrtnnourti,Mq Field Prep: Not Specified � Matrix: Water � Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General Chemistry-Westborough tati Solids,Total Suspended 7.1 � mgA � 5.0 NA 1� - 12lOS/14 0725 � 30,2540D DW _--..__-__-___- - __-.__ ......_......_______-.-_.._...._........._..._..__- __ - ...._-_______-- . _.-__.._. NRrogen,Ni[rite 0.30 mgA 0.050 - 1 - 12/06/1402:05 44,3532 DE - __ - ._._......__ - _______ _......._- _...... ._____ --_.___...... _.___ _____.. Nitrogen,Nitrate �� 2.9 �� mgll 0.10 �- 1 - 12/O6N402:51 � � 44,353.2 DE Nitrogen,Total Kjeldahl � 2.78 mgll 0.300 - 1 12/06/14 11:00 12/08/14 22:44 30,4500N-C AT BOD,5 day 5.4 mg/I 2.0 NA 1 12/06l14 00:05 12/10/14 18:55 30,5210B SE "��. Page 5 of 15 Serial No:12121412:47 � Project Name: DRINANE RESIDENCE Lab Number: L1429300 Project Number: BEA13-10579 Report Date: 12/12114 Method Blank Analysis Batch Quality Control ' � Dilution Date Date Analytical � Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method pnalyst I General Chemistry-Westborough Lab for sample(s): 01 Batch: WG746146-1 BOD,5 day ND mgfl 2.0 NA 1 12/06/14 00:05 12/10/14 18:55 30,5210B SE I General Chemistry-Westborough Lab for sample(s): 01 Batch: WG746152-1 ' Nitrogen,NiVate NO mgll 0.10 — t - 12l06/1400:48 44,3532 DE '� General Chemistry-Westborough Lab for sample(s): 01 Batch: WG746153-1 � NiVagen,Nitrrte _ ND mg4 0.050 — 7 - 12/O6/1400:50 44,3532 DE I General Chemistry-Westborough Lab for sample(s): 01 Batch: WG746268-1 � NiVogeq Total Kjeldahl ND m9fl 0.300 -- 1 12/06/1411:00 12/OS/14 22.30 30,4500N-C AT �� General Chemistry-Westbo�ough Lab for sample(s): 01 Batch: WG746433-1 Solids,Tofal Suspended ND mg/I 5.0 NA 1 - 12/OS/14 0725 30,2540� DW _�J'�v�•=-� Page 6 of 15 � , i � N I V N � +�+ .., �, �. d' O 7 M N O) N J o ,,, ,: o '.,. z,�� N I N I . . ,. . . _. 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C7 :c� a 5erial No:12121412:47 Project Name: DRINANE RESIDENCE Lab Number: L1429300 . Project Number: BEA13-10579 Report Date: 12/12/14 Sample Receipt and Container Information Were project specific reporting limits specified? YES i I i � Reagent H20 Preserved Vials Frozen on: NA Coaler Information Custody Seal Cooler ' A Absent Container Information Temp Container ID Container Type Cooler pH deg C pres Seal Analysis(") L1429300-01A Plastic 250m1 H2SO4 preserved A <2 37 Y Absent TKN�500(28) ��. L1429300-018 Plastic950mlunpreserved A 7 37 Y Absent N02353(2),BOD-5210(2),NO3- ', 353(2) L1429300-01C Plastic950mlunpreserved A 7 3.7 Y Absent TSS-2540(7) '� 'Values in parentheses indicate holding time in days ,,;� Page 10 of 15 Serial No:12121412:47 Project Name: DRINANE RESIDENCE Lab Number: L1429300 Project Number: BEA13-10579 Report Date: 12112/14 GLOSSARY Acronyms EDL -Fstimaced Derection Limit:This value represenu tLe level to which tazget analy[e concentrations are repor[ed as estimated � values,when those farget anal}rte concentrations aze quantified bebw the reporting limit(RL).The EDL includes any adjustmeufs from dilutions,concentrations or moisture confent,where applicable.The use of EDLs is specific to the analysis of PAHs usi¢g Salid-Phase Microextraction(SPME). . EPA -Environmental Protection Agency. LCS -Laboratory Canhol Sample:A sainple malri.e,free from[he analytes of interest,spiked with verified knowu amounts of aualytes or a material containiug knovm and verified amounts oFanalytes. LCSD -I,aboratory Control Sample Duplicate:Refer[o LCS. LFB -Laboratory For[itied Blaok:A sample matriz,&ee&om the anaty[es of interest,spiked with veri&ed knowu amounts of amlytes or a materiat coniaining Imown and v�eA amomts of anelytes. � MDL -Method DetecUon Limit:71tis value represents the level to which target analyte concenfratioas are repor[ed as wtimaud values, � when those target analyte concenrcations aze quantified below the reporting]imit(RL).The MDL includes any adjusUnents&nm