HomeMy WebLinkAbout2016 Sep 14 - Singulair Inspection and O&M Report from Bennett Environmental Associates, Inc. �
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: �ENNE�'I' EloT�IROleT1V�ENTAL �SSOCIATES, INC.
LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS
1573 Main Street,P.O.Bog 1743 {508)896-1706 �'
Brewster,MA 02631 , fax(508)896-5109 ''
LETTER OF TRANSMITTAL
TO: DATE: JOB NUMBER: i
Massachusetts Department of Environmental Protection 9/14/16 BEA15-10846
Attention:Title 5 Program ;
1 Winter Slxeet-6th Floor �
Boston,MA 02108 REGARDING: '
Vogler Residence
RECEIVED
38 Hawk's Wing Road i
SHIPPING METHOD: South Yaimouth,MA 02664 (�LT �3 ?��6 '
RegularMail � PickUp � HEALTH DEPT.
Priority Mail ❑ Hand Deliver ❑ ,;
Express Mail ❑ Other ❑
Certified Mail 0 Green Card/RR �
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COPIES DATE DESCRIPTION �
1 DEP Approved Inspection and O&M Form far Title 5 UA Treatment and Disposal Systems(Maz•ch, j
June and September 2016) !
1 Singulair Service Inspection Checklist(March,7une and September 2016)
1 3/18/16 Alpha Analytical Laboratory Report �
1 6/16/16 Alpha Analytical Laboratory Report
1 9/11/16 Alpha Analytical Laboratory Report �
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For review and comment: � Far approval: � As requested: � For your use: 0 ;
REMARKS: F
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Please find enclosed the DEP Inspection and O&M Forms,Singulair Service Inspection Checkiists,and laboratory analytical results for �
operation and maintenance conducted during the reporting period for the above referenced property. If you have any questions or require �
additional information,please contact us at your earliest convenience. Thank you. �
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cc:Yannouth Board of Health '
Paula Vogler,Properiy Owner '
Robin Cassidy-Norweco[via email] i
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FROM: Samantha Farrenkopf WWTO#13265 l
If enclosures are not as noted,kindly norify us at once ;
Massachusetts Department of Environmental Protection
, Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 1/A
�Treatrnent and Disposal Systems
A. I nstallation
Important:When Paula Vogler
filling out forms Owner
on the computer, '
use only the tab 39 Hawks Wing Road
key to move your Facility Street Address �
cursor-do not South Yarmouth, MA 02664 �
use the return '
key. City Zip
��1 Mailing address of owner, if different: '
YI�--�I
� Street Address/PO Box:
rzam
City State Zip
(774)254-2212 ext.
Telephone Number
6. Authorized Service Provider i
� �
Bennett Environmental Associates, lnc. �
O&M Firm f
1573 Main Street/PO Box 1743
Street Address I
Brewster MA 02631 �
. City State Zip �
{508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265 �
Certified Operator Name Certification Number I
C. Facili /S stem Information i
tY Y ;
Singular 960ND j
DEP ID Manufacturer ID Model Number j
Unknown 4/14/OS '
Installation Date Start of Operation I
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial I
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No �
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D. Operating Information �
3/10/16 NA
Inspection Date Previous Inspection Date
0"sludge, 0"scum Pumping Recommended ❑ Yes � No
Sludge Depth(to be checked yearly) �
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t5aiom.doc•rev.0411-13 Page 1 of 3
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Massachusetts Department of Environmental Protection I
Bureau of Resource Protection - Titie 5 ,
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems '
E. Field Testing
Field Inspection:
Color: ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid I
Effluent Solids: � no ❑ some I�il
pH 7.0 SU p� 5.0 mg/L Turbidity 14.3 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information �.
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
9Pd
� Parameters sampled: ❑ pH � BOD � CBOD � TSS � TN� Other(list below)
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Nitrate Nitrite TKN
j Other 1 Other 2 Other 3
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� G. Inspection and Maintenance
Description of any maintenance pertormed since previous inspection &during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis.
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' Notes and Comments:
; All mechanical components of the system are operating correctly. Effluent quality passed field testing
; parameters. Electrician need to evaluate electrical power source. Recycle pump needs electrical
junction box installed outside of riser. Recommend jetting of the pressure distribution lines.
