HomeMy WebLinkAbout2016 Jul 29 - Bennett Environmental Assoc. Inspection & Alpha Lab Reports :
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BE�Tl�E'TT �Ni�IR�I�TMEN'�AL ASSO�IATES� Il�TC.
LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS
1573 Main Street,P.O.Box 1743 (508)896-1706
Brewster,MA 02631 fag(508)896-5109
LETTER OF TRANSMITTAL
TO: DATE: JOB NUMBER:
Massachusetts Department of Environmental Protection �/29/16 BEA13-10579 �
Attention: Title 5 Program ��
1 Winter Street-6th Floor
Boston,MA 02108 REGARDING:
Drinane Residence
12 Dove's Wing Road
SHIPPING METHOD: South Yannouth,MA 02664
Regular Mail Pick Up ��,��� r -" �2 �
❑ ❑ �.���..���,� i
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Priority Mail ❑ Hand Deliver ❑ �, i
❑ ''"i i
Express Mail ❑ Other ,
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Certified Mail � Green Card/RR � H EALTH D��T. i
COPIES DATE DESCRIPTION
1 DEP Approved Inspection and O&M Form for Tide 5 UA Treatment and Disposal Systems(December
2015,June 2016)
1 Singulau Service Inspection Checklist(December 2015,June 2016)
1 12/22/15 Alpha Analytical Laboratory Report
1 6/16/16 Alpha Analytical Laboratory Report
For review and comment: � For approval: � As requested: � For your use: 0
REMARKS:
Please fmd enclosed the DEP Inspection and O&M Forms,Singulair Service Inspection Checklists,and laboratoiy analytical results for
operation and maintenance conducted during the reporting period for the above referenced property. If you have any questions or require
additional information,please contact us at your earliest convenience. Thank you.
cc:Yarmouth Board of Health
Lee Drinane,Property Owner
Robin Cassidy-Norweco[via email]
FROM: David Bennett WWTO#6243/Samantha Farrenkopf WWTO#13265/Joseph Smith WWTO#12529/Greg BrehmWWTO#16149
If enclosures aze not as noted,kindly notify us at once
_ �
` Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 1/A
Treatment and Disposal Systems
A. Installation
Important:When Lee Drinane
filling out forms Owner
on the computer,
use only the tab 12 Dove's Wing Road
key to move your Facility Street Address
cursor-do not South Yarmouth 02664
use the return City Zip
key.
� Mailing address of owner, if different:
�
StreetAddress/PO Box:
r�sn
City State Zip
(508) 398-3280 ext.
Telephone Number
B. Authorized Service Provider
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Zip
(508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265
Certified Operator Name Certification Number
C. Facility/System Information
Singulair 960 NR
DEP ID Manufacturer ID Model Number
7/2/08 7/8/08
Installation Date Start of Operation
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No
D. Operating Information
12/10/15 6/3/15
Inspection Date Previous Inspection Date
6"sludge, 1"scum
Sludge Depth(to be checked yearly) Pumping Recommended ❑ Yes � No
t5aiom.doc•rev.04-11-13 Page 1 of 3
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Massachusetts Department of Environmental Protection '
Bureau of Resource Protection - Title 5
DEP Approved Inspection and O&M F'orm for Title 5 I/A
Treatment and Disposal Systems
E. Field Testing
Field Inspection:
� Color: ❑ gray ❑ brown � clear ❑ turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offer�sive ❑ turbid
Effluent Solids: � no ❑ some
pH 7.0 SU p� 3.0 mg/L Turbidity 2.47 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Efftuent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
gpd
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS� TN � Other(list below)
N itrate N itrite TKN
Other 1 Other 2 Other 3
G. Inspection and Maintenance
Description of any maintenance performed since previous inspection &during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis.
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters. Final dosing pump chamber was inspected and mechanical components are operating
correctly.
t5aiom.doc•rev.04-11-13 Page 2 of 3
` Massachusetts Department ofi Environrr�ental Protection
Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: 1 have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusett ified operator in accordance with 257 CMR 2.00.
_ � � _ �I���lr
`Operator Signature D ta e
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection pertormed:
Remedial Use—by January 31 St of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31th of each year for the previous 12 months
General Use—by September 30t''of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108
t5aiom.doc•rev.04-11-13 Page 3 of 3
' Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
A. I nstallation
Important:When Lee Drinane
filling out forms Owner
on the computer,
use only the tab 12 Dove's Wing Road
key to move your Facility Street Address
cursor-do not South Yarmouth 02664
use the return C�ty Zip
key.
r�
Mailing address of owner, if different:
Street AddresslPO Box:
terten
City State Zip
(508) 398-3280 ext.
Telephone Number
B. Authorized Service Provider
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Zip
(508)896- 1706 ext. 129
Telephone Number .
