HomeMy WebLinkAbout2015 Nov 20 - Bennett Environmental Associates, Inc. �K� '
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� BENNETT ENVIRONMENTAL ASSOCIATES, INC. '
LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS
1573 Main Street,P.O.Boa 1743 (508)896-1706
Brewster,MA 02631 faz(508)896-5109
LETTER OF TRANSMITTAL �
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TO: DATE: JOB NUMBER:
Massachusetts Deparhnent of Environmental Protection 11/20/15 BEA13-10609
Attention:Title 5 Program
1 Winter Street-6th Floor
Boston,MA 02108 REGARDING:
Hughes Residence '
17 Dove's Wing Road
SHIPPING METHOD: Yannouth,MA �
G3C�C�C��dGD
Regular Mail � Pick Up �
JNi� U � [ii"I b �
Priority Mail ❑ Hand Deliver ❑ �
Express Mail ❑ Other ❑ HEALTH DEPT. �
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Certified Mail 0 Green Card/RR 0 �
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COPIES DATE DESCRIPTION
1 DEP Approved Inspection and O&M Form for Title 5 UA Treatment and Disposal Systems(June and
September 2015)
1 AdvanTex Field Maintenance Report(June and September 2015)
1 3/19/15 Alpha Analytical Laboratory Report
9/22/15 Alpha Analytical Laboratory Report
For review and comment: � For approval: � As requested: � For your use: � �
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REMARxs: i
Please fmd enclosed the DEP Inspection and O&M Forms, AdvanTex Field Maintenance Reports,and laboratory analytical results for °
operation and maintenance conducted during the reporting period at the above referenced property. If you have any questions or require �
additional information,please contact us at your earliest convenience. Thank you. '
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cc:Yarmouth Board of Hea1th '
Ms.Marilyn Hughes,Property Owner
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FROM: David Bennett WWTO#6243/Samantha Farrenkopf WWTO#13265/Joseph Smith WWTO#12529/Greg BrehmWWTO#16149
If enclosures aze not as noted,kindly notify us at once
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Massachusetts Department of Environmental Protection
� Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A '
Treatment and Disposal Systems
,
A. Installation !
Important:When Marilyn Hughes �
filling out forms Owner
on the computer, '
use only the tab 17 Doves Wing Road
key to move your Facility Street Address
cursor-do not South Yarmouth 02664
use the retum
key. City Zip
� Mailing address of owner, if different:
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� Street Address/PO Box:
�.n +
City State Zip f
(508)542-4622 ext. t
;
Telephone Number
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B. Authorized Service Provider i
Bennett Environmental Associates, Inc. ;
O&M Firm
1573 Main Street/PO Box 1743 �
Street Address �
Brewster MA 02631 f
City State Zip ;
(508) 896- 1706 e�. 129 i
Telephone Number
Samantha Farrenkopf 13265 �
Certified Operator Name Cert�cation Number `
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C. Facility/System Information ;
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Orenco AdvanTex AX-10 '
DEP ID Manufacturer ID Model Number I
7/26/2008 7/30/2008 �
Installation Date Start of Operation !
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial j
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Seasonal Residence—used less than 6 mo./year: ❑ Yes � No '
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D. Operating Information i
3/12/15 9/10/14 ;
Inspection Date Previous Inspection Date +
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Sludge Depth(to be checked yearly) Pumping Recommended ❑ Yes � NO j
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Massachusetts Department of Environmental Protection
Bureau of Resource Protection - Title 5 �
DEP Approved Inspection and O�M Form for Title 5 I/A
Treatment and Disposal Systems
E. Field Testing
_ �
Field Inspection:
Color: ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
Effluent Solids: � no ❑ some
pH 7.0 SU D0 3.0 mg/L Turbidity 5.89 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
gpd �
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS ❑TN� Other(list below) �
N itrate N itrite TKN �
Other 1 Other 2 Other 3 �
G. Inspection and Maintenance �
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Description of any maintenance performed since previous inspection &during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis.
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field
testing.
t5aiom.doc•rev.04-11-13 Page 2 of 3
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Massachusetts Department of Environmental Protection �
Bureau of Resource Protection -Title 5 `
DEP Approved Inspection and O&M Form for Title 5 1/A
Treatment and Disposal Systems
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H. Certification �
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods, �
have completed this report and the attached technology operation and maintenance checklist, and f
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts certifi perator in accordance with 257 CMR 2.00. �
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Operator Signature Dat i
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System owner must submit this report, technology O&M checklist, and any required sampling results i
to the local board of health as follows for each inspection performed: j
Remedial Use—by January 31�of each year for the previous calendar year i
Piloting Use-within 45 days of inspection date
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Provisional Use—by March 31th of each year for the previous 12 months !
