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Home My WebLink About2016 Sep 14 - Singulair Inspection and O&M Report from Bennett Environmental Associates, Inc. � �j�-v-�r�' ��'��,G�� 1�7��i �El�TNET� EIoTVIRONl�IE�TTAL ASSOCIATES, Il�C, LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,EliTGINEERS 1573 Main Street,P.O.Bog 1743 (508)896-1706 Brewster,MA 02631 fag(508)$96-5109 LETTER OF TRANSMITTAL TO: DATE: JOB NUMBER: Massachusetts Departrnent ofEnvironmental Protection 9/14/16 —� BEA16-10901 Attention:Title 5 Program 1 Winter Street-6th Floor Boston,MA 02108 REGARDING: Jason Residence 24 Hawk's Wing Road RECEIVED SHIPPING METHOD: South Yarmouth,MA 02664 aCT n 3 ?�16 RegularMail � PickUp � HEALTH DEPT. PrioriTy Mail ❑ Hand Deliver ❑ Eacpress Mail ❑ Other ❑ � Certified Mail � Green Card/RR 0 COPIES DATE DESCRIPTION 1 DEP Approved Inspection and O&M Form for Title 5 UA Treatment and Disposal Systems(September 2016) 1 Singulair Service Inspection Checklist(September 2016) 1 9/11/16 Alpha Analytical Laboratory Report For review and comment: � For approval: � As requested: � Fbr your use: 0 REMARKS: Please find enclosed the DEP Inspection and O&M Fonn,Singulair Service Inspection Checklist,and laboratory analytical results for operation and maintenance conducted during the reporting period for the above referenced properiy. If you have any questions or require additional information,please contact us at your earliest convenience. Thank you. cc:Yarmouth Board of Health Scott Jason,Property Owner Robin Cassidy-Norweco[via email] FROM: Samantha Farrenkopf WWTO#13265 If enclosures are not as noted,kindly notify us at once � Massachusetts Department of Environmental Protection Bureau of Resource Protection - Title 5 . DEP Approved Inspection and O&M Form for Title 5 1/A Treatment and Disposal Systems A. Installation Important:When Scott and Tamie Jason filling out forms Owner on the computer, use only the tab 24 Hawks Wing Road key to move your Facility Street Address cursor-c�o not South Yarmouth 02664 use the return Ci� Zip key. � Mailing address of owner, if different: � � Street Address/PO Box: 2aen City State Zip (508)776-4136 ext. Telephone Number B. Authorized Service Provider Bennett Environmental Associates, Inc. O&M Firm 1573 Main Street/PO Box 1743 Street Address Brewster MA 02631 City State Zip (508)896- 1706 ext. 129 Telephone Number Samantha Farrenkopf 13265 Certified Operator Name Cert�cation Number C. Facility/System Information Singulair 960DN-600 DEP ID Manufacturer ID Model Number . Unknown 05/26/2009 Installation Date Start of Operation Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial Seasonal Residence—used less than 6 mo./year: ❑ Yes � No D. Operating Information � 9/1/16 6/10/16 System evaluation visit Inspection Date Previous Inspection Date NA sludge, 5"scum (excessive scum) Pumping Recommended � Yes ❑ No Sludge Depth(to be checked yearly) t5aiom.doc•rev.04-11-13 Page 1 of 3 I I Massachusetts Department of Environmental Protection ' Bureau of Resource Protection - Title 5 DEP Approved Inspection and O&NI I�orm for Title 5 I/A Treatment and Disposal Systems _ _ E. Field Testing_ . _ _ _ ; _ _ __ _ _ -- __ _ _ _ _ _ _ _ _ __ __ _ ; _ _ _ _ _ Fieidlnspeciion: _. _ _ _ _ _ _ _ _ Color: ❑ gray ❑ brown ❑ clear �turbid � Other(specify): Cloudy Odor: ❑ musty � earthy ❑ moldy ❑ offensive ❑ turbid Effluent Solids: ❑ no � some ' pH 7.5 SU p� 1.0 mg/L Turbidity 38.3 NTU 6 to 9 2 or greater 40 or less Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected per Standard Methods and analyzed for BOD and TSS. F. Sampling Information Samples Taken: ❑ Influent � Effluent Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use nitrogen reducing systems: gpd Parameters sampled: ❑ pH � BOD ❑ CBOD ❑ TSS ❑ TN � Other{list below) Nitrate Nitrite TKN Other 1 Other 2 Ofher 3 G. Inspection and Maintenance Description of any maintenance performed since previous inspection &during this inspection: On June 10, 2016 a system evaluaiion visit was perFormed and repairs to the recycle pump and associate8 electrical, as well as pumping,was recommended. The homeowner directly completed repairs to the recycle pump and wiring. Conduct an operation and maintenance event on 9/1/16. Collect effluent samples for field testing and laboratory analysis. Notes and Comments: All mechanical components of the system are operating correctly. Effluent quality failed field testing parameters. Pumping of the primary section of the Singulair is recommended. � € E 4 t5aiom.doc•rev.04-11-13 Page 2 of 3 � i ' Massachusetts Department of Environmental Protection Bureau of Resource Protection -Title 5 DEP Approved Inspection and O&M Form for Title 5 I/A Treatment and Disposal Systems H. Certification I certify: I have inspected the sewage treatment and disposal system at the address above, have conducted the required Field Testing and/or sample collection in accordance with Standard Methods, have completed this report and the attached technology operation and maintenance checklist, and the information reported is true, accurate, and complete as of the time of the inspection. I am a Massachusetts ce ' d operator in accordance with 257 CMR 2.00. �I (E-(�[l� Operator Signature Date System owner must submit this report, technology O&M checklist, and any required sampling results to the local board of health as follows for each inspection performed: Remedial Use—by January 31�of each year for the previous calendar year Piloting Use-within 45 days of inspection date Provisional Use—by March 31ih of each year for the previous 12 months General Use—by September 30th of each year for the previous 12 months Send to: Department of Environmental Protection Attention: Title 5 Program One Winter Street, 5�' Floor Boston, MA 02108 t5aiom.doc•rev.04-11-13 Page 3 of 3 ' � i ��`a'�`� �� :�� , �� .��,I�� t"fi'`'�"'t' '�-��:�;�..� t --�---�+ �`*°''°,�:� �{et,�.,w,�.�..`-.s�Z Address: ��,�r-.�.��' �3<°�� :� Ow�er: �'�`�Q"`"°°° fl�r�c.�-�*...r�� 1��"" OperatQ ��C:`--v> " ��%� ,`^.�'�^�-- ,Date: �� "� `� �� 'This checicl.ist swnmarizeY'the seivice�oc�dures to�performed�tuing a routine�ingulair'�SO NR inspeckion.Refer to the �ino�,t��M��aal for a det�:�led explanation of each service pr�cedure and an O&1VI troubleshootino guide. (;Q,NTROL CE�1TElt SERVICE NOTESJC0�114E1��TS '�..Check operati�of control center l�'"��^ �'� '��''`''rt � �'i"'°'r�"' _ �`�`''"�'` C`�Adjust time cic�k when r�uireo �'�`,"�- ' �.�"."�-°'�, �=�'`"r`h..�``"°.' — �~1�eck operation of recirc�zla�on control panel NR EFFLUENT REC��CULATION SYSTE� �� .Che�k ogeration of recirc�ation p�p �'''��- �°�`�'�`>�'�' �`''�" `��Nnsp�ct rec�rculati.on wsli�i fittings �,,�..re,.- �iy.,,,,- �5 ,� ,�;,,��L�,.�.�i__.w x �,Test Operation �.�'o '�:.```�`"'�� '�•� �,�et reeircutation rate rate @ min/hr�'��,�� 1r,{' C'��'�T AERAT{�R S��ViCB �Check�erator op�ratic� j��,��c•.� .� -�,•3�cv�� - �'CI C}aeck aerator power ccrosa.�o� - <m ��Check aerat�r air delivery �„�.'�.� .... ;�`�.- �.�;�� t��,, ��»�. '� Clean s�vnless ste��aspirator sh�ft � ��.�� '�Cie�aspirator ti� 3~-�-�''u-�'�.. � � �.i:�� P-�� Clean fresh aa vem in concrete cover _ �Ir�.spect aerativn c�nber cox�.t� i'*�;°" �;..�� CLARI�TCATT�N CHAMBER S�RVI�E �2emoue the Bio-Kinetic system �� - �-:�`��'�`�"�``.t' ��,:'��j''� �Scrape t� clarific�ion cha��r t��.�...c�� ...�. �'�+��.4� �`��"'�, ❑Insp�t the�io-St�ic sl��.ge retum �.�r�`a�c;�..i�.