dilufions,wncenuations or moistuce contenS�+here applicable. MS -Mavix Spilce Sample:A sample prepared by adding a Imown mass oFtarget walyte to a specified amount of matrix sample for which an independent es[imate of target aoaly[e concentration is available. MSD -Matrix Spike Sample Duplicate:Refer to MS. NA -NotAppGcable. NC -Not Calculated: Term is utilized whrn one or more of the resu@s udlized in the calculation are non-detect at the pazametefs � reporting unit. � � HI -Notl�itable. . RL -Reporting Limit: The value at which an inshument cau accuiately measure an aualy[e at a speciEc concenVatiou.l'he RL includes any adjustments from dilufioas,concentrations or moisture content,where applicable. RPD -Relative Puce¢t Difference: The results from maVix and/or matrix spike duplicates are primarily duigned to assess the precision of aualy[ical resulu in a given matrix and are ezpressed as rela[ive percent diffuence(APD). Values which are less than Sve . times We reporting]imit for any individual parameter are evaluated by utilizing the absolute difference benveen the values; although the RPD value will be provided in the repoR. SRM -Sfandard Reference MateriaL A reference sample of a knowu or cerlified value tha[is of[he same or similar ma4ic as the associated field samples. Footnotes . 1 -77ie reference for this analyte should be coasidereA modified since this maly[e is absent from the target aoalyte list of the original method. Terms Total:With resput to Organic analyses,a Total'result is defined as fhe summation of results for individual isomers or Moclors.If a Total' result is requesleA,fl�e resulfs of its individual components wiR also be rcported 1Lis is applicable to'Total'resul4 For methods 5260,8081 and 8082. Analytical Method:Both the document from wluch the method originates and the anal}rtical reference method(Exarnple:EPA 8260B is shovm as 1,8260B.)The codes for tlie reference method documents are provided in the Refuences section of the Add�dum. Dafa Qualifiers A -Specha identified as"Aldol Condeosation Product". B -The anelyte was detecred above the reporeng limit in the associated method blank.Flag only applies to associated field samples tLat have detectable concenfrations of the analy[e at less than ten times(lOx)[he concentration found in[he blank.For MCP-related projects,flag ouly applies to associated field samples that have deteclaUle conceniratioas of the analyte az less than ten times(I Ox) flie wncen4ation found in the blmk For DOD-related projects,flag anly applies to azsociated field samples that have de[echeble concentrarions of the analy[e at]ess than ten times(lOx)the conceutratiou found in the blank AND the analyte was detected above one-Lalf the reporting Iimit(or above the reporting limit for common lab contaminants)in the associated me[hod blank.For NJ- Air-rela[ed projects,flag only applies to usociated 5eld samples that have de[ectable concentrations of the analyte above the reporting limit For N]-related projecfs(excluding Air),flag only applies to associated field samples that have detectable concentrations of the aoalyte,which was detected above the reporting limit in the assceiated method blank or above five times the � reporting limit for common lab contaminants(Pbfhalates,Acetone,Methylene Chloride,2-Butanone). C -Co-elution:1'he tazget analy[e co-elutes wi[h a known.lab sfandard(i.e.surrogate,intemal standards,etc.)for co-exltected anzlyses. D -Concentration of analyte was quantified from diluted anelysis.Flag only applies to field samples that have detutable concenhatlons oFtlie analyte. E -Concentration of analy[e exceeds the rauge of[he calibra[ion curve and/or linear range of the inshument Report Format: Dafa UsabiliTy Report �. Page 11 of 15 Serial No:12121412:47 Project Name: DRINANE RESIDENCE Lab Number: L1429300 Project Number: BEA13-10579 Report Date: 12/12/14 Data