General Use—by September 30th of each year for the previous 12 months i
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Send to: �
Department of Environmental Protection �
Attention: Title 5 Program �
One Winter Street, 5th Floor �
Boston, MA 02108 �
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t5aiom.doc•rev.04-11-13 Page 3 of 3
Massachusetts Department of Environmental Protection
; Bureau of Resource Protection -Title 5 '
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
i
A. I nstallation �
I
Important:When Marilyn Hughes '
filling out forms Owner f
on the computer, �
use onty the tab 17 Doves Wing Road �
key to move your Facility Street Address '
cursor-do not South Yarmouth 02664 '
use the retum City Zip
key.
� Mailing address of owner, if different:
�
Street Address/PO Box: �
�I
City State Zip ;
(508)542-4622 ext. '
Telephone Number i
I
B. Authorized Service Provider �
Bennett Environmental Associates, Inc. i
O&M Firm �
1573 Main Street/PO Box 1743
Street Address �
Brewster MA 02631 ?
City State Zip
(508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265
Certified Operator Name Certification Number
C. Facility/System Information
Orenco AdvanTex AX-10 �
DEP ID Manufacturer ID Model Number �
7/26/2008 7/30/2008 �
Installation Date Start of Operation j
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial �
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No i
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D. Operating Information
9/14/15 3/12/15
Inspection Date Previous Inspection Date
4"sludge, 3"scum Pumping Recommended ❑ Yes � No
Sludge Depth(to be checked yearly)
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t5aiom.doc•rev.04-11-13 Page 1 of 3 ,
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Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5 �
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
E. Field Testing
,
Field Inspection: �
Color: ❑ gray ❑ brown � clear ❑turbid �
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
EfFluent Solids: � no ❑ some
pH 7.0 SU p� 2.0 mg/L Turbidity 2.53 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Effluent ii
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use �I
nitrogen reducing systems: �
9Pd
Parameters sampled: ❑ pH � BOD 0 CBOD � TSS ❑TN � Other(list below)
Nitrate Nitrite TKN
Other 1 Other 2 Other 3
G. Inspection and Maintenance �
Description of any maintenance performed since previous inspection &during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis.
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field
testing.
t5aiom.doc•rev.04-11-13 Page 2 of 3
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Massachusetts Department of Environmental Protection
Bureau of Resource Protection - Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and j
the information reported is true, accurate, and complete as of the time of the inspection. I am a ;
Massachusetts certified operator in accordance with 257 CMR 2.00. ';
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Operator Signature ~� � Date I
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System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection performed:
Remedial Use—by January 31�of each year for the previous calendar year
� Piloting Use-within 45 days of inspection date
Provisional Use—by March 31t^of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5�' Floor
Boston, MA 02108
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Quarterly lnspection �508� 895-17os k
Property Ownerll'rackfng 0 � �P�� �
Marilyn Hughes f f 7:.D�.�� � � I
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97 Raves 1Ning Rd,Yarmouth MA 42664 (5�8}542-4622 i
AX Stte!D @ Caunty tp# Pod A RTU�/t!L# Date af L.ast Inspectinrt �
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Odor. �(+lnrtnal ❑P�gem Lafera(s/Oriffces� �
Perform FPeld SamplinglObserva#ions � �
Bioma� armal ❑Ekc�sive Pod Boftom
N7U(18�NT,Us} pH(&S) �(7-6J �rtdging/pomiing: �one/Minor ❑Excessive intake Vent.,�,.�; ,Q ❑
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Odor of Sampte lnsy�peci fnspect Clean {
Riset/L9d (L.. F�� � � ' i
Typicai �Musty ❑�hy ❑Moldy o �
3plice Bax � Pump
Non-typicai SaifEda ❑Cabbage ❑Decay
Float cnrds � f
4ily film la PVU ❑Yes �No
�oam ire t�ank ❑ves No Inspeat(Service 4ther System Components �
Inspect Ciean I pecf Clean `
Ch�Ck C011t1'ol Pane1 I�isinf�l[on Equipmerrt ❑ ❑ Dispersa!La#erals/Oritices� ❑ �
Recirc Amps Discharge Amps i
,� Observatlons �
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❑Clear�ed tsxtila sheeE.s? ❑Replaced W itemsZ �
Audible and visuai afarrns OK '
� ❑Replaced/Used other items7 �
Dlai tone(telernetry wdy) Yes !
Parts Used;W=1Narranty,B=RillabEe�✓ap}�ropriate selection}
inspect/Clean Pump System w s nem Number Deacrlptlon '
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.........Ir�s,�p,e{c�t Clean ;
Rtser/Licl ........... L�J G
Sptice Box.....•-•........... � . ;
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� Flaat Cartis .................. �
r„_ �loats........................ ❑ Fin�allSafety Inspection �
�" Pump........................ ❑ �RSV reinstal{eci �Lids boltad on ;
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� Biotuhe"Ftlter................. ❑ ��`nwanifatd reconnected;flosh vaives closed Contro!panel reactivated ;
�i 8€oiube Pump Vault ....._...... ❑ Summary/Recommendations �
� Recirculating Spli#ter Vafire....... � ❑ System pec#orming;no further action r►eeded ❑Tank needs pumping , � �
�'"� r�Cali for servtc - / (- t �JO�er?_ /
� Comme{nts �� i j � 2l'���:%, C��(t"G�� , E=. � o,�� `1f�..aLt/; L G/SJ'P `P G�
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A�Iva�ex� Field Main�enanee Report gennefit Environmental Associ�
Quarterly inspection (508) 896-�706
Property Ownw/�racidng� Operatnr
Marilyn Hughes �a� "�,.�`Yv.,��• j��-� >� ,
Site A+fdreas Cn Phnne . .