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Massachusetts Department of Environmental Protection ,
: Bureau of Resource Protection - Title 5 '
DEP Approved Inspection and O&M �orm for Title 5 IlA '
�
Treatment and Disposal Systems ;
H. Certification
1 certify: I have inspected the sewage treatment and disposal system at the address above, have '�,
conducted the required Field Testing and/or sample collection in accordance with Standard Methods, '
have completed this report and the attached technology operation and maintenance checklist, and '
the information reported is true, accurate, and complete as of the time of the inspection. I am a I
Massachusetts ce " 'ed operator in accordance with 257 CMR 2.00. '
�.�j�-�C�t�
Operator ignature Date
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection performed:
Remedial Use—by January 31St of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31�of each year for the previous 12 months
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General Use—by September 30�of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor '
Boston, MA 02108
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t5aiom.doc•rev.04-11-13 Page 3 of 3
Massachusetts Department of Environmental Protection
i Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
A. Installation
Important:When Paula Vogler
filling out forms Owner
on the computer,
use oniy the tab 39 Hawks Wing Road
key to move your Facility Street Address
cursor-do not South Yarmouth, MA 02664
use the return
key. City Zip
� Mailing address of owner, if different:
�
� Street Address/PO Box:
� City State Zip
(774)254-2212 ext.
Telephone Number
B. Authorized Service Provider
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Zip
(508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf ' 13265
Certified Operator Name Cert�cation Number
C. Facility/System Information
Singular 960ND
DEP ID Manufacturer ID Model Number
Unknown 4/14/08
Installation Date Start of Operation
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial
Seasonal Residence—used less than 6 moJyear: ❑ Yes � No
D. Operating Information '
6/10/16 3/10/16
Inspection Date Previous Inspection Date
Sludge Depth(to be checked yearly) Pumping Recommended ❑ Yes � No
t5aiom.doc•rev.04-11-13 Page 1 of 3
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Massachusetts Department of Environmental Protection �
Bureau of Resource Protection - Titie 5 i
�EP Approved Inspection and O&iVl Form for �itle 5 I/A
Treatment and Disposal Systems
E. Field Testing
_ _
Field lnspection:
Color: ❑ gray ❑ brown � clear ❑ turbid . �
❑ Other(specify): �g
k
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid �
;
Effluent Solids: � no ❑ some �
pH 6 SU D0 2.0 mg/L Turbidity 4.62 NTU j
6 to 9 2 or greater 40 or less �
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected %
per Standard Methods and analyzed for BOD and TSS. �I
F. Sampling Information
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
gpd
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS ❑TN � Other(list below)
Nitrate Nitrite TKN
Other 1 Other 2 Other 3
G. Inspection and Maintenance
Description of any maintenance performed since previous inspection &during this inspection:
Complete jetting of pressure dosing lateral lines on 4/22/16. Conduct an operation and maintenance
event on 6/10/16. Collect effluent samples for field testing and laboratory analysis.
IVotes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters. Electrician need to evaluate electrical power source. Recycle pump needs electrical
junction box installed outside of riser
t5aiom.doc•rev.0411-13 Page 2 of 3
Massachusetts Department of Environmental Protection
` Bureau of Resource Protection -Title 5
DEP Approved Inspection and �&M Form for Title 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts certified operator in accordance with 257 CMR 2.00.
= �� +���� -
Operator igna ure Date -�
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection perFormed:
Remedial Use—by January 31�of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31'"of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108
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t5aiom.doc•rev.04-11-13 Page 3 of 3 I
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Mas�achuse�ts Department of Environmental Protection
� Bureau of Resource Protection -Title 5
DEP Appr�ved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
A. I nstallation
Important:When Paula Vogler
filling out forms Owner
on the computer,
use only the tab 39 Hawks Wing Road
key to move your Facility Street Address
cursor-do not South Yarmouth, MA 02664
use the return
key. C�� Zip
� Mailing address of owner, if different:
,�
Street Address/PO Box:
tetren
City State Zip
(774)254-2212 ext.
Telephone Number
B. Authorized Service Provider
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Zip
(508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265
Certified Operator Name Certification Number
C. Facility/System Information
Singular 960ND
DEP ID Manufacturer ID Model Number
Unknown 4/14/08
Installation Date Start of Operation '
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial '
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No
D. Operating Information ;
9/1/16 6/10/16 �
Inspection Date Previous Inspection Date �
f
Sludge Depth(to be checked yearly) Pumping Recommended ❑ Yes � NO j
t5aiom.doc•rev.04-11-13 Page 1 of 3 '
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Massachusetts Department of Environmentai Protection ��
Bureau of Resource Protection -Title 5 `
DEP Approved inspection and O&iVl Form for �'itle 5 UA
Treatment and Disposal Systems �
;
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e
k
E. Field Testing
_ i
Field Inspecfion:
Co1or: ❑ gray ❑ brown � clear ❑turbid
❑ Other s eci �
( p fY)�
i
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid �
Effluent Solids: � no ❑ some �
pH 7.0 SU p� 3.0 mg/L Turbidity 1.46 NTU �
6 to 9 2 or greater 40 or less i
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected �
per Standard Methods and analyzed for BOD and TSS. !