Qual�ers � ' G -The concentrafion may be biaseA high due to matrirz interFereuces(i.e,co-eWtion)with non-target compound(s).1'he result should be considered estimated. H -The analysis ofpH was perfolxned beyond the regulatory-required holding time of 15 mirmtes from the time of sample collection. I I -The lower value Cor the two columns has been reporteA due[o obvious interference. ; M -Reporting L'unit(RL)ezceeds the MCP CAM Reporfing Limit for this aualyte. �� NJ -Presumptive evidence of compound.This represents an esNmated concenhation for Tenta[ively Identified Compounds('LICs),where , the ide¢�cation is based on a mass speMral library search. , P -The RPD between the resulu for the hvo colwnns exceeds the method-spuiSed cateria. �'� Q -The quality control sample eacceeds the associated accep[ance criterta.For DOD-related projects,LCS anNor Continuing Calibrntion � Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries �. when the sample concentration is greater thau 4x the spike added or for bamh duplicate RPD when the sample concentrations are less ��.. iha¢Sx the RL.(Metals only.) � �', R -Analytical results are 5rom sample re-aualysis. ' '��. RE -Analy6cal results are from sample re-extractioa . �: S -Analytical resu@s are from modified scceening analysis. ', J �Fstimated value.This represents au estimated concentration for Tentatively Identified Compounds(T[Cs). ��. ND -Not detected at the reporting limit(RL)for t6e sample. �. Report Format: Data Usability Report , ;��• Page 12 of 15 � Serial No:12121412:47 Project Name: DRINANE RESIDENCE Lab Number: L1429300 � Project Number: BEA13-10579 Report Date: 12/12/14 REFERENCES 30 Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. i 44 Methods for the Determination of Inorganic Substances in Environmental Samples, EPA/600/R-93/100,August 1993. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error,the sole and exclusive responsibiliry of Alpha Analytical shall be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. �e, � Page 13 of 15 f Serial No:12121412:47 � Certification Information Last revised April 15,2014 � The following analytes are not included in our NELAP Scope of Accreditation: i Westborough Facility i EPA 524.2: Acetone,2-Butanone(Methyl ethyl ketone (MEK)),Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, � 1,3,5-Trichlorobenzene,4-Methyl-2-pentanone(MIBK), Carbon disulfide, Diethyl ether. I EPA 8260C: 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene, lodomethane(methyl iodide), Methyl methacrylate, � Azobenzene. � EPA 8330A/B: PETN, Picric Acid, Nitroglycerine,2,6-DANT,2,4-DANT. EPA 8270D: 1-Methylnaphthalene, Dimethylnaphthalene,l,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline,4-MethylphenoL SM4500: Soil:Total Phosphorus,TKN, NO2, NO3. EPA 9071: Total Petroleum Hydrocarbons, Oil &Grease. Mansfield Facility EPA 8270D: BiphenyL EPA 2540D: TSS ' EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-l-pentene,Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500CI-D, SM23206, SM2540C,SM4500H-B EPA 332: Perchlorate. Microbiology: SM92156; SM9223-PIA, SM9223B-Colilert-QT, Enterolert-QT. Non-Potable Water EPA 200.8: AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn; EPA 200.7: AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; EPA 245.1,SM4500H,B, EPA 120.1, SM25106,SM2540C,SM2340B,SM2320B, SM4500CL-E,SM4500E-BC, SM426C,SM4500NH3-BH, EPA 350.1:Ammonia-N, LACHAT 10-107-06-1-B:Ammonia-N,SM4500NO3-F, EPA 353.2: Nitrate-N,SM4500NH3-BC-NES, EPA 351.1,SM4500P-E,SM4500P-B, E,SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664,SM14 510AC, EPA 420.1,SM4500-CN-CE, SM2540D. ' EPA 624:Volatile Halocarbons&Aromatics, EPA 608: Chlordane,Toxaphene,Aldrin, alpha-BHC, beta-BHC, gamma-BHC,delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC(Acid/Base/Neutral 6ctractables), EPA 600/4-81-045: PCB-OiL � Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9222D-MF. I For a complete listing of analytes and methods, please contact your Alpha Project Manager. III Page 14 of 15 _..... ...... ... . . . . . , - �.