-, �J�>�., . �In.spect outlet couplirr� �Insta.11 a cl�an Bio-Kinetic system -.�--� I�Fi13 B�:��yst�l feed�(if ia�tstalled} ��F�ll.Bio-Neutralizer feed tube�if installed} GENERAL SERTVI�� -�"� .t,� -. � O�.sc�t effluent p�sp cha�n�er � �:�^'' .��',��,`: .S �-.t.��.,�;y c..��,f''��•� Ir,s��ct efflu�nt c�aa.lity °i��`��' � � �/' �-�. , �outlet line ��'"' � . ,��, �-� �`In.�±ect ground�aa�s< ::�lief pa��f i�-�stalled) � �„ : `' �I��ct e£�uent�sposal.syst�� "��'"� �er*�-�;�= �,G�mpi��owne��ervice€ecoi� c� - 1;" \: t��'� 9 Co�nplc,�heat#h dep�r�na�notific�tion � ,�.y� � 3 - �..� ti-e, � � n. ---.�-�,,-�c.�.� �Con�alete distributor serviu�record "1 ° C 1^�-`�5 `� � �Mai1 health depa�ern ncatification �,,,�� \�i�' �,� ' S S ;:S,"^��r�-,.- e�� -�v"i� ��r�--� J+S - Siegm Enviroa�mental Serviees,Ina t'�„,C-,+('�'� � �� FLUID THINI�IVG.CLEAi2 SOLtJ�IONS. �.'�f'��'`� � �y 5'�� ,,� �LVW.SiCL�Q1Urid�TOi117.COTii '�. � 5 �� • :��= Serial_No:09111619:53 � �� 5,4�4� � �� ,� : .9'f,V A L.Y.��,T/ C A L ANALYTICAL REPORT Lab Number: L1627749 Client: . Bennett Environmental Associates 1573 Main Street Brewster, MA 02631 ' ATTN: David Bennett Phone: (508)896-1706 Project Name: JASON RESIDENCE ' Project Number: BE,416-10901 Report Date: 09/11/16 The original project report/data package is held by Alpha Analyticai.This report/data package is paginated and shouid be reproduced only in its entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Cert�cations&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086), PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240). Eight Waikup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com �; ��a �. _ �.� Page 1 of 15 � E :a=; �s G1 �+. � � � � ,. � (O ~ � � N _ ti N � � � tl � � � � � J O � O _ _ " O O Z i ' L � � � � � � � � � � � d r Z L O O �� `r�° s Q. � J � � � � o a � UO o Q � � � _ I-- ( � , O � � Q c } a� o = a'� t- � c�o o O N J Cq � x w � � w U Z W � r W � � � � O � � z � w cn a W C J � m � � U W L d d � � � Z Z Q � � � T V V � � O �O O N Q t� N a` a` Q� � °' � I Q tn � `° a f Serial No:09111619:53 Project Name: JASON RESIDENCE Lab Number: L1627749 Project Number: BEA16-10901 Report Date: 09/11/16 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all NELAP accredited parameters unless otherwise noted in the foliowing narrative.The data presented in this report is organized by parameter (i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds (TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List, even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality controi corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE", respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.All specfic QC information is also incorporated in the Data Usability format of our Data Merger tooi where it can be reviewed along with any associated usability implications.SoiUsediments,solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualfiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance criteria for CAM and RCP methods allow for some ' quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. ' Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numericai Standards requested on the Chain of Custody. ' HOLD POLICY � For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless : you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will be disposed after 3 business days from the date the project is compieted. ' Please contact Client Services at 800�24-9220 with any questions. I,the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report,such information is accurate and complete. This certificate of analysis is.not complete unless this page accompanies any and all pages of this report. , ��(�� Kelly Stenstrom Authorized Signature: � Title: Technical