�
F. Sampling Information '
Samples Taken: ❑ Influent � Effluent �
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
i
nitrogen reducing systems: '
;
gpd
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS �TN � Other(list below) '
�
N itrate N itrite TKN l
Other 1 Other 2 Other 3 �
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G. Inspection and Maintenance
Description of any maintenance performed since previous inspection&during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters Electrician need to evaluate electrical power source for the recirculation pump.
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t5aiom.doc•rev.04-11-13
Massachusetts Department of Environmental Protection
� Bureau of Resource Protection - Title 5
DEP Approved Inspection and O&M Form for Title 5 IIA
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have com�leted this report and the attached technology operation and maintenance checklist, and
' the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts ce 'fied operator in accordance with 257 CMR 2.00.
� ����.�1�
Opera or ignature Date
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection performed:
Remedial Use—by January 31�of each year for the preyious calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31'h of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108
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Page 3 of 3 ;
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��T��,�I�� ��� I��I.t�.�'�''E'�.AL'I'EI�'�'���iTI��'� SY�'I'�M
S�RVICE �.N�P '�'I�+�N CHE�I�I_.I�� ��r�,��, tf.''s�u�
Address: 3���.���� tJi.1��in�, � Owner: s.v U�G�' ��i�
1
4perator. �ra� �nt�.�� ,�?,�,� �LP�v�� Date: _ �,r�.o��cp
��
This checl�list summarizes the service procec�ures to b�performed during aroutirle Singulair 960 NR inspectian.�efer to th�
Singulair Manual for a detailed explanation of each service procedure and an O&M troubleshoo#i�g guide.
C�NTROL CENTLR SERVICE NUT�-7,n;�C0�11�.�ENTS
�Check operat�an of conlral center ,/ r1� �
❑�_�djust time clack w3ien req��ired J�.f� . /�v •k�a.�-`��J/
�Check operation of recircutation conirol panet' �1, � �a.s y
�s.,��, ,�o.K�. t�.5 4,r.... �1�rr.Y
N Ek'FLUENT RECIRCULA"�'��N S ��TEM 4 ,
eck oper�sion of recircula�zon ptu��p b � tz��� C� � -�
#i
nspect recirculation welt&�ittin s �c�,� � �• ' ti c�. c�2c,,�.
i��est Operati.on �- �.��,r�•�,�,� +3Sv�-- �h In 2 0
CI Set recirculation ra.te rate Q min/hr 3+��,,,� �3 � T,
�'"� w�.,�,.U� `
���RATOR SERVICE
�Check aerator operation '?r��, ��n C-zr��Lz... '
❑Check aerat.�ir power consumptic� :
l�'t,`heck aerator air deliven' ��� T�r►ca� . '
16�Glean stainless steel aspirator shaft
i —sa
�'Ciean aspiratortip
�iean fresh air vent in concrete cover � v � � � ��,;���•..-
I�Inspe.��aeration chamber conten#s
CI,Ak2IFI.�ATIOI�i CHAI��ER SBRVICE
■,i�move the Bio-I�inetic system �„ . i ,�..-� �_�
B�Scrape#he clarification ahamber ;�,1�._ctiL � �--erc_. S-� �v►5 �.�t �
�pect#he Bio-Static sludge retum
pe�t outlet caupling
0 Install a�lean Bio-K�etic s�stem
C]�'ill Biue Crystal feed tube{if installed)
�FiII Bio-Neu.tralizer feed iube{if installed)
G NERAL SER ICE
�spect e$Iuen#punip cham6er
�peet ef.�uent qttality � ' - w,.e�. �gj�
Inspec#ou�et line .�. .- ��
D Inspect ground wat�x'relief poi�(if i't�.stalled} �, - �
�nspect effluen#disposat system ,r��+, �SGIr� �
❑Complete owner service record , yy �w. �i� ,
❑Complete heaitlt department no 't�f'icatian ( t, � �
❑Complete distributar service;record j
r' d!
l�Mail healtla depaztment notification �- .(�,.- . ; '
��1 �t1� Siegmund Es��iru2tmental Services,lnC. J
��i�Zi ��� FLUID TIiI1VHING.CT.EAR SOLUTIOPTS
.i �
1"�'i (� �6 wwsv.sieamund�'oup.c.am
No� � -t�� -1'�,�
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���8 @J��� ��R� �'Y.�.►'�`�'�r����� .4 J���1'l��� ,1��' ►.��t��'�1�`R
SERVICE II�SPEC`TTON �HECKLIST
Address: �-��.,�" } �'.���� �-- Owner: ��^i.i1��., ��,���,.