17 Do�es Wing Rd,Yarmouth MA 02664 (508)542-4$22 �
AX SNa IQ R Ca�ty 1D @ Pad� RN AtUL� Date f Last 1 speciion �
Ax-��s�as 4o�ss �-ru�2s7�s � (Z ( 5 ;
Retrleve O&M Infa Measure Studge/Scum �
Dafiy flaw Sladge Scum �
istCompartment CurGe�t�` Previo3l\ Cun�E{, Previaus�l\ ( ;
Recirc ratio � � I
Tuner settings: �
� 3 ,� � y� ��� ^ � � � 2rrct compartment currere�� Previou�� cu e�` Frevrou��\ ;
t Z' �� C�` 4
1��, � � �'�,�_ �p Inspeot/Clesn AdvanT�Pilter '
$ �t i E
Odoc Narmai ❑Punger�t LaEerals/Orifices j
Pertorm Field SampiinglObservations 4
Btotrtat: Normal ❑Excessive ?od Bottom
NTU(ts±Nlvs) pH(6-9) �O I2-B) BrtdginglPanding NaneJM�or ❑Excessive Intake Vent ❑ �
2��� � �� liL� Ins�eat/Clean Discharge Pump System f
Odar of Samp e Insp ct Insp Clean i
Typloal �.O�usty ❑Earthy ❑Mo1dy Rfserli.td _ Fioats ❑
Tlon-typicai ❑Sutfide ❑Ca6b e ❑pecay sp�i�B� Pump ❑ �
Float cords �
091y fi�m in PW ❑Yes No ±
Foam in tank ❑Yes Mo InspecUService Other System Gomponents ;
rnspect crean t eot j
Check Control Panel Disinfection Eqaipment ❑ ❑ �jA��t
R�irc Amps Rischarge AmPs phse�ya�ons �
� ��� � 1� ditional Servfces Etendered ;
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Cleaned fextile sheets? ❑Replaced UV iterns? E
Audible and vlsuaE afarms �OK
{�� ❑ fac�llUsed other items? i
Dial fone{telemefry only) ❑Yes t Q�I No k
`f t Parts Used:W=Warranty,8=.Bilhable{✓approprfate setection) i
inspeot/Clean Pump System w B Item Number Descrlption '
. Insp E Glean t
RisedLid ................ . �
Splice Sox..................::� 4
Ftoat Gords.................
�toats........................ �, �' Safety Inspection
. pump...................... SV reinstalled ids hotted on
Btotube°Fitier.................� Manifold reconnected;flush vaives closed Co�rol panel reactivated
Biotuhe Pump Vault ............ �ry/�����endatians
Recirculating Spl'dter Va(ve....... �System perfiorming;no#urther action needed ❑Tank needs pumping �
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` ❑Casl far senriee ❑Otlte f
Commen 'l �.'� ` -1.^+ti�\� �9J'.f'./`"� � V".a.'>> 4 � � f
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IFax cornpleted farm to 7�866-�384-7404 ;
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Serial_No:03191514:06 '
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T I C A L i
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ANALYTICAL REPORT
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Lab Number: L1504802 �
Client: Bennett Environmental Associates �
1573 Main Street �
Brewster, MA 02631
ATTN: David Bennett �
Phone: (508)896-1706
Project Name: HUGHES RESIDENCE
Project Number: BEA13-10609
Report Date: 03/19/15
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The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced oniy in its
entirety.Alpha Analytical holds no responsibility for results and/or data.that are not consistent witfi the original. '
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L221�,USDA(Permit #P-330-11-00240).
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Eight Walkup Drive,Westborough, MA 01581-1019 �
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com �
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Page 1 of 15
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Serial No:03191514:06
� Project Name: HUGHES RESIDENCE Lab Number: L1504802 ;
Project Number: BEA13-10609 Report Date: 03/19/15 :
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation ,
or analysis unless othervvise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. ��i
Results contained within this report relate only to the samples submftted under this Alpha Lab Number and meet all of the requirements of ,
NELAC,for all NELAC accredited parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample
specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample, :
followed by the Laboratory.Batch Quality Control at the end of each parameter.If a sample was re-analyzed or re-extracted due to a '
required quality control corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is
designated with an"R"or"RE",respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the '
associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific°r6
recovery or RPD value that is outside the listed Acceptance Criteria is balded in the report.All specific QC information is also incorporated in �
the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments, ;
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solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this �
report are provided in the Glossary located at the back of the report.