Director/Representative Date: 09/11/16 ti Page 3 of 15 �j\-°�� , � Serial No:09111619:53 � __ _ _ __. _ __ _ __ _ . . _ _ _____ , _ _ INORGANICS � & MISCELLANEOU� � :�� w„�.. - , Page 4 of 15 � I , Serial No:09111619:53 Project Name: JASON RESIDENCE Lab Number: L1627749 Project Number: BEA16-10901 Report Date: 09/11/16 SAMPLE RESULTS ' Lab ID: L1627749-01 Date Collected: 09/01/16 11:45 Client ID: EFFLUENT Date Received: 09/02/16 Sa111pIB LOCatlOfl: SOUTH YARMOUTH,nna Field Prep: Not Specified Matrix: Water Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General Chemistry-Westborough Lab Nitrogen,Nitrite ND mg/I 0.050 -- 1 - 09/02/1623:54 44,353.2 MR ---- ------------ _---------- - ----- _----- ----- ----- Nitrogen,Nitrate ND mg/I 0.10 -- 1 - 09/02/1623:54 44,353.2 MR , ..._------------------------------ - --- ---------._- ------.._.._-- ----._..........-.___ .-- --- --------------....-- ----....--------------..__...------ ..._--— Nitrogen,Total Kjeidahl 78.0 mg/I 3.00 - 10 09/07/16 09:07 09/09/16 00:15 121,4500N-C AT BOD,5 day 58. mg/I 12 NA 6 09/03/16 00:30 09/07/16 23:15 121,5210B JC �.-. . �ii`� Page 5 of 15 I Serial No:09111619:53 Project Name: JASON RESIDENCE Lab Number: L1627749 Project Number: BEA16-10901 Report Date: 09/11/16 Method Blank Analysis Batch Quality Control ( ; � Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Me4hod Analyst General Chemistry,Westborough Lab forsample(s): 01 Batch: WG928643-1 Nitrogen,Nitrate ND mg/I 0.10 — 1 - 09/02/16 22:39 44,3532 MR General Chemistry-Westborough Lab for sample{s): 01 Batch: WG928645-1 Nitrogen,Nitrite ND mg/I 0.050 — 1 - 09/02/16 22:42 44,3532 MR General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928708-1 BOD,5 day ND mgA 2.0 NA 1 09/03/16 00:30 09/07/76 23:15 121,5210B JC General Chemistry-Westborough Lab for sample(s): 01 Batch: WG929421-1 ' Nitrogen,Total Kjeldahl ND mg/I 0.300 — 1 09/07/16 09:07 D9/OS/16 23:49 121,4500N-C AT —------ _-------------- -- - --- ---- ----- ------- - ----- —___.—._—_—_ , __�L�J�?I"A`` Page 6 of 15 M I � � � CO +�< � � N � �, � = � h � � ��.,��z�� O N T -� � � ��-�^'�t O � ` N N z � O� n . : - . . . � . 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N i M N �.".�i . � � � �J . � . � .� � ��`� � T f� � N N N � � I � C�O � N Q Q j fl Q 4 � � � � � � ' � � Z �' � � (n (� : U� f� _� ; �a a � , � , � � , � , .� � � i,; � p Q � p p � R �' �' ! "' � c � c c � ;;+ ..N �M .N N � N � :. N .. s � � � � � � � Z p t� V � V � I V � U ^ .Q Q• � J ' � d � t � ' � r ,, � O O � O O , R � � � � 7 � � � � � N N : N N C4 CO ; Cfl t0 d J J J J � � i, N V � � N � � N � , � � �� ! � � N � N l0 ; N N k � � � � � z O .� c ,a C'! C3 � C� ' t� � = V � � � � � � � � �y c� � oo � � d' O N Q � � � � ' � � : y � � � � ', �' ;' � � V � > L � � � > � � m �+ p p ,f p p � GI - o — �n — — 9 � � � � L rn t rn � O 6 N � f�Q N V � m m � m o � � ; �� •, � .. � = 0 d' � d' ,� 0 � � � ap � ��.. �LL fA ...fA � .(A. �N � . � N I � N a a a• Q � � � � m � d � � N v � �' o � �o �� -a -o • � �� a� m m a� W Q m m m io ', Zu�i oi oi r� � � � ;Q ¢ p Q O Q c� Q � I � Q � � � Z @ Z � ri � ,- W � Z N J J ' J J � � � � � L L .� z (� � �� i � �� . O � 7 7 7 7 � Q O O , O O � W � � ` � � m � � � � � � � ; � , � G� ' , i ' � c�u E � in i � n i� °' � Y Z Z "E y' i 'E : �E -m u�i �` m -- ! a� m � � � z � z ; � � '. .c t°- � G1 C� � U � C� c I U � U c v- �� d N rn cL6 °�rn ; c�6 � � rn � a a � N o a� o ; a� � '` N o ao ea � Z � Z � � m : � z � c� � a C7 C� U U � M � � . ti � � ti � N � y �o � � � � � � � J � J N fO N N M � N y�'`"''sa t p .Q 'Q. �� Q: � � R �. � . �� z�. �� . Z� p: � c�� J � N �- �- �- LL: �-. d � � Q � � � W Q Z i � � � � 0 O � �. c c' c c J � a� a� .