Operator.--�,� Dafe: ��, .�' i r`�`• 1�
�
This checklist stu�nmarrizes the service procedures to be perfonm ed during a routine Sing�.�air 960 NR inspeciiou Refer to the
Singulair Manual far a detailsd explanation of eaeh service procedure and ara O&M t�'oub2eshooting guide.
CONTROL CEN'T�R S�RVIC� NOTESjCOMMENTS
�Check operation o£control eenter � ,Pl'�' �.��v�c:� C�-�`'��� ' �sZ-
�Adjust tuna ciQek when required � k. ' �� � .�'� �e't.
Cheak o eration ofrecireul 'on control panel �,��.�. �/'G5 V' ��. 6�''�� ".
� ��d.� ����
�FFLUENT�E IRCULATION SYSTEM t
Check operation ofrecucuta�ian pump '`f"s�ft�, ' � c��" rrJ -.�� '�..ey�
Inspect recirculation wel�&fi �L e�� �.- �;
�
'�`est Operation -- t,' '�i`.�v� �
Set recirculafiion rate rate Q minlhr � •_ !��
����
A�RAT-O�R SERVTCE / �
G`�1ELJ EC�C A8T'Q�OT O�.IeT'd�t011 � ��!r �'if.�
heck aerator power cflnsumption rr� r�� .���►�� -t.,
Check aerator air delivery
Clean stainless steel aspir�or shaft
�Clean aspirator tip
lean fresh an-vsnt in conorete cover �}3 �trryti �`` 5(J p�.
Inspect aeration chamber contents �
FICATION C�IAMBER SERVICE
Remove tt�e BiaKinetic system
Scrape the clarifica.tion chambex
spect the Bio-Static sludge r�furn
Inspect outlet coupiing � _
. O Install a clean Bio-Kinetic system
❑�ill Blue Crys�l feed tube(if installed}
�Fill Bio-Neutralizer feed tube(if installed}
VERAL SBRVICE
Inspect e.f�lue�t pump ch,amber �l��M.�-? �l� �{��i:��vt fvf{`a���
spect effluent quality . . � i
Tnspec�outlet line � .
��nspect ground water relief point(if installed) �. , c �� �y, ��.-��k'fn�
6�Inspect efflusnt disposal system ..�3 �'.� � �i.��zei �- � "����
❑Complete owner service record �.�j r� ��� ;
C1 Coznplete health depar#ment no#i�oation `.� # � �. �� � '�e,t� . i
C3 Conaplete distributor service reccsrd ___���� - �
0 Mai1 health department notification �, L ot.{.�.g; �� ��c,�
.� (,, �j� S' und Environmentai Services Inc.
�t S 4^` ��'`'�` �'�.c� F�I.LTIll 1`HIIVKiNG.CLEAR SOLU3'IO1V8.
�'1��" Y/� ''��j� '�j wa��ndgx'out>.cam
� (_�J,I
���'� ��� ` 1��uj
�,�� ��U
I �G�,�v�. .
� � ., ' �C,�
��TC�� 9�� � TE�VAT`�+ 1� � 1�T l�� S�S��
�E�.�TICE �T��'��'�'IOl� CI���,IS'�'
�.aa��ss:3�� ��°,�� t��--� �� o�: �f�►<��
Operator._'`)�� C.�-'� `� �'��=�` ,-�-��. Date: � O'�; �o 'C"� � � ��
�
Tbis checklist s�ummarizes the service procedures to be p�ionned during a rouhne Singulair 960 NR inspection Refer to the
Singulair Marival for a detailed�xplanation of each se�vice procedure and an O&M troubleshootinj Duide.
CONTROL CENTER SERVICE I>T�TESfGOMMENTS
�Check operation of control center �� ���..�:.��4��' �. �-'����"�--< ���°�� �`"'�
�Adjust time clock when required � --a,f�•.�'� �; ���..
�heck operation of recirculation control panel �,�F�`v��-- V�:°-=\ i�� +J�,�e.;�.`�� ����,.
NR EFFI;UENT RE�IRCULATION SYSTEM
e�heck operatian of recirculation pump ���h�"�-; �a���^.� v�� t��-�=�._{.�,�•. �w L:- �
`�Inspect recirculation well&fittinas �Os� �.�.,,�'.� ��.��� :°�5<,�<... _ ���.� ���:., ;,@;.,--
�Test Operation _ e,���> ��-� ,`?f'°-r�-' � PLy�ti,r.