�� "- � '.� ��;��.;: .�. - .��a��. - � �A : l�b� z � ��"' g� �sr r �� 0 2� � � ¢�� N �� n i ' u o 0 0 p + a�'v�:A,': A'._ j { C C Z 9 m W'C4 O G.V.,��:Sa:', � �k � O 2 � � m^ m G n� 3 :� g Y N a � i't O � � S O .`4.8 �8 y+� s.g`��P3 .��,*" N �..: _ Z �� . � ❑ O � O � ■ � ■ . E �� t�� m - �::•�: � U . .] Nd:�0,.' � "��a:� m - ' 1 F�='; W d= N t � � � .r.. n i�J � ❑ ❑ m � m �i m J � • � – i a' . �`�.. W Q � � ❑ :��' �'P' _,_;,:_ E. � . � � n�S . �;:. @ �- a o � e::. w v — � � � • � o J . SSl a O � ❑ ❑ � � 009'�9!P!�B]eA!N 6 O m Q m 1 y � W d a � @ p m G � m � C N y y �m m 4 � a i LL � V O Q LL 2 K � m w � ._. � E W '� m a c � � = N � " m ' O Cm L .,,,}•-- a € m w .J v LL' �" V � � m � . � g ❑� E � � o � 0 � ~ � Q N —� e � c �a m # � v O � '.�� W m � � � ' ti — � N c o o J m � �" z � a� � a � � a � � . Na�'i m m m a N � a�'i � o 0 0 0 � � � a` a` a` a` ¢ � o � . � m E � o 0 Z «� M a � m m { a Q i6 x ng, a� m . . J y N = o $ e E � � � 0 � � � U � '' W " ' a m a m p� d � � m m �m � � m c �i � E 2' c a c� � . � " >� o N �o .� o � � w �< f tw- •� c � � m . � W � N O. � � -."n 's, a5 p y "•_�j A,. � O � u] Y � F ' - t . S� � `eY S' � A a � � � S y �' c w�„�,�� r':� . K'•� s O .. m � m `� g o °° � � }6 �: �' •a � § . �.,,,, ��t � �, � m m ?3 � o m �- Q y ' � iz�:i3� '� N� { �4,� ^2 m .. � m v � s m E � t �'�� +'�' 1 _. r. ?� .`1`�'... �$ � 3 K� n U Q m a LL W CI O ��J ?.:: :l�-. � '� ?i-:C., '": d Seri al_No:06091512:41 F_...� �... • I� ■ �/ \ ��. A N A L Y T I C A L � � ANALYTICAL REPORT Lab Number. L1512292 Client: Bennett Environmental Associates 1573 Main Street Brewster, MA 02631 ATfN: David Bennett Phone: (508)896-1706 Project Name: DRINANE RESIDENCE Project Number: BEA13-10579 Report Date: 06/09/15 The original project report/data package is held by Alpha Analytical.This repoNdata package is paginated and should be reproduced only in its entirety.Alpha Analylical holds no responsibility for resutts and/or data ihat are not consistenl with ihe original. Cert�cations&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086), PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Pertnit #P-330-11-00240). Eight Walkup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com � idi�;,� �=x,,.. Page 1 of 15 i .�; m �� , .. W V N 0 N N � � � �n N rn �y o ; � � o u i m � � � � � I o , 0 Z i I m y ai o � � R O (n � � C d � 7 Z O �£ � C J G_' � d O U � o Q � 2 F- � O � � Q c �' m o = a'� � � o O N J tn � % W ..�+ ~ � � W . U I Z W � � W � � � w o r ¢ M o w Z Q C J 2 W � m � I�i U W L • d Q� �C � G R � � Z Z � lY.1 f~.1 � N � d m d N N �O O R C �`1 � a` a` a� � �' m Qy � a Serial No:06091512:41 , Project Name: DRINANE RESIDENCE Lab Number: L1512292 Project Number: BEA13-10579 Report Date: 06/09/15 Case Narrative The samples were received in accordance with ihe Chain of Custody and no significant deviations were encountered during the preparation or analysis uniess othervvise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. Resufts contained within fhis report relate only to the sampies submitted under this Alpha Lab Number and meet all of the requirements of NELAC,for all NELAC accrediled parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample specfic Qualily Control data(i.e.Surrogate Spike Recovery)is reported at the erM of the target analyle list for each individual sample, tollowed by the Laboratory Batch Quality Control at the erM of each parameter.if a sample was re-analyzed or re-extraded due to a � required qualiry control corrective action and if both sets of data are reported,the Laboratory ID of the re-anaysis or re-e�Rrac[ion is � designated with an"R"or"RE",respectively.When multiple Batch 4uality Control elemerrts are reported(e.g.more