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In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods allow for some �
quality control failures to occur and stiil be within method compliance. In these instances the specific failure is not narrated but noted in the �
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed �
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody. �
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
from the date the project is compieted.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will
be disposed after 3 business days from the date the project is completed.
Please contact Client Senrices at 800-624-9220 with any questions.
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I,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained ,
in this analytical report,such information is accurate and complete. This certificate of analysis is not ;
complete unless this page accompanies any and all pages of this report.
��,_., C�ntt�ia MFtQueen
Authorized Signature: �
Title: Technical Director/Represen#ative Date: 03/19/15
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Serial No:03191514:06
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INORGANICS
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MISCELLANEOUS
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Page 4 of 15
, Serial No:03191514:06 '
, Project Name: HUGHES RESIDENCE Lab Number: L1504802 '
Project Number: BEA13-10609 Report Date: 03/19/15 '
SAMPLE RESULTS
Lab ID: L1504802-01 Date Collected: 03/12/15 15:45
CII@tlt ID: EFFLUENT Date Received: 03/13/15
S8Il1pl@ LOCB#IOtI: SOUTH YARMOUTH,nna Field Prep: Not Specified
Matrix: Water '
Dilutlon Date Date Analytical '
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
�eneral Chemistry Westborough Lab;: �.- '. : .; _ , _ . . . :.. =�_.., _.. . _.f _
Solids,Total Suspended 5.3 mg/I 5A NA 1 - 03/16/15 18:35 30,2540D JT
Nitrogen,Nitrite 0.27 mg/I 0.050 - 1 - 03/13/15 23:10 44,353.2 DE
-----------------...----------_.--------------....-----...--------------------------------.._....-----_._._._-----...—...______-----.._..-----...........--------........._------ -------_----....-----.__..........._.__..- ---------
Nitrogen,Nitrate 15. mg/I 0.50 -- 5 - 03/14115 00:09 44,353.2 DE �
— --------_._.._.__..._..----..�__^.__.___.._..—.._._._......__ -�----.—�_._...,------ ---------._..
Nitrogen,Total Kjeldahl 3.59 mgil 1.50 - 5 03/16/1514:30 03/18/15 21:32 30,4500N-C AT
— ------ - --------- ----- �
BOD,5 day 6.2 mg/I 2.0 NA 1 03/13l15 22:20 03/18/15 17:25 30,5210B SE �
�_.---._.__--.-------------___---------..-------------------------._-_.__...__ --------------------------------------------- -_--------------------- C
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Serial_No:03191514:06 �
Project Name: HUGHES RESIDENCE Lab Number: L1504802 -
Project Number: BEA13-10609 Report Date: 03/19/15
Method Blank Analysis
Batch Quality Control
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst ,
Gener�l Ghemistry,,�1Nestborougti Lab fqr sample(s) .,01 Batch. WG768180-1 ; � .: , F..,. , ��,������ '.;;
BOD,5 day ND mg/I 2.0 NA 1 03/13l15 22:20 03/18/1517:25 30,52106 SE
General Ghemis�try 1Nestboro�ghn Lab for sample(s): 01 Batch: 1NG768183-1 a, a. � ; ,,,,� �,�,„� ,�w, ���_;.,',
Nitrogen,Nitrate ND mg/I 0.10 — 1 - 03/13/15 22:46 44,353.2 DE
General Chernistry.-Westborou,g'ti Lab fo�sample(s): 01 Batch: WG768184-1 - T :
Nitrogen,Nitrite ND mg/I 0.050 -- 1 - 03/13/15 22:49 44,353.2 DE
_
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG768525=1
NiVogen,Totai Kjeldahl ND mg/I 0.300 — 1 03/16/15 14:30 03/18/15 21:13 30,4500N-C AT
General Chemistry-Westborough Lab for sample(s): D1 Batch: WG768537-1 '
Solids,Total Suspended ND mg/i 5.0 NA 1 - 03i16/75 18:35 30,2540D JT
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Serial No:03191514:06
Project Name: HUGHES RESIDENCE Lab Number: L1504802 �
Project Number: BEA13-10609 Report Date: 03/19/15
Sample Receipt and Container Information
Were project specific reporting limits specified? YES
Reagent H20 Preserved Vials Frozen on: NA �
Cooler Information Custody Seal j
Cooler
A Absent ,
(
(
Container Information Temp
Container ID Container Type Cooler pH deg C pres Seal Analysis(*)
L1504802-01A Plastic 500m1 H2SO4 preserved A <2 3.0 Y Absent TKN-4500(28)
L1504802-016 Plastic 950m1 unpreserved A 8 3.0 Y Absent NO2-353(2),BOD-5210(2),NO3-
353(2)
L15U4802-01C Plastic 950m1 unpreserved A 8 3.0 Y Absent TSS-2540(7)
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"Values in parentheses indicate holding time in days
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Page 10 of 15
' II
Serial No:03191514:06 I
. Project Name: HUGHES RESIDENCE Lab Number: L1504802 ;
Project Number: BEA13-10609 Report Date: 03/19/15 i
GLOSSARY ;
�
Acronyms �
EDL -Estimated Detection Limit:This value xepresents the level to wluch target analyte concentrations are reported as estimated i
values,when those target analyte concentrations aze quantified below the reporting limit(RL).The EDL includes any
adjustments from dilutions,concentrations ar moishire content,where applicable.The use of EDIs is specific to the analysis of i
PAHs using Solid-Phase Microextraction(SPME).