�Set recirculation rate rate @ min/fir °3 �`�".��
5`l �=4�.����
pFR ATOR SERVICE
eck aerator operation ��-�C'�S,L✓' �� ��•^,�-:�'.�%�-^��^�, �'�^'���"�`�,
❑Check aerator power cansumption �
�Check aerator air deliveay y3`=1`�-� ���-
,�.Clean.stainless steel aspirator shaft �
��Clean aspirator tip , �v ��>` , �;�„ . �.���•.. 1� l���'�
C�Clean fresh a�ven.t in.concrete cover �,r� ;�,,,y:�"s..�-�.
❑Inspect aea�tian chamber corteats
CLARIFICATI�N CHA.MBER SERVIGE
emove the Bio-IKinetic system ��,c �- �`�-.��w�l� ��<,��.-�.r' �.�.���S�<� ���`'
�Scrape tb.e clarificati.on�hamber
Inspec�the Bio-Static sludn8 iSil]fII `C� .,, �:� � � �,:�.�;�:µ,; �,�=�-~�-�= �'"'�
ect outlet coupling 3 tis eb
�Install a clean Bio-Kine#ic system
�Fill Blue Crystal feed tube(if installed) �
8 Fill Bio-Neutralizer feed tube{if installed)
GENERAL SERVICE ���'� ��
t�.� pectefEluentptnnp chamb� ,� , 3•� �,v�,,, C,��•r.�,�' -�������� ��"���-"�"`�i ;
v�.lnspect effluent quality �;;;1r, ._`d�� j
�Inspect outlet li.ne 5 Z, U 5,u^^ .�a 1A.,S --'s-. �-ti:���� �����:�� '
�Iaspect ground water relief poin#(if installed) ��. y Z,, �t, �
�Ins p e ct effluent d i s posal s ystem N��-- �3 ;
�Complete owner service record �., -, �,� C.,� ° ;�� ' \ 9;^r'=� 5=�•.:� �' �$�" i
8 Corapiete health department notification� `` �. �� t`�a��,` _ �
�Complete disiributor service record 1`���j� ��
�Mail health department noti�ication �'��- \'� -" .�° �e. � - ='S`�- �`��'� ��
�``��� ��� Siegmund Environmen#ai Servioes,Ina
: V� ��;�` FLUID THINHING.CLEAR SOLUTIOIVS.
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Serial No:03181615:06 �` ``
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ANALYTICAL REPORT
Lab Number: L1607100
Client: Bennett Environmental Associates '
1573 Main Street
Brewster,MA 02631
ATTN: David Bennett
Phone: (508)896-1706
Project Name: VOGLER RESIDENCE
Project Number: BEA15-10846
Report Date: 03/18/16
The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its
entirety.Aipha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Certifications&Approvais: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 8d0-624-9220-www.alphalab.com
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Page 1 of 15
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' Serial No:03181615:06
Project Name: VOGLER RESIDENCE Lab Number: L1607100
Project Number: BEA15-10846 Report Date: 03/18/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and tf�e Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for ail
NELAP accredited parameters unless othervuise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data�.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(T1Cs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if oniy a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corcective
action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multipie Batch Qualiry Control elements are reported(e.g.more_than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific°!o recovery or RPD value that is oirtside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qual�ers and acronyms used in this report are provided in the Glossary
located at the back of the report.
' In reference to questions H(CAM)or 4(RCPj when"NO"is checked,the performance criteria for CAM and RCP methods allow for some
quality controi failures to occur and still be within method compliance. In these instances the specfic failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
from the date the project is completed.After 21 qlendar days,we will dispose of aii samples submitted inciuding those put on hold unless
you have contacted your Ciient Service Representative and made arrangements for Alpha to continue to hoid the samples.Air canisters will
be disposed after 3 business days from the date the project is completed.
Please contact Client Senrices at 800-6249220 with any questions.
I,the undersigned, a#test under the pains and penaities of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
—�-I�-��d� Lu ra L Troy
O~- .