� � � `U U U U a � Z � Z � N r-. � o 0 0 0 a� a� o� o0 c�o m � � . N N N N CO C4 C4 C4 ,�; J - J - J - J - •= o� o� o� ` a� � � � � � � � � � � Q Q. Q. Q •�1� N N N f�6 � � � � � � � — U U U U Qcj � C'1 C� �'1 C'1 d.�+ ;+a � M M M M cV � � wd � Z � Z O � N � V � � � � � � � •� t� •7 {� � � �. 0m � � � >� � � � � � � �6 — J t .c .c .� � .� .� .;? m m m m p�p � C7 C7 � C3� : ln 0 � � v � � Z � Z � � � � .� O O O O :�:+ t6 �j . v �N ..� �. Z � . .� � ..� .. Q Q Q Q � . �� .�.�. � . �� N .� :...N� � . � N N N uj t�6 (�6 f-�Q 6 V � .0 Q �� Z N N � N p Q Q 4 Q _ � v� o � � � .fl rn � � J J J J Z cp t ..c t t O � � � � � � Q O O O O W � m .n � � :� � N N � . a`� � � � � � � ,Q � � � , � � � L � L L . . .L N .. Z Z (n N U] � tn fn Y .� � , .� � -� ,� m O G� Q1 L _C z ' t z t (0 ,� � � '-` '� Gf O c U � U � U � O O O .,.+ , a` a` � � o � a � o � o � � a� -- a� -- a� o a� -- a, i, � Z '. �C Z . C m C Z � (� a c� c� c� c� °' r v Serial No:09111619:53 — , Project Name: JASON RESIDENCE La6 Number: L1627749 Project Number: BEA16-10901 Report Date: 09/11/16 Sample Receipt and Container Information Were project specific reporting limits specified? YES _ _ _ _. _ f ; __ _ _ ; Cooler Information Custody�eal - . Cooler A Absent Container Information Temp Container ID Container Type Cooler pH deg C pres Seal Analysis(*) L1627749-01 A Plastic 250m1 H2SO4 preserved A <2 2.3 Y Abse�t TKN-4500(28) L1627749-01 B Plastic 950mi unpreserved A 7 2.3 Y Absent NO2-353(2),BOD-5210(2),NO3- 353(2) I I *Values in parentheses indicate holding time in days ;_'�[��i:at;,� .;k„�.. Page 10 of 15 Serial No:09111619:53 Project Name: ,1ASON RESIDENCE Lab Number: L1627749 Project Number: BEA16-10901 Report Date: 09/11/16 GLOSSARY Acronyms EDL -Estimated Detection Limit:This value represents the level to wluch tazget analyte concenh�ations are reported as estimated values,when those target analyte concentrations are quantified below the reporting lixnit(RL).The EDL includes any adjustinents from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextracfion(SPME). EPA -Environmental Protection Agency. LCS -Laboratory Control Sample:A sample matrix,free froin the analytes of interest,spiked widi verified known amounts of analytes or a material containiug lmown and verified amounts of analytes. LCSD -Laboratory Control Sample Duplicate:Refer to LCS. LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing]mown and verified amounts of analytes. MDL -Method Detecrion L'unit:Tlus value represents the level to which target analyte concentrations are reported as esUmated ' values,when those target analyte concentrations are quantified below the reporting limit(RL).The 7vIDL includes any adjustments fiom dilufions,concentrations or moisture content,where applicable. MS -Matrix Spike Sample:A sample prepazed by adding a known mass of target analyte to a specified amount of matrix sample far which an independent estimate of target analyte concentration is available. MSD -Matrix Spike Sample Duplicate:Refer to MS. NA •Not Applicable. ' NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculafion are non-detect at the parameter's reporting unit NDPA/DPA -N Nitrosodiphenylamine/Diphenylamine. Nf -Not I�itable. NP -Non-Plasdc:Term is utilized for the analysis-of Atterberg Limits in soiL RL -Reporting Limit: The value at which an instrument can accurately measw�e an analyte at a specific concentration.The RL includes any adjustments from dilutions,concentrations ar moisture content,where applicable. RPD -Relative Percent Difference: The results from matrix and/or mairix spike duplicates aze primarily designed to assess the precision of analytical results in a given matrix and aze expressed as relative percent difference(RPD). Values which are less than five times the reporting limit for