EPA -Environmental Protection Aaency. i
r
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes �
or a material containing known and verified amounts of analytes. ;
LCSD -Laboratory Control Sample Duplicate:Refer to LCS. !
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes
or a material containing known and verified amounts of analytes. ;
MDL -Method Detection Limit:This va(ue represents the level to which tazget analyte concentrations are reportecl as estimated values,
when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjustments from
dilutions,concentrations or moisture content,where applicable. k
MS -Matrix Spike Sample:A sample prepazed by adding a known mass of target analyte to a specified amount of matrix sample for �
which an independent estimate of target analyte concentration is avaIlable.
MSD -Matrix Spike Sample Duplicate:Refer to MS. �
NA •Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utdized in the calculation are non-detect at the pazameter's i
reporting unit. �
NI -Not Ignitable.
RL -Reporting Limit: The value at which an instrument can accurately measure an analyte at a spec�c concentration.The RL
includes any adjustments from dilutions,concentrations or moistLue content,where applicable.
RPD -Relative Percent Difference: The results from matrix and/or matrix spike duplicates aze primarily designed to assess the precision
of ana(ytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less than five
times the reporting limit for any individual parameter aze evaluated by utilizing the absolute difference between the values;
although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a lrnown or certified value that is of the same or similar matrix as the
associated field samples.
!
Footnotes
1 -The reference for this anatyte should be considered modified since tivs analyte is absent&om the tazget analyte list of the original
method. ,
Terms
Total:With respect to Organic analyses,a'Total'result is defined as the summation of resu(ts for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and the analytical reference method.(E�mple:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Qualifiers �
A -Spectra identified as"Aldol Condensation Product". �
B •The analyte was detected above the reporting limit in[he associated method blank.Flag only applies to associated field samples that �
have detectable concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank.For MCP-related f
projects,flag only applies to associated field samples that hav.e detectable concentrations ofthe analyte at less than ten times(1�) �
the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable �
concentrations of the analyte at less than ten times(10�c)the concentration found in the blank AND the analyte was detected above �
one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ- �
Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the �
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
C -Co-elution:The tazget analyte co-elutes with a known lab standard(i.e.surrogate,intemal standazds,etc.)for co-exVacted
analyses.
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations '
of the analyte. �
E -Concentration of analyte exceeds the range of the calibration curve andlor lineaz range of the instnunent. �
€
Report Format: Data Usability Report (
e.� `
I
Page 11 of 15 �
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Serial No:03191514:06 ;
Project Name: HUGHES RESIDENCE Lab Number: L1504802 -
Project Number: BEA13-10609 Report Date: 03/19/15 �
Data Qualifiers
G -The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should
be considered estimated.
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. '
I -The lower value for the two colwnns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reportino Limit for this analyte.
t
NJ -Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral library search �
P -The RPD between the results for the two columns exceeds ihe method-specified criteria (
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration �
Standard exceedences aze also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less E
than Sx the RL.(Metals only.) �
R •Analytical results aze from sample r�analysis. (
RE -Analytical results are from sample re-extraction. k
S -Analytical results aze from modified screening analysis.
J -Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(T'ICs).
ND •Not detected at the reporting limit(RL)for the sample.
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Repo►t Formafi Data Usability Report II
.y.. Q/�L '�.',.
Page 12 of 15
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Serial No:03191514:06
, Project Name: HUGHES RESIDENCE Lab Number: L1504802
Project Number: BEA13-10609 Report Date: 03/19/15 �
REFERENCES
30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-
WPCF. 18th Edition. 1992. �
44 Methods for the Determination of Inorganic Substances in Environmental Samples, ;
EPA/600/R-93/100,August 1993. '
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LIMITATION OF LIABILITIES
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perForm the work at iYs own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to,damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. �
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
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Certification Information
Last revised December 16,2014
The following analytes are not included in our NELAP Scope of Accreditation:
Westborough Facility
EPA 524.2:Acetone, 2-Butanone(Methyl ethyl ketone(MEI�),Tert-butyl alcohol,2-Hexanone,Tetrahydrofuran,
1,3,5-Trichlorobenzene,4-Methyl-2-pentanone(MIBI�, Carbon disulfide, Diethyl ether. i
EPA 8260C: 1,2,4,5-Tetramethylbenzene,4-Ethyltoluene, lodomethane(methyl iodide), Methyl methacrylate,
Azobenzene.
EPA 8270D: 1-Methylnaphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine.
�EPA 625: 4-Chloroaniline,4-Methylphenol.