Authorized Signature:
Title: Technical Director/Representative Date: 03/18/16 '
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Page 3 of 15 �' ��, ��
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Page 4 of 15 -
. Serial No:03181615:06
Project Name: VOGLER RESIDENCE Lab Number: L1607100
Project Number: BEA15-10846 Report Date: 03/18/16
SAMPLE RE3ULTS
Lab ID: L1607100-01 Date Collected: 03110/16 12:15
Client(D: EFFLUENT Date Received: 03/11/16
S2111p1@ LOCatIOCI: SOUTH YARMOUTH,Ma Field Prep: Not Specified
Matrix: Water
� Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method pnalyst
General Chemistry-Westborough Lab
Solids,Total Suspended 6.1 mg/I 5A NA 1 - 03/17/16 03:12 30,2540D RT
Nitrogen,Nitrite 0.54 mgll 0.050 — 1 - 03/11/16 21:47 44,353.2 MR
---------•------_._---...------------..------..- ------------------------..__---_.---..�___.._.---------------....--------------
Nitrogen,Nitrate 1.3 mg/l 0.10 — 1 - 03/11/16 21:47 44,353.2 MR
Nftrogen,Total Kjeldahl 49.8 mg/I 3.00 -- 10 03/13/16 20:00 03/16/16 22:42 30,4500N-C AT
BOD,5 day 37. mg/I 2.0 NA 1 03/12/16 04:55 03/16/16 23:10 30,52106 TA '
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Page 5 of 15
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Serial No:03181615:06 '
Project Name: VOGLER RESIDENCE Lab Number: L1607100 , '
Project Number: BEA15-10846 . Report Date: 03/18/16 �
Method Blank Analysis
Batch Quality Control
I
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared �4nalyzed Methoe! Analyst '
General Chemistry-Westbor,ough Lab #or sample(s); 01 Batch: WG873113-1
_ _ : _ �
Nitrogen,Nitrate ND mg/l 0.10 — 1 - 03/11/16 21:30 44,3532 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873114-1
Nitrogen,Nitrite ND mg/I 0.050 — 1 - 03/11/16 21:32 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873206-1 ` � ��
BOD,5 day ND mg/I 2.0 NA 1 03/12/16 04:55 03/16/16 23:10 30,5210B TA
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873440-1 I
t
Nitrogen,Totai Kjeldahl ND mg/I 0.300 — 1 03/13/16 20:00 03/16/16 22:31 30,4500N-C AT �
i
General Chemistry-Westborough Lab for sample(s): 01 Batch`. WG874594-1
Solids,Total Suspended ND mg/I 5.0 NA 1 - 03/17/16 03:12 30,2540D RT �
_......._._.... ......_........... ..................................._...__..._..........._........_. _._.._....._..._..___.._....__.................._._....... .__...._............_..._
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Serial No:03181615:06
Project Name: VOGLER RESIDENCE Lab Number: L1607100 3
Project Number: BEA15-10846 Report Date: 03/18/16 '
�
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Sample Receipt and Container information i
Were project specific reporting limits specified? YES �
Cooler Information Custody Seal
Cooler
A Absent
Container Information Temp �
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1607100-01A Piastic 250m1 H2SO4 preserved A <2 3.5 Y Absent TKN-4500(28) '
L1607100-01 B Plastic 950mi unpreserved A 7 3.5 Y Absent NO�-353(2),BOD-5210(2),NO3-
353{2)
L1607100-01C Plastic 950m1 unpreserved A 7 3.5 Y Absent TSS-2540(7) ,
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*Values in parentheses indicate holding time in days ��� ;�
Page 10 of 15
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' Seriai No:0318'1615:06
Project Name: VOGLER RESIDENCE Lab Number: L1607100
� Project Number: BEA15-10846 Report Date: 03/18/16
GLOSSARY
Acronyms
EDL •Fstimated Detection Limit:Tlris value represents the level to which target analyte concentrations are reported as estimated
values,when those target analyte concenharions are quantified below the reporting limit(RL).The EDL includes any
adjustments from dilutions,concenh�ations or moisture content,where applicable.The use of EDLs is specific to the analysis of
PAHs using Solid-Phase Microextraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratory Conh�ol Saznple:A sawple matrix,fi�ee from the analytes of interest,spiked with verified lmown amounts of analytes
or a material containing lmown and verified amounts of analytes.
LCSD -Laboratory Control Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample maffix,free from the analytes of interest,spiked with verified known amounts of analytes
or a material containing known and verified amounts of analytes.
14IDL -Method Detection Limit:Tlus value represents the level to which target analyte concenirations are reported as estimated values,
when those target analyte concenh•ations are quantified below the reporting limit(RL).The MDL includes any adjushnents from
dilutions,concentrations or moisture content,where applicable.
MS -Matrix Spi�ce Sample:A sampie prepazed by adding a lrnown mass of target analyte to a specified amount of mahix sample for
which an independent estimate of tazget analyte conceatration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS
NA -Not Applicable.
NC. -Not Calculated: Term is utilized when one or more of Nie results utilized in the calculation are non-detect at the parameter's
reporting uni�
NI -Not Ignitable.
NP -Non-Plastic:Terrn is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit The value at which an instrument can accurately measure an analyte at a specific concentration.The RL
includes any adjustments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results from matrix and/or matrix spike duplicates aze primarily designed to assess the precision
of analytical results in a given mahix and are e�ressed as relative percent difference(RPD). Values wluch aze less than five
times the reporting limit for any individual pazameter are evaluated by utilizing the absolute difference between the values;
althouoh flie RPD value will be provided in the report.