Samantha Farrenkopf 13265
Certified Operator Name Certiflcation Number
C. Facility/System Information
Singulair 960 NR
DEP ID Manufacturer ID Model Number
7/2/08 7/8/08
Installation Date Start of Operation
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No
D. Operating Information
6/10/16 12/10/15
Inspection Date Previous Inspection Date
Sludge Depth(to be checked yearly) Pumping Recommended ❑ Yes � No
t5aiom.doc•rev.04-11-13 Page 1 of 3
�
Massachusetts Department of Environmental Protection �
Bureau of Resource Pro#ection - Title 5
DEP Approved Inspection and O&iVl Forrri for Title 5 I/A
Treatment and Disposal Systems
E. I�ield T`esting
Field Inspection:
Color: ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
Effluent Solids: � no ❑ some
pH 6.0 SU p� 5.0 mg/L Turbidity 0.56 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
gpd
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS ❑TN� Other(list below)
Nitrate Nitrite TKN
Other 1 Other 2 Other 3
G. Inspection and Maintenance
Description of any maintenance performed since previous inspection &during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis.
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters.
t5aiom.doc•rev.04-11-13 Page 2 of 3
c
Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5
DEP Approvec! Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts ce � � d operator in accordance with 257 CMR 2.00.
�Z�tlt�
Opera or Signature Date
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection performed:
Remedial Use—by January 31�of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31'h of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108
t5aiom.doc•rev.04-11-13 Page 3 of 3
:
SIN��LT�,E��t. 9b� I�1����`I`�+�1-L�I'�I� T��+ ATI�I�T� SYS�'El�
��RVICE INSPECT:I4N CHECKLIST
5
Address: �2. �1�5 �--'�1^� �� Owner: �Y'�1n�'�r�
Operatar.�'t-' �Vn��-'�,�• � "j���� L�v�z.. Date: �2��1`�� �� \�"� ��r '� �
This checklist summarizes the service procsdures#o be performed during aroutine Singulair 960 NR inspection Rsfez-to the
Singuiair Manuat for a detailed expianation of each service procedure and an O&M�roubleshooting guide.
CONTROL C�+NTER SERVICE NOTFS/COMII�ENTS
�hecic operation o£cflntrol center �� �titr• �f�.•w"' ��,,•f'C, . V�^"''� )
OAdjusttim.eclockwhenrequired t,� -��, ., ��-.\ �u�`� ���.�c>\ L.�-�,r"�.
�Check operation of recirculation control panel c .r C_.• W'^=� .n�
NR EFFLUEI�IT RECIR�ULATIOI�T SYSTEM
Check operation af recircutation pump ���.�C.. -��}v�.,� :� Ct��w'� ����"L•
C1 Iiaspect recircula#io:n well&fittings
�,Test Operation
C7 S et recircula.tion rate rate @ min/hr
RAT4R SERVICE
Check aerator operation ���1'��CW' w�S C.�f��Z. �-���-
C�Check aerator power cansumption {�v�. 'b�-�*-.�`�c7 ��-J'v�st-c�-
Check aerator air delivery 1�
Clean s#ainless steel aspirator shaft j � ���-�'.�a.r�--�m �, 5����'"
�Clean aspirator tip -� �^ t•• SLv^^
�Clean fresh air vent uz concrete cover ��,,,,. �;� ��,,,,�,.�,..
C]�nspect aeration chamber contents � ^ �,`` ��w�,.
CLA.RiFICATION CHAMBER SERVICE `
Itemave the Bio-Kinetaa sysbein ��.Q " ��v�-��v ��� � ���=�,�
0 Scrape the clarif'ication charnber r��-.��¢e.
�Inspect the Bio-Static sludge reiurn
�Inspect oixtl�c�upling
�Install a cIean Bio-Kinetic system � �, `,��k:� ..�,. �\� �(' v.r. �.�--
G�F�1 Blue Cxystal feed tube(if installed)
�FiIl Biv Neutralizer feed tube{if installed}
GENERAL SERVICB �
Inspect effiuentpump chamber '� �`�+�.(� G�.�.r-.�rj,�.C' �u S,�..5 L�'� �`'�
Inspect effluent qualit}' C.,,}��l'-a-t..�,v� -
�Inspect outiet line
Q Inspe�t ground water relief point(if install.ed) �ti^•� 5 a� � v SS�`l
�Inspect effluent disposal system f. �'-M .�� :`�5 C,�,r'w�.��.