SM4500: Soil:Total Phosphorus, TKN, NO2, NO3.
EPA 9071: Total Petroleum Hydrocarbons, Oil&Grease. �
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Mansfield Facility ?
EPA 8270D: Biphenyl. �
EPA 2540D: TSS
EPA TO-15: Halothane,2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene,Thiophene,2-Methylthiophene, j
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, �
Benzothiophene, 1-Methylnaphthalene.
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The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: ;
Drinking Water �
EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury;
EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N;SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C,
SM4500CN-CE, EPA 180.1,SM2130B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B
EPA 332: Perchlorate. I
Microbiology: SM9215B; SM9223-P/A,SM9223B-Colilert-QT, Enterolert-QT. �
Non-Potable Water
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; �
EPA 245.1,SM4500H,B, EPA 120.1,SM2510B,SM2540C,SM2340B,SM2320B,SM4500CL-E,SM4500E-BC, �
SM426C,SM4500NH3-BH, EPA 350.1:Ammonia-N, LACHAT 10-107-06-1-B:Ammonia-N, SM4500NO3-F, 4
EPA 353.2: Nitrate-N,SM4500NH3-BC-NES, EPA 351.1,SM4500P-E,SM4500P-B, E,SM5220D, EPA 470.4,
SM5210B,SM5310C,SM4500CL-D, EPA 1664,SM14 510AC, EPA 420.1,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608: Chlordane,Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC,delta-BHC, Dieldrin, DDD, DDE, DDT,
Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625:SVOC(Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Page 14 of 15
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ANALYTICAL REPORT
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Lab Number: L1522584
Client: Bennett Environmental Associates �
1573 Main Street �
Brewster, MA 02631 ;
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ATTN: David Bennett i
Phone: (508)896-1706 �
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Project Name: HUGHES RESIDENCE �
Project Number: BEA13-10609
Report Date: 09/22/15 i
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The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its
entirety.Alpha Analytical hofds no responsibility for results and/or data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
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Eight Walkup Drive,Westborough, MA 01581-1019 ;
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com ;
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Serial No:09221519:16
+ Project Name: HUGHES RESIDENCE Lab Number: L1522584 ;
Project Number: BEA13-10609 Report Date: 09/22/15 '
Case Narrative
The sampies were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation �
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
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Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of '
NELAC,for all NELAC accredited parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample '
specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample, �
followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds(TICs),if requested,are ;
reported for compounds identified to be present and are not part of the method/program Target Compound List,even if only a subset of the �
i
TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of
data are reported,the Laboratory ID of the re-analysis or re-e�ctraction is designated with an"R"or"RE",respectively.When multiple Batch !
Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded I
header line of each data table.Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside the listed Acceptance :
Criteria is boided in the report.All specific QC information is also incorporated in the Data Usability format of our Data Merger tooi where it '
can be reviewed along with any associated usability impiications.Soil/sediments,solids and tissues are reported on a dry weight basis ;
unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of
the report.
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In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods allow for some !
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the �
associated QC table.The information is also incorporated in the Data Usabifity format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
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Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numericai '
Standards requested on the Chain of Custody. I
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days �
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will �
be disposed after 3 business days from the date the project is completed. �
Please contact Client Services at 800-624-9220 with any questions. f
I,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report. k
(' �
����,r���� Kelly Stenstrom �
Authorized Signature: �
Title: Technical Director/Representative Date: 09/22/15 �
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Serial No:09221519:16 i
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INORGANICS �
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MISCELLANEOUS
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Serial No:09221519:16 f
; Project Name: HUGHES RESIDENCE Lab Number: L1522584
Project Number: BEA13-10609 Report Date: 09/22/15 ;
SAMPLE RESULTS �
Lab ID: L1522584-01 Date Collected: 09/14I15 13:40
Client ID: EFFLUENT Date Received: 09/14/15
Sa171p1@ LOCatlOtl: SOUTH YARMOUTH,nna Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method qnalyst �
General Chemistry=1Nestborough Lab.', '
8olids,Total Suspended ND mg/I 5A �NA 1 - 09/15/1519:20 30,2540D RP �
-----._...___.._.__......_.._..—._..------...__....----------- ------------------------._�...------..—_....--------------------- ----------.—.. �
Nitrogen,Nitrite 0.18 mg/I 0.050 - 1 - 09/15/15 00:21 44,353.2 ML
--------... ._ _.._....... ._. .-.._....._ _..._-. _____ ---__ --_ _..__._ -.__. ..._._ . _..... . ._.. . _ _. . ___._._..__ .. . __..._.