any individual parameter aze evaluated by utilizing the absolute difference between the values;although the RPD value will be provided in the i�eport. SRM -Standazd Reference Material:A reference sample of a lmown or certified value that is of the sazne or similar tnatrix as the : associated field samples. ', STZP -Semi-dynamic Tank Leaching Procedure pet EPA Method 1315. TiC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound list(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations. Foofnotes 1 .The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. Terms Total:With respect to Organic analyses,a Total'result is defined as the summation of results for individual isomers or Aroclors.If a'TotaP result is requested,flie results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081 and 8082. Analytical Method:Both the document from wluch the method originates and the analytical reference method.(Example:EPA 8260B is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qnalifiers A -Spectra identified as"Aldol Condensation Product". B -The analyte was detected above the reporting limit in the associated method blaok.Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(lOx)the concentration found in the blank.For MCP-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox) the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(lOx)the concentration found in tl�e blank AND the analyte was detected above one-half the reporting limit(or above fl�e reportina limit for common lab contawinants)in the associated method blank.For NJ- Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit For N7-related projects(excluding An-),flag only applies to associated field samples that have detectable concentrafions of the anaiyte,wluch was detected above the reporting limit in the associated method blank or above 5ve tiunes the Report Format: Data Usability Report ' L�L'�F;A Page 11 of 15 i , � Serial No:09111619:53 ' — , � Project.Name: JASON RESIDENCE Lab Number: L1627749 Project IVumber: BEA16-10901 Report Date: 09/11/16 Data Qualifiers reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone). i C -Co-elution:The target analyte co-elutes with a known lab standard(i.e.sm-rogate,inteinal standards,etc.)for co-extracted � analyses. _ _ __ — : _ . D -Concentration of analyte was quanfified fi•om diluted analysis.Flag only applies to field samples fliat have detectable concentrations � of the analyte. _ E -Concentration of analyte exceeds the range of the calibrarion curve and/or lineaz range of the instrument G -The concenhation may be biased high due to matrix interFerences(i.e,co-elution)with non-target compound(s).The result should be considered estimated. H -The analysis of pH was performed beyond the regulatory-required holding t'vne of 15 minutes from the time of saznple collection. I -The lower value for the two columns]�as been reported due to obvious interference. ', M -Reporting L'unit(RL)exceeds the MCP CAM Reporting Limit for flus analyte. , NJ -Presuxnptive evidence of compound.This represents an estimated concentrafion for Tentstively Identified Compounds(TICs),where ' the identification is based on a mass spectral library seazch. P -The RPD beriveen the results for the two columns exceeds the method-specified criteria. Q -The quality control sample exceeds the associated acceptance criteria For DOD-related projects,LCS and/or Continuing Calibration ' Standard exceedences ue also qualified on all associaYed sample results. Note:This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrafions aze less ' than Sx the RL.