�Complete owner service record
❑C�mplete health deparhnent nai'af�ication � ' � �.,v �4��tr:. U,�,t�y
�Complete dislribu#or service record �..r,r.t, U
❑Mait health deparfinent notification
g� ��'� �� �,�� �`� tic� �.,,r�-`Z,,��1 c� �` �� ?`-^��� °��
Si und Envirorimentat Services Inc. F��'��` i
{�� FL IU D THiNKFIVG.CLEAR SOLUTIOI3sh� l ��� � � �
•�]G j ,.''� �� �G�-� V �`�`7j�' [� 1'� �vw.sie�nund�roun.com.�J�J�,�J,I�V� L�V c�o•n�� ����-� i
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�E]E�.VICE It'�SPE�TI�N CI--�+CKLI�T
Address: ��I�'�'�_, �� ��t�-�L�`��wner. ��`j.�"��t.� .
Operator. "'�-Yi �_�� 1t� �!�� � Date: �r�11�C3��'� ����� `
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This checklist sum�►arizes the service procedwres to be performed dzuYng a routine Singulair 950 NR insgection.Refex to the
Singuiair Manual for a�etailed explanation of each service procedure and an O&M tronbleshooting guide.
CONTROL CENTER SERVICE NUTESICOIIIAIENTS
�Check operationaf control center `�j'�� ;;�L� ��l"Cr� Gw-�,`�`��.�. �+gry
�Adjust time clock w13en required �_c�, ����v�.C.'�-c.`�,. t��z'.�i�,.�'`� . i
Check ogeration of xecirculatzon conirol panel ;
I
EFFLUENT RECIRCi7LATI01�SYSTEM I
Check operation ofxecirc�Iation pump ;`�.��i l�f- • �1��N�..� �t ' vw.�.
C�'Inspect recirculation well&fittings _�,�f,�.����
�Test Operation
C7 Set recirculatiort rate rate @ min/hr
RATOR SERVICE
Check aeratar aperation �
Check aerator power consumption ���C�'a,� c'�� t . � rs�" +��a2�-�'e�
Check aerator aix deiivery +�,�� t'��,t�►S-��et-�
Ciean seainless stee]aspirator shaft
Clean aspirator tip
Clean fresh air veut in concxeie cover
D Inspect aeration chamber contents
C AltIFICATTON CHAMBER SERVICE
Remove the Bio-Kineti.c system � ;� ,� �E� ��i�,�r`�'��-- .�V��'
�crape the clarification chamber �L��—i,r�-c��p��c�l2-� �[�.�-�-t��G�
. �sgect the 8io-Static slutlge return
� �ect outlet coupling � U � :��`
�`Install a clean Bio-Kinetic system
l�Fi11 Blue Ciystal feed tube{if installed)
C�Fi31 Bio-Neulralizer feed fube(if inst�lled)
'�� ��G N�R.A.L SERVICE � - ... ;�;,:.,_: ...:�.,�`3
Inspect ef�-Iuen#pump chamber �' � �}-�_ ('i 19- ' ;
• � Inspect efIluent quality r - ���"'- �.. . ` ,; .
❑Inspect outlet line -�`� -' �- � ;
�Inspect ground water reli ef point(if ins#alled} . �,�c �
O Inspect effl�tent disposal system i�r t• . �- , .
�0 Complete owner service record r j r � ��. ��E��
L�Complete health department notification ��',��.1� � �. �(i.��c�`'� �Y) �3�r�i'��''°�
�Ct Complete distributor service record '(• � ; ��c--�����.
CI Mail health department noti�catzon p�pq :�
�. � �� .` �js� Siegmund Environmental5ervices,Inc.
,,. �}- PT,[JID TFIWI�iVG.CLEAR SOLt3TION8.
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unvwsie�mundtrroup.com
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; Seriai No:12221513:23
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ANALYTICAL REPORT
Lab Number: L1532813
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
ATfN: David Bennett
Phone: (508)896-1706
Projeat Name: DRINANE RESIDENCE
Project Number: BEA13-10579.
Report Date: 12/22/15
The original project report/data package is heid by Alpha Analytical.This reportldata package is paginated and should be reproduced only in its
entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666)�TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.aiphalab.com
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Page 1 of 16
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, Serial_No:12221513:23
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Project Number: BEA13-10579 Report Date: 12/22/15
Case Narrative
The samptes were received in accordance with the Chain of Gustody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Aipha Lab Number and meet all of the requirements of
NELAC,for ail NELAC accredited parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample
specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample,
followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds(TICs),if requested,are
reported for compounds identified to be present and are not par#of the method/program Target Compound List,even if only a subset of the
TCL are being reported.If a sample was re-analyzed or re-extracted due to a required qualiry control corrective action and if both sets of
data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",respectively.When multiple Batch
Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded
header line of each data table.Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside the listed Acceptance
Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data Merger tool where it .
can be reviewed along with any associated usability implications.Soil/sediments,solids and tissues are reported on a dry weight basis
unless otherwise noted.Definitions of ail data qualifiers and acronyms used in this report are provided in the Glossary located at the back of
the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods ailow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tooi where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hoid unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters wili
be disposed after 3 business days from the date the project is compieted.