SRM -Standard Reference Material:A re€erence sample of a lmown or certified value that is of the same or similaz mahix as the
associated fieid samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TIC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound list
(TCL)for the method and/or program.All TICs are qualitatively idenfified and reported as estimated concentrarions.
Footnotes
1 -The reference for tivs analyte should be considered modified since this analyte is absent from the target analyte list of the original
method.
Terms
Total:With respect to Organic analyses,a'Total'resuit is defined as the summation of results for individual isomers or Aroclors.If a'TotaP
result is requested,the results of its individual componenis will also be reported.This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from wluch the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Qualifiers
A -Specha identified as"Aldol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrarions of the analyte at less than ten times(l Ox)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concenirations of the analyte at less than ten times(l Ox)
the concentration found in the blank.For DOArelated projects,flaa only applies to associated field samples that have detectable
concenlrations of the analyte at less than ten times(I Ox)the concenh�ation found'm the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated field samples ihat have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentcations of ihe analyte,which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab wntaminants(Phthalates,Acetone,Methylene Chloride,2 Butanone). '
Report Format Data Usability Report
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� Serial No:03181615:06 ' �
Project Name: VOGLER RESIDENCE Lab Number: L1607100 '
Project Number: BEA15-10846 Report Date: 03/18/16 �
Data Quali�ers �
C -Co-elution:The tazget analyte co-elutes with a known lab standard(i.e.surrogate,intemal standards,etc.)for co-extracted �
analyses.
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrarions �
ofthe analyte.
E -Concentration of analyte exceeds the range of ihe calibrafion curve and/or lineaz range of the inshument.
G -The concentration may be biased high due to mahix interferences(i.e,co-elution)with non-target compound(s).The result should
be considered estimated. �
H -The analysis of pH was performed beyond the regulatory-reqnired holding time of 15 minutes&om the time of sample collecdon.
I -The lower value for the two columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for flris analyte. �
NJ -Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICs),where �
the identification is based on a mass spec�al library search. �
P -The RPD behveen the results for the two columns exceeds the method-specified criteiia. '
Q -The quality control sample exceeds the associated acceptance criteiia.For DOD-related projects,LCS and/or Continuing Calibration �
Standard exceedences are also qualified on all associated sample results. Note:Tlus flag is not applicable for matriac spike recoveries I
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concenh�ations are less �
than Sx the RL.(Metals only.) �
R -Analytical results aze from saznple re-analysis. `
RE -Analytical results are from sample re-extraction. �
S -Analytical results are from modified screening analysis. ;
J •Estimated value.This represents an estimated concenh•adon for TentaGvely Identified Compounds(TICs). �
ND -Not detected at the reporting limit(RL)for the sample. `
i
Report Format: Data Usability Report
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� Serial No:03181615:06
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Project Name: VOGLER RESIDENCE Lab Number: L1607100
Project Number: BEA15-10846 Report Date: 03/18/16
REFERENCES
30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-
WPCF. 18th Edition. 1992.
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100,August 1993.
LIMITATION OF LIABILITIES
Alpha Analytical perForms services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
sha�l be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequen#ial or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. '
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling,
containers,sampling procedures, holding time and splitting of samples in the field. '
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Page 13 of 15
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Serial No:03181615:06 i
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 6 �
Department: Quality Assurance Published Date:2/3/2016 10:23:10 AM ,
Title� Certificate/Approval Proqram Summarv Paqe 1 of 1
Gertification Information
The foilowing analytes are not inciuded in our Primary NELAP Scope of Accreditation:
Westborough Facility �
EPA524.2:1,2-Dibromo-3-chloropropane,1,2-Dibromoethane,m/p-xylene,o-xylene '
EPA 624:2-Butanone(MEK),1,4-Dioxane,tert-Amylmethyl Ether,tert-Buryl Alcohol,m/p-xylene,o-xylene '
EPA 625: Aniline,Benzoic Acid,Benzyl Alcohoi,4-Chloroaniline,3-Methylphenol,4-Methylphenoi.
EPA 1010A: NPW: Ignitability
EPA 6010C: NPW:Strontium;SCM: Strontium
EPA8151A: NPW:2,4-DB,Dicamba,Dichloroprop,MCPA,MCPP;SCM: 2,4D6,Dichloroprop,MCPa,MCPP
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene,Isopropanol;SCM:lodomethane(methyl iodide),Methyl methacrylate
(soil);1,2,4,5-Tetramethylbenzene;4-EthyRoluene.