than one LCS),the �. associated samples for each element are noted in the grey shaded header line of each data table.Any Laboralory Batch,Sample Specific% recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.All specific QC informalion is also incorporetetl in the Data Usabiliry format of our Data Merger tool where R can be reviewed along with any associated usability implirations.SoiVsediments, . solids and tissues are reported on a dry weight basis unless otherwise noted.Definilions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance aitena for CAM and RCP methods allow for some quality conVol failures to occur and still be within method compliance. In these instances the specific failure is not nartaled but noted in ihe associated QC tabie.The infortnalion is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limifs that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days from the dale llie prqed is completed.ARer 21 plendar days,we will dispose of all samples submitted inGuding those put on hold unless you have contactetl your Client Senrice Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will . be disposed after 3 business days from the date the project is campleted. Please contact Client Services at 800E24-9220 with any questions. I,the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: ��+"`•u� Michelle M. Morris Title: Technical Director/Representative Date: 06/09/15 Page 3 of 15 '�r��'�• i Serial No:06091512:41 I I � i I INORGANICS & MISCELLANEOUS , � i � i ,a�;a Page 4 of 15 ! i Serial No:06091512:41 Project Name: DRINANE RESIDENCE Lab Number: L1512292 Project Number: gEq13-10579 Report Date: 06/09l15 SAMPLE RESULTS Lab ID: L1512292-01 Date Collected: 06/03/15 14:00 Client ID: EFFwENT Date Received: 06/03/15 . SBfilPl2 LOC8110f1: SOUTH YARMOUTH,MA Field Prep: Not Specified Matrix: Water Dilution Date Date AnalyUcal Paremeter Resuk Qualifier Units RL MDL Factor Prepared Analyzed Method qnalyst General Chemistry-Westtiorough Lab _ Solids,Total Suspended ND mg/I 5.0 NA 1 -�� O6/04115 14:30 30,2540D DW Nitrogen,Nitrite 0.066 mg/I 0.050 – � - O6/03I1520:11 44,3532 ML _.___ _...._ __..._ . ._._ . ____ ........__ .. ....... . ._._ .___. ___.__ _-___ ....._.. ........... Nitrogen,Nitrate 2.9 mgA 0.10 – 1 - O6/03115 20:11 44,3532 ML ___—_..........__...—_.... .--...__--__ ___..._.— Nitrogen,TotalKjeldahl 227 mg/l 0.300 – � O6/03/1522:30 06104/1520:49 30,4500N-C AT BOD,5 day 2.5 mg/I 2.0 NA 1 O6/03/15 23:15 O6/08115 17:20 30,5210B SE ��.��. Page 5 of 15 7 Serial No:06091512:41 ` Project Name: DRINANE RESIDENCE Lab Number: L1512292 Project Number: BEA13-10579 Report Date: 06/09/15 Method Blank Analysis � Batch Quality Control � i j Dilution Date Date Analytical ' Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General Chemistry-Westborough Lab for sample(s): 01 Batch: WG790480-1 ' Nitrogen,Ndrate ND mgA 0.10 — 1 - - 06/03l15 19:07 44,3532 � ML General Chemistry-Westborough Lab for sample(s): 01 Batch: WG790481-1 ' Nitrogen,Nitnte ND mg/I 0.050 — 1 - 06/03/15 19:09 44,3532 ML ___._ ._... ..___ _..._ ._.. ._.. ._. _ ....... . ..._. ._.. _. ._. ._ _ ________ ._.__. General Chemistry-Westborougti Lab for sample(s): 01 Batch: WG790513-1 BOD,5 day ND mg/l 2.0 NA 1 O6/03/15 23:15 06�08�75 1720 30,5210B SE General Chemistry-Westborough Lab for sample(s): 01 Batch: WG790536-1 Nitrogen,TOWIKjeldahl N� mgll 0.300 — 1 O6/03/1522:30 OB/64l1520:37 30,4500N-C AT General Chemistry-Westborough Lab for sample(s): 01 Batch; WG790620-1 Solids,Total Suspended ND mg/I 5.0 NA 1 - O6/04/15 14:30 30,2540D DW .._..._ ... .. . . _ _..._.. __.__. _. _ __ . .. ..._. _. _ .._ _ ....... ._..._. .. . .._...._...._..__.._. ____.._ .. .. ... II � ( I ...---��. ''C=. �. Page 6 of 15 � N � ,�: S° � N T £ ',. ., i �I�'j'.1 ON � J , o .. o , \,I . O tq � ,' � ,I � ,,, • 0 z� J O � ,,,.. ',, ,,.. f6 ,� . . ,,, I . � '.. � . ,�,. ., . . . .. N r.d+ . ,I . ', . a R � E o : i or - . . � . . , . ��. Zp . . � ' ' '�, J OL O � , � K � �.. � . ..