Please contact Client Services at 800-624-9220 with any questions.
�
Page 3 of 96 =�'�a,
�.,,
Serial No:12221513:23
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Projeet Number: BEA13-10579 Rep�rt Date: 12/2_2/15
Case Narrative(continued)
BOD, 5 day
The WG849287-2 LCS recovery(76°/a), associated with L1532813-01, is outside the acceptance criteria. Due
to the expiration of the method required holding time, no further action was taken.
I,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and atl pages of this report.
�,.,�.���1� Lu ra L Tro1r
Authorized Signature•
Title: Technical Director/Representative Date: 12/22/15
Page 4 of 16 ���`
; Serial No:12221513:23
INORGANICS
&
MISCELLANEOUS
���
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Paqe5of16
Serial No:12221513:23 -
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Project Number: BEA13-10579 Report Date: 12/22/15
SAMPLE RESULTS
Lab ID: L1532813-01 Date Collected: 12/10/15 12:25
Client ID: EFF�uENT Date Received: 12/11/45
Sal'ilplB LOCatlOtl: SOUTH YARMOUTH,Ma Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab
Solids,Total Suspended ND mg/I 5.0 NA 1 - 12/14/15 23:55 30,2540D RP
Nitrogen,Nitrite ND mg/I 0.050 - 1 - 12111/1522:54 44,353.2 MR
---._..._._-------...-- -----._..------------------- - ...._..--------..-------------- _- ------ _-------- --------------------- -----._...---------.....------
Nitrogen,Nitrate 3.2 mg/I 0.10 - 1 - 12/11/1523:16 44,353.2 MR
Nitrogen,Total Kjetdahl 1.61 mg/I 0.300 - 1 12/14/15 18:45 12/15/15 00:57 30,4500N-C AT
BOD,5 day 4.2 mg/I 2.0 NA 1 12/12l15 19�15 12/17/15 23:30 30,52108 RP
__�.s
Page 6 of 16
Serial No:12221513:23
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Project Number: BEA13-10579 Report Date: 12/22/15
Method Blank Analysis
Batch Quality Control
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG849135-1
Nitrogen,Nitrate ND mgfl 0.10 — 1 - 12l11/1522:35 44,3532 MR
General Chemi"stry-Westborough Lab for sample(s): 01 Batch: WG849136-1'
Nitrogen,Nitrite ND mg/I 0.05� — 1 - 12/11/15 22:38 44,3532 MR
General Chemistry-Westborough Lab for sample{s): 01 Batch:-WG849287 9'
BOD,5 day ND mgA 2.0 NA 1 12/12/15 19:15 12/17/15 23:30 30,5210B RP
General Chemistry-Westborough Lab for sample(s): 01 Batch; WG849616-1
Nitrogen,Totai Kjeldahl ND mg/I 0.300 — 1 12/�4/15 18:45 12l15/15 00:35 30,4500N-C AT
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG849672-�
Solids,Total Suspended ND mgA 5.0 NA 1 - 12/14/15 23:55 30,2540D RP
��L�t�A
Page 7 of 16
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, Seriai No:12221513:23
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Project Number: BEA13-10579 Report Date: 12/22/15
Sample Receipt and Container Information
Were project specific reporting limits specified? YES
Cooler Information Custody Seal
Cooler
A Absent
Container Information Temp �
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1532813-01A Plastic 250m1 H2SO4 preserved A <2 3.7 Y Absent TKN-4500(28)
L1532813-01 B Plastic 950m1 unpreserved A 7 3.7 Y Absent NO2-353(2),BOD-5210(2),NO3-
353(2)
L1532813-01C Plastic 950mi unpreserved A 7 3.7 Y Absent TSS-2540(7)
*Values in parentheses indicate holding time in days � �
,
Page 11 of 16 =����'MT„"`
Serial No:12221513:23 .
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Project IVumber: BEA13-10579 Report Date: 12/22/15
GLOSSAI2Y
Acronyms
EDL -Estimated Detecfion L'unit:This value represents the level to which target analyte concentrations aze reported as estimated
values;when those targebanalyte concentraflons aze quantified below the reporting limit(RL).The EDL includes any
adjushnents from dilufions,concenhations or moisture content,where applicable.The use of EDLs is specific to the analysis of
PAHs using Solid-Phase Microextraction(SPME).
EPA. -Environmental Protection Agency.
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified lmown awounts of analytes
or a material containing known and verified amounts of anal}rtes.
LCSD -Laboratory Control Sample Duplicate:Refer to LCS.
LFB. -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes
or a material containina known and verified amounts of analytes.
MDL -Method Detection Limit:This value represents the level to which target analyte concent�ations aze reported as estimated values,
when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjustments from
dilutions,concentrations or moisture content,where applicable.