Nitrogen,Nitrate 19. mg/I 0.50 - 5 - 09/15/15 00:48 44,353.2 ML
---------...._....-------------------- ---------__.._..--------- --_.....------ -----
Nitrogen,Total Kjeldahl 3.42 mgll 1.50 - 5 09/16/15 07:27 09/16/15 22:33 4,351.3/.1 (M) AT
---------------....----._..._----------- - --...------..__....----- ----_------.�..--------_.._
BOD,5 day 16. mg/l 2.0 NA 1 09l14/15 23:55 09/19/15 17:55 30,52106 SE
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Page 5 of 15 �',
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Serial No:09221519:16
Project Name: HUGHES RESIDENCE Lab Number: L1522584 �
Project Number; BEA13-10609 Report Date: 09/22/15
Method Blank Analysis
Batch Quality Control
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry=-Westborough Lab for sample(s): 01 Batch:-WG821181-1
BOD,5 day ND mg/I 2.0 NA 1 09/14/15 23:55 09/19/15 17:55 30,5210B SE
General Chemistry-Westborough Lab for sample(s): 01 .Batch: WG821189-1 : ;, ,. ,. '` ;
.
Nitrogen,Nitrate ND mg/I 0.10 -- 1 - 09/14/15 23:37 44,353.2 ML (
— ------ _-----. ._......_.. . - ----._._. ......._-._.— . _...__.... . . ............. _......__ _ _..._. ... .........__. _.__....._ ----...... . ....__..__.____._.----------- --._._... --.._. �
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General Chemistry-Westborough Lap #or sample(s): 01 Batch: WG821190-1 : �
Nitrogen,Nitrite ND mgA 0.050 — 1 - 09/14/15 23:39 44,353.2 ML �
---------- - --__- -- ---- --- ----------- ------ _.._..- -- -- ---------...---- --- �
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG821531-1
Solids,Total Suspended ND mgll 5.0 NA 1 - 09/15/15 19:20 30,2540D RP �
--__ _------—-- ---_ . _.__._...---------.. . .......... ..— --.._._ .. ......_
---...--- _...---- �
General Chemistry-Westborough Lab for sample(s): 01 'Batch: WG821720-1
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Nitrogen,Total Kjeldahl ND mg/I 0.300 — 1 09/16/15 07:27 09/16/15 22:14 4,351.3/.1(M) AT �
__. ..... _..__. _.._..__..... _ ......__.... _.. ......_ .._.._.. ...... .. ......__. _ .._....._..
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Serial No:09221519:16
Project Name: HUGHES RESIDENCE Lab Number: L1522584 ;
Project Number: BEA13-10609 Report Date: 09/22/15
Sample Receipt and Container Information
Were project specific reporting limits specified? YES
Reagent H20 Preserved Vials Frozen on: NA
Cooler Information Custody Seal
Cooler
A Absent
' j
Container Information Temp `
Container ID Container Type Cooler pH deg C pres Seal Analysis(*) �
L1522584-01A Plastic 950m1 unpreserved A 7 3.7 Y Absent NO2-353(2),BOD-5210(2),NO3- �
353(2) i
L1522584-01 B Plastic 250m1 H2SO4 preserved A <2 3.7 Y Absent TKN-351(28) �
L1522584-01C Plastic 950m1 unpreserved A 7 3.7 Y Absent TSS-2540(7) �
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*Values in parentheses indicate holding time in days �' ��,��
Pa e 10 of 15 i�`�'^"`
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Serial No:09221519:16
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Project Name: HUGHES RESIDENCE Lab Number: L1522584
Project Number: BEA13-10609 Report Date: 09/22/15 �
GLOSSARY
Acronyms '
EDL -Estimated Detection Limit:This value represents the level to which target analyte concentrations aze reported as estnnated
values,when those target analyte concentrations aze quantified below the reporting limit(RL).The EDL includes any �
adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis of f
PAHs using Solid-Phase Microextraction(SPME). k
EPA -Environmental Protection Agency. I
LCS -Laboratory Control Sample:A sample matrix,&ee from the analytes of interest,spiked with verified known amounts of analytes �
or a material containing known and verified amounts of analytes.
LCSD -Laboratory Conh•ol Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free&om the analytes of interest,spiked with verified known amounts of analytes !
or a material containing known and verified amounts of analytes.
MDL -Method Detecdon Limit:Tlus value represents the level to wluch tuget analyte concentrations aze reported as estimated values,
when those target analyte concentrarions aze quantified below the repor[ing limit(RL).The MDL includes any adjustments from
dilurions,concentrations or moisture content,where applicable. '
MS -Matrix Spike Sample:A sample prepazed by adding a lmown mass of target analyte to a specified amount of matrix sample for
which an independent estimate of tazget analyte concentration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -NotApplicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation aze non-detect at the parameter's j
reporting unit.
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NI -Not Ignitable. .
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RL �
includes any adjustments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percenf Difference: The results&om matriaz and/or matrix spike duplicates aze primazily designed to assess the precision
of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which aze less than five
times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values;
although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a laiown or certified value that is of the same or similar mafrix as the
associated field saznples.
TIC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target coinpound list
(TQ.)for the method and/or progiam.All TICs are qualitatively identified and reported as estimated wncentrations. k
Footnofes
1 -The reference for this analyte should be considered modified since tlus analyte is absent from the target analyte list of the original'
method.