� � ,, .. ,..... � d , 0 a� O �, O` . h , . N _ N � � 'T � J . om , rn �'.� m I,., r I � i R ' , . , .. ,.. � .��. 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' >.p �p �.. QN �. �fA N : � .VJ . 'NJ ,,.. W � Q. . .Q :Q :Q Q ,.. � W O �J �.J J . I .�J J�� . Z � �L� �, L� ,C.� I iL� �L�� . Q M m . ..� .m , ..�. � ,�. z .7 �'7 7 .�� . O� .O. �-0 : -b O � W . O �I �O .O.'_ �, ..O. .O.. .',,. � m �.�� ,, -��. � . , ..� � ,. �.W ' .N ��N � �j.N� .N . y .��. �� . �i� L � N � C ,`�. . �� ,.,. �: N � d.,�,. Z Z �..N N . ��N� � N I,. �.W Y .N j ',. ' :•� m ,��. � �� . �� q �E y �,. � Z , Z f G . N Oi G7 U C �,. U. C .U . a �,., U� C .0 F '. O 'p "p .,, m . . m �n � a� a` a` £ � o � o � o � o � a � � .a`� -- � `m = m � o ; �..`m: = . a� s '�. rn L �C . z ,. :C Z C � m - � C. Z C � ,� � a t� c7 c7 ' c�' U'� } Serial No:06091512:41 � Project Name: DRINANE RESIDENCE Lab Number: L1512292 Project Number: BEA13-10579 Report Date: 06/09/15 � i Sample Receipt and Container Infortnation I Were project specific reporting limits specified? YES I �I Reagent H20 Preserved Vials Frozen on: Nq Cooler Information Custody Seal Cooler A Absent Container Information Temp Container ID Container Type Cooler pH deg C pres Seal Analysis(*) L1512292-01A Plastic250mIH2SO4preserved A <2 3.9 Y Absent TKN-4500(28) . L1512292-01 B Plastic 950m1 unpreserved A 7 3.9 Y Absent NO2-353(2),BOD-5210(2),NO3 353(2) L1512292-01C Plastic950mlunpreserved A 7 3.9 Y Absent TSS-2540(7) I I i i i *Values in parentheses indicate holding time in days /�ir�,� ' Page 10 of 15 ', � Serial_No:06091512:41 � Project Name: DRINANE RESIDENCE Lab Number: L1512292 Project Number: BEA13-10579 Report Date: 06l09/15 GLOSSARY Acronyms EDL -Estimated Detection Limit:This value represents the level to which target analyte wncenVations are reported as estimated � values,when those target anzlyte conce�trations are quant�ed below$e repoRing limit(RL).The EDL i¢cludes arry ' adjustments from dilu[ions,concentra[ions w moisture content,where applicable.The use of EDLs is spce�c[o the analysis of PAHs using Solid-Phase Micrcextraction(SPME). EPA -Emironmenfal Pro[ec[ion Agency. � LCS -Lxborntory Control Sample:A sample malrix,&ee&om the ar�sl}rtes of interest,spiked vrith vuified kriown amounts of analytes or s material containing knaum and verified amounts of artaly[es. LCSD -Labora[ory ConVol Sample Duplicate:Refer to LCS. LFB -I.aboramry Fortified Blarilc:A sample matrix,free from tAe analytes of interest,spiked with verified known aznounfs of analyles or a material containing known and verified amounts of analytes. MIlL -Method Deteclion Limit:This value represents the level to which target analy[e conceMrn[ions are reported as estimated values, � when those target analyte concenVations are quantified below the repor[ing limit(RL).The MDL includu any adjuslments from dilutions,concenVations or moisture content,where applicable. MS -MaVic Spike Sample:A sample prepared by adding a known muc of target ar�aly[e to a specified amount of matri�c sample for which an i�dependert est'unate of target analyte concenUa[ion is available. MSD -Matrirz Spike Sample Duplicate:Refer ro MS. NA -NotApplicable. NC -No[Calculated: Tean is u[ilized when one or more of the results utiliud i�tk�e calcWa[ion aze non-detect at the parameter'-s reporting uni[. M -NotIgnitable. NP -Noo-Plastia Term is utilized for the analysis of Atterberg Limits in soil. . RL -Reporting Limik The value a[which an ias[rument can accurately measure an arialyte at a specific wncentration.The RL � includes any adjushnents from dilu[ions,concentra[ions or moisture content,where applicable. RPD -Relative Percent Difference: The results from matrix and/or maVirz spilce duplicates are primarily designed W assess the precision of arialytical