MS -Matiiac Spike Sample:A sample prepazed by adding a known mass of target analyte to a specified aznount of matrix sample for
which an independent estimate of target analyte concentration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the pazameter's
reporting unit.
NI -Not Ignitable.
NP -Non-Plastic:Term is utilized for tbe analysis of Atterberg Limits in soil.
RL -Reporting Limit: The value at which an instrument can accurately measure an analyte at a spe�ific concentration.The RL
includes any adjustments from dilurions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results from matriac and/or matrix spike duplicates are prunarIly designed to assess the precision
of analytical results in a given matrix and aze expressed as relative percent difference(RPD). Values which are less than five
times Ute reporking limit for any individual pazameter aze evaluated by utilizing the absolute difference between the values;
although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a]mown or certified value that is of the same or similar matrix as the
associated field samples.
S'IZP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TTC -Tentatively Idenrified Compound:A compound that has been identified.to be present and is not part of the target compound list
(TCL)for the method and/or program.All TICs are qualitatively idenfified and reported as estimated concentrations.
Foofnotes
1 -The reference for ttus aaalyte should be considered modified since this analyte is absent from the tazget analyte list of the original
method
Terms
Total:With respect to Organic analyses,a"Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.Tlus is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Bo.th the document from which the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References secdon of the Addendum.
Data Qualifiers
A -Spectra identified as"Aldol Condensafion Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flaa only applies to associated field samples that
have de.tectable concenh�arions of the analyte at less than ten times(10�c)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(lOx)
the concentration found in the blank.For DOD-related projects,fla�only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-hatf the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit.For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,wluch was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
Report Format: Data Usability Report
�h i' a�`
Page 12 of 16 �
• Serial No:12221513:23
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Project Number: BEA13-10579 Report Date: 12/22/15
Data Qualifiers
C -Co-elution:The target analyte co-elutes with a known lab standazd(i.e.surrogate,intemal standazds,etc.)for co-extracted
analyses.
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations
of the analyte.
E -Concenfration of analyte exceeds the range of the calibration curve and/or lineaz range of the instrument.
G -The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should
be considered estimated.
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 xninutes from the time of satnple collection.
I -The lower value for the tv✓o columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for tlus analyte.
NJ -Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds{'I'ICs),where
the identification is based on a mass spectral library search.
P -The RPD between tlie results for the iwo columns exceeds the method-specified criteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DODxelated projects,LCS and/or Continuing Calibration
Standaz•d eacceedences are also qualified on all associated sample results. Note:Tlus flag is not applicable for matruc spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than Sx the RL.(Metals only.)
R -Analytical results are from sample re-analysis.
RE -Analytical results are from sample re-e�traction.
S -Analytical results are from modified screenina analysis.
J -Estimated value.Tlus represents an estimated concentration for Tentafively Identified Compounds(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
Report Format: Data Usability Report
�
e..,�_. IiA
Pana 1�nf 1 R
Serial No:12221513:23 -
Project Name: DRINANE RESIDENCE Lab Number: L1532813
Projecf Number: BEA13-10579 Report Date: 12/22/15
REFERENCES
_
30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-
WPCF. 18th Edition. 1992
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100,August 1993.
LIMITATION OF LIABILITIES
Alpha Analytical performs services with reasonable care and diGgence normal to the analytical testirig
laboratory industry. In the event of an error,the sole and exclusive responsibiliry of Alpha Analytical
shall be to re-perForm the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, cansequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
,��a
Page 14 of 16
• Serial No:12221513:23
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 5
Department:Quality Assurance Published Date: 1 2/9/201 5 3:49:20 PM
Title: Certificate/Approval Program Summarv Paqe 1 of 1
Certification Information
The following analytes are not included in our Primary NEL.AP Scope of Accreditation:
Westborough Facility
EPA 524.2: 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, m/p-xylene, o-xylene
EPA 624: 2-Butanone(MEK), 1,4-Dioxane,tert-Amylmethyl Ether, tert-Butyl Alcohol, m/p-xylene, o-xylene
EPA 625: Aniline, Benzoic Acid, Benzyl Alcohol, 4-Chloroaniline, 3-Methylphenol,4-Methylphenol.
EPA 1010A: NPW: Ignitability
EPA 6010C: NPW:Strontium; SCM: Strontium
EPA 8151A: NPW:2,4-DB, Dicamba, Dichloroprop, MCPA, MCPP; SCM: 2,4-DB, Dichloroprop, MCPA, MCPP
EPA 8260C: NPW: 1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene, Isopropanol; SCM: lodomethane(methyl
iodide), Methyl methacrylate(soil); 1,2,4,5-Tetramethylbenzene;4-Ethyltoluene.
EPA 8270D: NPW: Pentachloronitrobenzene, 1-Methylnaphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine; SCM:
Pentachloronitrobenzene, 1-Methylnaphthalene, Dimethylnaphthatene,1,4-Diphenylhydrazine.