Terms
Total:With respect to Organic analyses,a'Total'result is defined as the swnraation of results for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Qualifiers 4
f
A -Spech-a identified as"Aldol Condensation Product".
B -The analyte was detected above flie reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank.For MCP-related �
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox) �
the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable i
concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab contazninants)in the associated method blank.For NJ- '
Air-related projecls,flag only applies to associated field samples fliat have deteetable concentrations of the analyte above the
reporting limit.For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
C -Co-elution:The target analyte co-elutes wifli a known lab standazd(i.e,sunogate,internal standazds,etc.)for co-extracted
analyses.
Report Format: Dafa Usability Report
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Serial No:09221519:16
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Project Name: HUGHES RESIDENCE Lab Number: L1522584 ,�
Project Number: BEA13-10609 Report Date: 09/22/15
Data Qualifiers
D -Concentrarion of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrarions
of the analyte.
E -Concentration of analyte exceeds the range of the calibration curve and/or lineaz range of the instrument.
G -The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should i
be considered estimated. ;
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collecfion. i
i
I -The lower value for the two columns has been reported due to obvious interference.
4
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for this analyte. !
NJ -Presumptive evidence of compound.This represents an estunated concentration for Tentatively Identified Compounds(TICs),where �
the identification is based on a mass spectral library seazch. �
P -The RPD between the results for the two colucuns exceeds the method-specified criteria. �
Q -The quality conhol sauiple exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration �
Standard exceedences aze also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries i
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than Sx the RL.(Metals only.)
R -Analytical results are from sample re-analysis. 4
4
RE -Analytical results are from sample re-extraction.
S -Analytical results are from modified screening analysis. `
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J •Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(TICs).
ND •Not detected at the reporting lixnit(RL)for the sample. �
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Report Format: Data Usability Report
__��L,`�"`�.
Page 12 of 15
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Serial_No:09221519:16 ;
~� Project Name: HUGHES RESIDENCE Lab Number: L1522584 �
Project Number: BEA13-10609 Report Date: 09/22h5 '
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REFERENCES '
4 Methods for Chemical Analysis of Water and Wastes. EPA 600/4-79-020. Revised j
March 1983. `
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30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA- �
WPCF. 18th Edition. 1992. �
44 Methods for the Determination of Inorganic Substances in Environmental Samples, �
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EPA/600/R-93/100,August 1993. j
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LIMITATION OF LIABILITIES }
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Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing ;
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical ,
shall be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable .
for any incidental, consequential or special damages, including but not limited to, damages in any way �
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. �
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling, �
containers,sampling procedures, holding time and splitting of samples in the field.
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Serial No:09221519:16
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Certification Information
Last revised December 16,2014
The following analytes are not included in our NELAP Scope of Accreditation: ;
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Westborough Facility ;
EPA 524.2:Acetone,2-Butanone(Methyl ethyl ketone(MEK)),Tert-butyl alcohol, 2-Hexanone,Tetrahydrofuran,
1,3,5-Trichlorobenzene,4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether.
EPA 8260C: 1,2,4,5-Tetramethylbenzene,4-Ethyltoluene, lodomethane(methyl iodide), Methyl methacrylate,
Azobenzene. �
EPA 8270D: 1-Methylnaphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 625: 4-Chloroaniline,4-Methylphenol. �
SM4500:Soil:Total Phosphorus,TKN, NO2, NO3.
EPA 9071: Total Petroleum Hydrocarbons, Oil&Grease.
Mansfield Facility E
EPA 8270D: Biphenyl. �
EPA 2540D: TSS
EPA TO-15: Halothane,2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene,Thiophene,2-Methylthiophene, !
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, �
Benzothiophene, 1-Methylnaphthalene.
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The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: �';
Drinking Water i
EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; �
EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C,
SM4500CN-CE, EPA 180.1, SM2130B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B j
fPA 332: Perchlorate. �
Microbiology:SM9215B; SM9223-P/A,SM9223B-Colilert-QT, Enterolert-QT. r
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Non-Potable Water �
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn; i
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn;
EPA 245.1,SM4500H,B, EPA 120.1,SM2510B,SM2540C,SM2340B, SM2320B,SM4500CL-E,SM4500E-BC,
SM426C,SM4500NH3-BH, EPA 350.1:Ammonia-N, LACHAT 10-107-06-1-B:Ammonia-N, SM4500NO3-F, �
EPA 353.2: Nitrate-N, SM4500NH3-BC-NES, EPA 351.1,SM4500P-E,SM4500P-B, E,SM5220D, EPA 410.4, ;
SM5210B,SM5310C,SM4500CL-D, EPA 1664,SM14 510AC, EPA 420.1, SM4500-CN-CE,SM2540D. '
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608: Chlordane,Toxaphene,Aldrin,alpha-BHC, beta-BHC, gamma-BHC,delta-BHC, Dieldrin, DDD, DDE, DDT,
Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625: SVOC(Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology:SM9223B-Colilert-QT; Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Page 14 of 15
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