results in a given matrix and are earyressed as rela[ive percent difference(RPD). Values wltich are less than 5ve times the reporting]imit for any individual parame[er aze evaluated by utilizing the absolute differerice between the values; although the RPD value will be provided in the report. SRM -Standard Reference MateriaC A refemnce sample of a Imown or cert�ed value that is ofthe same or similar maVix as the associated field samples � Footnotes 1 -The reference for this analyte should be considereA modi5ed since tt�is analyte is absent from ihe farge[analyte lis[of the original method. Terms Total:With rospec[[o Organic analyses,a'Total'resWt is de5ned as tlie summatlon of results for individual isomers or Aroclors.If a'Total' result is reques[ed,lhe resvlfs of its individual componenfs will also be reported.This is applicable to'TotaP resWts for methods 8260,8081 and 8052. Analy[ical Me[hod:Both the document from which the method ori��AlPs and the analytical reference me[hod.(E�mple:EPA 8260B is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A -Spectra identified u"Aldol Conde�sation Product".- B -7tie analyte was detec[eA above the reporting limit in the asaociated method blank.Flae only applies to associated£eld samples that have detectable concenVations of the anzlyte at less thzn ten times(IOx)the concenha[ion found in[he blank For MCP-related projects,flag only applies[o associated field samplu Utat have detectable concentrations of the analyte at less[han ten times(IOrz) [he concentration fo�nd in tAe blank For DOD-related projec4,flag only applies to associa[ed fielA samples tha[have deteciable concentrations of the analyte ffi less thari[en times(]Oz)the concentration found in ihe blank AND the ar�alyte was detec[ed above onFhalf tl�e reporti�g limit(or above the reporting limit for common lab wrtaminanfs)in the associated method blank.For NJ- Air-related projecis,flag only applies to ascociated field samples tha[have de[ecfable concentratioas of the analyte above the reporting Iimit For NJ-related projects(excluding A'v),flag only applies to assceiafed field samples that have dMutable concentrations of the arielyte,wltich was detected above the roporting limit in the associated method blank or above five times the reporting]imit for commo�lab co�taminants(Phthalates,Ace[one,Methylene Cliloride,2-Butsnone). C -Coclution:The target analyte co-elutes with a known]ab sfandard(i.e.surtogate,intemal standards,etc.)for co-exfracted ar�alyses. D- -Concentmtion of analyte was quan[ifiW from dduted arialysis Flag only applies[o field samplu that have detectsble conce�trations ofthe analyte. Report Format: Data Usability Report ':\ �.��. Page 11 of 15 t Serial_No:06091512:41 � i Project Name: DRINANE RESIDENCE Lab Number: L1512292 �, Project Number: BEA13-10579 Report Date: 06/09/15 � Data Qualifiers E -Concentration of analyte exceeds the range of the calibration curve and/or Iinear range of ihe instnunent. ( G _ -The mncentration may be biased high due[o matrix interferences(i.e,co-elution)with non-target compound(s).The resWt shoWd I be considered es[imateA. . H -The analysis of pH was performed beyond the regilatory-requrted holding time of IS minutes from the time of sample wllection � I -The lower value for the two columns has been mported due to obvious interference. '��,. M �Repo�ting Limi[(RL)ezceeds ffie MCP CAM Repo�[ing Limi[for tltis analyte. . � NS -Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICs),where the iden�cation is based on a mass specVaf library search. P -The RPD belween the ruulu for the two wlumns exceeds the method-specified criteria. Q -The quality conVol sample exceeds lhe associated aceeptance criteria.Fo�DOD-relateA projects,LCS a�d/or Contirming Calibration � Sfandard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries when the sample concenVation is greater than 4x the spike added or for batch duplicate RPD when the sample wncenVations are less Nan Sx the RL.