EPA 9010: NPW: Amenable Cyanide Distillation,Total Cyanide Distillation
EPA 9038: NPW: Sulfate
EPA 9050A: NPW:Specific Conductance
EPA 9056: NPW: Chloride, Nitrate, Sulfate
EPA 9065: NPW: Phenols
EPA 9251: NPW: Chloride
SM3500: NPW: Ferrous Iron
SM4500: NPW: Amenable Cyanide, Dissolved Oxygen; SCM:Tbtat Phosphorus, TKN, NO2, NO3.
SM5310C: DW: Dissolved Organic Carbon
Mansfield Facility
EPA 8270D: NPW: Biphenyl;SCM: Biphenyl
EPA 2540D: TSS
EPATO-15: Halothane,2,4,4-Trimethyl-2-pentene,2,4,4-Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Te�ramethylbenzene,
Benzothiophene, 1-Methylnaphthalene.
The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility:
Drinking Water
EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury;
EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA.353.2: Nitrate-N, Nitrite-N;SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500.F-C,
SM4500CN-CE, EPA 180.1,SM2130B, SM4500C1-D,SM2320B, SM2540C,SM4500H-B
EPA 332: Perchlorate.
Microbiology:SM9215B; SM9223-P/A,SM9223B-Colilert-QT, Enterolert-QT.
Non-Potable Water
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn; �
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn;
EPA 245.1,SM4500H,B, EPA 120.1,SM2510B,SM2540C,SM2340B, SM2320B,SM4500CL-E, SM4500E-BC,
SM426C,SM4500NH3-BH, EPA 350.9:Ammonia-N, LACHAT'10-107-06-1-B:Ammonia-N, SM4500NO3-F,
EPA 353.2: Nitrate-N,SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, SM4500P-B,E,SM5220D, EPA 410.4,
SM5210B,SM5310C,SM4500CL-D, EPA 1664, SI11114 510AC, EPA 420.1,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Hafocarbons&Aroma#ics,
EPA 608: Chlordane, Toxaphene,Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD,DDE, DDT,
Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs
EPA 625: SVOC(Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil.
Microbiology: SM9223B-Colilert-QT; Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods, please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: OS-113
Paae 15 of 16
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• Serial No:06161621:23
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,A�l�l A�L�'Y.:�T f C A L �
ANALYTICAL REPORT
Lab Number: L1617853
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
ATTN: David Bennett
Phone: (508)896-1706
Project Name: DRINANE RESIDENCE
Project Number: BEA13-10579
Report Date: 06/16/16
The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its
enfirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH{2003);NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC{666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com
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• Serial No:06161621:23
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
Case Narrative
The samples were received in accordance with the Chain of Custodq and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e:VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality controi corcective
action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability forrnat of our Data
Merger tool where it can be reviewed along with any associated usability implications.SoiUsediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance criteria for CAM and RCP methods allow for some
quality control failures to occur and still be within method compliance. In these instances the specfic failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatbry Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will
be disposed after 3 business days from the date the project is completed.
Please contact Client Services at 800-&24-9220 with any questions.
I,the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
G��� Cristin Walker
Authorized Signature:
Title: Technical Director/Representative Date: 06/16/16
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Serial No:06161621:23 `
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Page 4 of 15
' Serial No:06161621:23
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
SAMPLE RESULTS
Lab ID: L1617853-01 Date Collected: 06/10/16 11:00
Client ID: EFF�uENT Date Received: 06/10/16
Sample Location: souTH va,RtwouTH,Mn Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifer Units RL MDL Factor Prepared Analyzed Method qnalyst
General Chemistry-Westborough Lab _ _
Solids,Total Suspended ND mg/I 5.0 NA 1 - 06/13/16 16:35 121,2540D SG
- --------------------------.........-------------------._....------..._..._...---------------------__-- -------...-----____---....