(Metals only.) ; R -Anatytical results are from sample re-analysis. RE -Analytical results are from sample re�xtraction. S -Analytical results aze&om modified screening analysis. J -Estimated value.This represenTs an estimated concentration for Tentatively Identified Compounds(TICs). ND -Not detected at the reporting lunit(RL)for the sample. ! i � i Report Format. Data Usability Report "-�i„1 Page 12 of 15 i M Serial No:09111619:53 Project Name: ,1ASON RESIDENCE Lab Number: L1627749 Project Number: BEA16-10901 Report Date: 09/11/16 REFERENCES 44 Methods for the Determination of Inorganic Substances in Environmental Samples, EPA/600/R-93/100,August 1993. 121 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WEF. Standard Methods Online. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at iYs own expense. In no event shaU Alpha Analytical be held liable . for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha AnalyticaL We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling, containers, sampling procedures, holding time and splitting of samples in the field. .r 1 �� Page 13 of 15 i � Serial No:09111619:53 — . Alpha Analytical, Inc. ID No.:17873 '� Facility: Company-wide Revision 7 Department:Quality Assurance Published Date: 8/5/2016 11:25:56 AM Title• Certificate/ aproval Proqram Summarv Paqe 1 of 1 Certification Information f � � The following analytes are not included in our Primary NELAP Scope of Accreditation: _ _ ._ _ Westborough Facility _ __ EPA 624:m/p-xylene,o-xylene EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene;SCM:lodomethane(methyl iodide),Methyl methacrylate,1,2,4,5- Tetramethylbenzene;4-Ethyltoluene. EPA8270D: NPW:Dimethylnaphthalene,l,4-Diphenylhydrazine;SCM:Dimethylnaphthalene,1,4Diphenylhydrazine. EPA300: DW:Bromide EPA 6860: NPW and SCM:Perchlorate EPA 9010: NPW and SCM: Amenable Cyanide Distillation EPA 9012B: NPW:Total Cyanide EPA 9050A: NPW:Specific Conductance SM3500: NPW:Ferrous Iron SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3. , SM5370C:DW:Dissolved Organic Carbon ' Mansfield Facility ; SM 2540D: TSS ' EPA 3005A NPW EPA 8082A:NPW: PCB:1,5,31,87,101,110,141,151,153,180,183,187. EPATO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4Trimethyl-1-pentene,Thiophene,2-Methylthiophene, 3-Methy�thiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene. B9ological Tissue Matrix: EPA 30306 The following analytes are included in our Massachusetts DEP Scope of Accreditation Westborough Facility: Drinking Water EPA 300.0:Nitrate-N,Fluoride,Suffate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1, SM2130B,SM4500CI-D,SM23206,SM2540C,SM4500H-B ' EPA 332:Perohlorate;EPA 524.2: THMs and VOCs;EPA 504.1:EDB,DBCP. ' Microbiology:SM9215B;SM9223-P/A,SM92238-Colilert-QT,SM9222D. � Non-Potable Water I SM4500H,B,EPA 120.1,SM25106,SM2540C,SM2320B,SM4500CL-E,SM4500E-BC,SM4500NH3-BH,EPA 350.1:Ammonia-N,LACHAT 10-107- 06-1-B:Ammonia-N,SM4500NO3-F,EPA 353.2:Nitrate-N,EPA 351.1,SM4500P-E,SM4500P-B,E,SM4500SO4-E,SM5220D,EPA 410.4, SM5210B,SM5310C,SM4500CL-D,EPA 1664,EPA 420.1,SM4500-CN-CE,SM2540D. EPA 624:�folatile Halocarbons&Aromatics, I EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan 1,Endosulfan II, � Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epo�ade,PCBs EPA 625:SVOC(Acid/Base/Neutral Extractables),EPA 600/4-81-045:PCB-Oil. Microbiology.SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF. Mansfield Facility: Drinkfng Water EPA 200.7:Ba,Be,Cd, Cr,Cu,Ni,Na,Ca.EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TL.EPA 245.1 Hg. Non-Pota6/e Water EPA200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,TL,Ti,V,Zn. EPA200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TL,Zn. EPA 245.7 Hg. SM23406 For a complete listing of analytes and methods,please contact your Alpha Project Manager. 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