(Me[als only J �. R -Analytical results are from sample re-analysis ' RE -Analytical resWu are from sample re-erztractiort '. S -Analy[ical results are from modified screening analysis. J �Estimated value.This represents an es[ima[eA conce�tration for Tentatively Ide�tified Compowds(TICs). ND -Not detu[ed a[t6e reporting limit(RL)for the sample. i I Report Fortnat: Data Usability Report .%��`dL}-�FiA Page 12 of 15 ' Serial No:06091512:41 � Project Name: DRINANE RESIDENCE Lab Number: L1512292 � Project Number: BEA13-10579 Report Date: 06/09/15 REFERENCES 30 Standard Methods for the Examination of Water and Wastewater.APHA-AVWVA- WPCF. 18th Edition. 1992. 44 Methods for the Determination of Inorganic Substances in Environmental Samples, EPAI600/R-93/100, August 1993. LIMITATION OF LIABILITIES Alpha Analytical pertorms services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error,the sole and exGusive responsibility of Alpha Malytical shall be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Malytical. We strongty urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. '�� i� :�di�:a� I � Page 13 of 15 i i Serial_No:06091512:41 ' ; . + . �i Certification Information � Last revised December 16,2014 '��.. i The following analytes are not included in our NELAP Scope of Accreditation: i Westborough Facility � EPA 524.2:Acetone, 2-Butanone(Methyl ethyl ketone (MEI�),Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, ' 1,3,5-Trichlorobenzene,4-Methyl-2-pentanone(MIBI�, Carbon disulfide, Diethyl ether. ; EPA 8260C: 1,2,4,5-Tetramethylbenzene,4Ethyltoluene, lodomethane(methyl iodide), Methyl methacrylate, Azobenzene. EPA 8270D: 1-Methylnaphthalene, Dimethylnaphthalene,1,4Diphenylhydrazine. EPA 625: 4-Chloroaniline,4-MethylphenoL ' SM4500: Soil:Total Phosphorus, TKN, NO2, NO3. , EPA 9071: Total Petroleum Hydrocarbons, Oil&Grease. ' Mansfleld Facility EPA 8270D: BiphenyL EPA 2540D: TSS EPA TO-15: Halothane, 2,4,4-Trimethyi-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methyfthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.7: Mercury; EPA 300.0: NiVate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C, SM4500CN-CE, EPA 180.1,SM2130B,SM4500CI-D,SM2320B,SM2540C, SM4500H-B EPA 332: Perchlorate. Microbiology: SM9215B; SM9223-P/A,SM92236-Colilert-QT, Enterolert-QT. Non-Pofable Water EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn; EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; EPA 245.1,SM4500H,B, EPA 120.1, SM2570B,SM2540C,SM2340B,SM2320B, SM4500CL-E, SM4500E-BC, SM426C,SM4500NH3-BH, EPA 350.1:Ammonia-N, LACHAT 10-107-06-1-B:Ammonia-N, SM4500NO3-F, EPA 353.2: Nitrate-N,SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, SM4500P-B, E,SM5220D, EPA 410.4, SM5210B,SM5310C,SM4500CL-D, EPA 1664, SM14 510AC, EPA 420.1,SM4500-CN-CE,SM2540D. EPA 624:Volatile Halocarbons&Aromatics, I EPA 608: Chlordane, Toxaphene,Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, � EndosuHan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachior, Heptachlor Epoxide, PCBs I EPA 625: SVOC(Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. � Microbfology: SM92236-Colilert-QT; Enterolert-QT,SM9222D-MF. � t I � For a complete listing of analytes and methods, please contact your Alpha Project Manager. Page 14 of 15 . _ : _ _ . . , , ... � ; �g a9 � _= �n �a � m€��adnm a o '° .. �` Q c�m� r � ¢ 8 v° ° �o° 8 � -uonEa_'m� V � � w c i E � 9 & €. ":$-�a`wd N 3e a � o o a 2 a ; nE �4o'R- $n r o � E o z 3 m � mm aE g�a'Pm�SEQ� �n - e � �a - � n- .� `nO � � ¢ OB.n wu nmc��8:2 � � J � ❑ o � m Z # m � -� I � . � � t�1 c0 -� � � � O !f � � a in 'c � f✓ M . a • � � ❑ ❑ - r 1 i s I � � a � m �. > m i •d 0 � � � O >?� i � a g� � w a � . � ❑ l � � � n N NNl �� ' , _ � � � N a ❑ x m . � . 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