Nitrogen,Nitrite 0.081 mgA 0.050 – 1 - 06/10/16 22:08 44,353.2 MR
-�-----�---�------...._...---._..__�_—.—..__._�_---------------------...---------------.._�_.__...--------------------------...--------
Nitrogen,Nitrate 3.1 mg/1 0.10 – 1 - 06/10/16 22:08 44,353.2 MR
--------------__.___---____----------------------..:__.�—.._._..__..__.._..---------...__..__...--------_-----------------...-------------._...------�—
Nitrogen,Total Kjeldahl 2.05 mgA 0.300 – 1 06/13/16 20:00 06/15/16 22:20 121,4500N-C AT
-----.�_..---._.._.__._......_.....-----...-------------....-----.._._.�--------.._..__._......_..__..__....._.__...----...._.._._._..._....__------------__------._....—.....---....-----...__--------......_._.._.__.._
BOD,5 day ND mg/l 2.0 NA 1 06/11/16 04:15 06/15/16 23:10 121,52108 TA
'��
n..,,.., c ,.f�G
Serial No:06161621:23 '
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
Method Blank Analysis
Batch f�uality Control
Dilution Date Date Analytical
Parameter Result Qualifier Units RL IVIDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG902832-1
Nitrogen,Nitrate ND mgll 0.10 — 1 - 06/10/16 20:58 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG902833-1
Nitrogen,Nitrite ND mg/I 0.050 — 1 - 06/10/16 21:00 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG902977-1
BOD,5 day ND mgll 2.0 NA 1 06/11/16 04:15 06/15/16 23:10 121,5210B TA
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG903365-1
Solids,Total Suspended ND mg/I 5.0 NA 1 - 06/13/16 16:35 121,2540D SG
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG903494-1
Nitrogen,Total Kjeldahl ND mgll 0.300 — 1 O6/13/16 20:00 06/15/16 22:07 121,4500N-C AT
�.
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Page 6 of 15
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Serial No:06161621:23 `
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
Sample Receipt and Container Information
Were project specific reporting limits specified? YES '
Cooler lnformation Custody Seal
�ooler
A Absent
Container Information Temp
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1 61 7 853-0 1A Plastic 250m1 H2SO4 preserved A <2 3.3 Y Absent TKN-4500(28)
L1617853-01 B Plastic 950m1 unpreserved A 7 3.3 Y Absent NO2�53(2),BOD-5210(2),NO3-
353(2)
L1617853-01C Plastic 950m1 unpreserved A 7 3.3 Y Absent TSS-2540(7)
*Values in parentheses indicate holding time in days �,a►
:�,�.�
Page 10 of 15
' Serial No:06161621:23
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:Tlus value represents the level to which target analyte concentrations aze reported as estimated
values,when those target analyte concentrations are quantified below the reporting limit(RL).The EDL includes any
adjustrnents from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with veiified lmown amounts of
analytes or a material containing lmown and verified amounts of analytes.
LCSD -Laboratory Control Sample Dupiicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of
analytes or a materiat confaining known and verified amounts of analytes.
IvIDL -Method Detection Limit:This value represents the level to which target analyte concentrations aze reported as estimated
values,when those target analyte concentrations aze quantified below the reporting limit(RL).The MDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.
MS -Mairix Spike Sample:A sample prepued by adding a known mass of tazget analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
I�OI'trIIp U1llL
NDPA/DPA -N Nitrosodiphenylamine/Diphenylamine.
NI -Not Ignitable.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit: The value at wlrich an instrument can accurateiy measure an analyte at a specific concentration.The RL
inciudes any adjusiments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The resuits from matr�and/or matrix spike duplicates aze primarily designed to assess the
precision of analytical results in a given mah-ix and aze expressed as relative percent difference(RPD). Values which are less
than five times the reporting limit for any individual parameter aze evaluated by utilizing the absolute difference between the
values;although the RPD value will be provided in the repork
SRM -Standard Reference Material:A reference sample of a Imown or certified value that is of the same or similaz mahix as the
associated field samples.
STLP -Semi-dynamic Tank I.eaching Procedure per EPA Method 1315.
TIC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound
list(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations.
Footnotes
i -The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
Terms
Total:With respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors.If a Total'
result is requested,the results of its individual components will also be reported Tlus is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and ihe analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in The References section of the Addend»m
Data Qua/ifters
A -Spech�a identified as"Aldol Condensation ProducY'.
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated fieid samples that
have detectable concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox)
the concentration found in the blanlc For DOD-related projects,flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated field sampies that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectabie
concenh-ations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the
•Report Format: Data Usability Report
�,,
����
Serial No:06161621:23 '
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
Data Qualifiers
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
C -Co-elurion:The target analyte co-elutes with a known lab standard(i.e.smrogate,intemal standards,etc.)for co-exh�acted
analyses. _ _ __ _
D -Concentrarion of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations
of the analyte.
E -Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
G -The conceniration may be biased Irigh due to mahix interferences(i.e,co-elution)with non-target compound(s).The result should
be considered estimated.
H -The analysis of pFi was performed beyond the regulatory-required holding time of 15 minutes from the tixne of sample collection.
I -The lower value for the two columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for tlus analyte.
NJ -Presumptive evidence of compound.This represents an estimated concenh-ation for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral library search.
P -The RPD between the results for the two colmnas exceeds the method-specified criteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the saznple concentrations aze less
than Sx the RL.(Metals only.)
R -Analytical results are from sample re-analysis.
RE -Analytical results are from sample re-estraction.
S -Analytical results aze fiom modified screening analysis.
J -Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
Report Format: Data Usability Report
��
_Page 12 of 15
' Serial No:06161621:23
Project Name: DRINANE RESIDENCE Lab Number: L1617853
Project Number: BEA13-10579 Report Date: 06/16/16
REFERENCES
44 Methods for the Determination of Inorganic Substances in Environmental Sampies,
EPA/600/R-93/100, August 1993.
121 Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
LIMITATION OF LIABILITIES
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume,preservation,cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
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Serial No:06161621:23
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 6
Department: Quality Assurance Published Date: 2/3/2016 10:23:10 AM
Title: Certificate/Approval Proqram Summarv Paqe 1 of 1
Certification Information
The following analytes are not included in our Primary NELAP Seope of Accreditation:
Westborough Facility
EPA52A.2:1,2-Dibromo-3-chloropropane,1,2-Dibromoethane,m/p-xylene,o-xylene
EPA 624:2-Butanone(MEK), 1,4-Dioxane,tert-Amylmethyl Ether,tert-Butyl Alcohol,m/p-xylene,o-xylene
EPA 625: Miline,Benzoic Acid,Benzyi Aicohol,4-Chloroaniline,3-Methylphenol,4-Methylphenol.
EPA 1010A: NPW: ignitability
EPA 6010C: NPW:Strontium;SCM: Strontium
EPA8151A: NPW:2,4-DB,Dicamba,Dichloroprop,MCPA,MCPP;SCM: 2,4-DB,Dichloroprop,MCPA,MCPP
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyitoluene,Azobenzene,Isopropanol;SCM:lodomethane(methyl iodide),Methyl methacrylate
(soil);1,2,4,5-Tetramethylbenzene;4-Ethyltoluene.
EPA 8270D: NPW:Pentachloronitrobenzene,1-Methylnaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Pentachloronitrobenzene,1-
Methylnaphthalene,Dimethylnaphthalene,l,4-Diphenylhydrazine.
EPA9010: NPW: Amenable Cyanide Distillation,Total Cyanide Distillation
EPA 9038: NPW: Sulfate
EPA 9050A: NPW:Specific Conductance
EPA 9056:NPW:Chloride,Nitrate,Sulfate
EPA 9U65: NPW:Phenols
EPA 9251: NPW:Chloride
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved Organic Carbon
Mansfield Facility
EPA 8270D:NPW: Biphenyl;SCM: Biphenyi,Caprolactam
EPA 8270D-SIM Isotope Dilution: SCM: 1,4Dioxane
SM 2540D: TSS
SM2540G: SCM:Percent Solids
EPA1631E:SCM: Mercury
EPA 7474: SCM: Mercury
EPA808'IB:NPW and SCM:Mirex,Hexachlorobenzene.
EPA8082A: NPW: PCB:1,5,31,87,101,110,141,151,153, 180,183, 187.
EPA 8270�SIM: NPW and SCM: Alkylated PAHs.
EPATO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4-Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methyfthiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,Indan, Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene,n-
Butylbenzene,n-Propylbenzene,sec-Butylbenzene,tert-Butylbenzene.
Biological Tissue Matrix: 8270D-S1M;30508;3051A;74718;80818;8082A;6020A:Lead;8270D:bis(2-ethylhexyl)phthalate,Butyibenrylphthalate,
Diethyl phthalate,Dimethyl phthalate,Di-n-butyl phthalate,Di-n-ocryl phthalate,Fluoranthene,Pentachlorophenol.
The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility:
Drinking Wafer
EPA200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA200.7:Ba,Be,Ca,Cd,Cr,Cu,Na;EPA245.1:Mercury;
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1,
SM2130B,SM4500CI-D,SM23206,SM2540C,SM4500H-B
EPA 332:Perchlorate.
Microbiology:SM9215B;SM9223-P/A,SM92238-Colilert-QT,Enterolert-QT.
Non-Potable Water
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;
EPA200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn;
EPA 245.1,SM4500H,B,EPA 120.1,SM2510B,SM2540C,SM23406,SM2320B,SM4500CL-E,SM4500E-BC,SM426C,SM4500NH3-BH,EPA
350.1:Ammonia-N,LACHAT 10-107-06-1-B:Ammonia-N,SM4500NO3-F,
EPA 353.2:Nitrate-N,SM4500NH3-BC-NES,EPA 351.1,SM4500P-E,SM4500P-B,E,SM5220D,EPA 410.4,SM5270B,SM5310C,SM4500CL-D,
EPA 1664,SM14 510AC,EPA 420.1,SM4500-CN-CE,SM2540D,
EPA 6?A:Volatile Halocarbons&Aromatics,
EPA608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,deita-6HC,Dieldrin,DDD,DDE,DDT,Endosulfan I,Endosulfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC(Acid/Base/Neutral Extractables),EPA 600/4-81-045:PCB-Oil.
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: 08-113
Paqe 14 of 15
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