EPA8270D: NPW:Pentachloronitrobenzene,1-Methyinaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Pentachloronitrobenzene,1-
Methylnaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 9010: NPW: Amena6le Cyanide Distillation,Total Cyanide Distiliation
EPA 9038: NPW: Sulfate
EPA9050A: NPW:Specific Conductance ;
EPA 9056:NPW:Chloride,Nitrate,Sulfate
EPA 9U65: NPW:Phenols
EPA 9251: NPW:Chloride
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3. '
SM5310C:DW:Dissolved Organic Carbon
Mansfield Facility
EPA 8270D:NPW: Biphenyl;SCM: Biphenyi,Caprolactam !
EPA8270D�IM Isotope Dilution: SCM: 1,4-Dioxane .
SM 2540D: TSS
SM2540G: SCM:Percent Solids '
EPA 1631E:SCM: Mercury
EPA 7474: SCM: Mercury
EPA8081B:NPW and SCM:Mirex,Hexachlorobenzene.
EPA 8082A:NPW: PCB:9,5,31,87,101,110,141,151,153,180,183,18Z
EPA 8270SIM: NPW and SCM: Alkylated PAHs. '
EPA TO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4-TrimetMyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene,n-
Butylbenzene,n-Propylbenzene,sec-Butylbenzene,tert-Butylbenzene.
Biological Tissue Matrix: 8270D-SIM;3050B;3051A;7471B;80816;8082A;6020A:Lead;8270D:bis(2-ethylhexyl)phthalate,Butylbenrylphthalate,
Diethyl phthalate,Dimethyl phthalate,Di-n-butyl phthalate,Di-n-octyl phthalate,Fluoranthene,PentachlorophenoL ',
The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility:
Drinking Wafer
EPA200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA200.7:Ba,Be,Ca,Cd,Cr,Cu,Na;EPA245.1:Mercury;
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1,
SM2130B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate.
Microbiology:SM9215B;SM9223-P/A,SM9223B-Colilert-QT,Enterolert-LIT. j
i�ll
Non-Pota6le Water
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;
EPA200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; '
EPA 245.1,SM4500H,B,EPA 120.1,SM25106,SM2540C,SM2340B,SM2320B,SM4500CL-E,SM4500E-BC,SM426C,SM4500NH3-BH,EPA
350.1:Ammonia-N,LACHAT 10-107-06-1-8:Ammonia-N,SM4500NO3-F,
EPA 353.2:Nitrate-N,SM450UNH3-BC-NES,EPA 357.1,SM4500P-E,SM4500P-B,E,SM5220D,EPA 410.4,SM5210B,SM5310C,SM4500CL-D,
EPA 1664,ShA14 510AC,EPA 420.1,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan I,Endosulfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC(AcidBase/Neutral Extractables),,EPA 600/4-87-045:PCB-Oil.
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID:08-113
Page 14 of 15
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Serial No:06161621:23
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ANALYTICAL REPORT
Lab Number: L1617850
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
ATTN: David Bennett '
Phone: (508)896-1706
Project Name: VOGLER RESIDENCE ;
Project Number: BEA15-10846
Report Date: 06/16/16
The original project report/data package is held by Alpha Analyticai.This reportldata package is paginated and should be reproduced only in its
entirety.Alpha Analytical holds no responsibility for resuits and/or data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI{LA000065),ME(MA0008&),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www,alphalab.com
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Page 1 of 15
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• Serial No:06161621:23
� Project Name; VOGLER RESIDENCE Lab Number: L1617850
Project Number: BEA15-10846 Report Date: 06/16/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Resufts contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individuai sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective
action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is boided in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4{RCP)when"NO"is checked,the pertormance crfteria for CAM and RCP methods allow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical ,
Standards requested on the Chain of Custody. '
HOLD POLICY i
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days !
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless '
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will
be disposed after 3 business days from the date the project is completed.
Please contact Client Services at 800-624-9220 with any questions.
1,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowiedge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This cert�cate of analysis is not
complete unless this page accompanies any and all pages of this report.
G��� Cristin Walker �
Authorized Signature:
Title: Technical Director/Representative Date: 06/16/16 '
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Page 3 of 15 ',�g��-�'„`a.
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Serial No:06161621:23 . I
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_ _ _ _ _ _ _ _ __ . . _ _ _ _ __
INORGANICS
&
MISCELLANEOUS
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Page 4 of 15 I
Serial No:06161621:23
� Project Name: VOGLER RESIDENCE Lab Number: L1697850
Project Number: BEA15-10846 l2eport Date: 06/16/16
SAMPLE RESULTS
Lab ID: L1617850-01 Date Collected: 06/10/16 12:30
Client ID: EFF�uENT Date Received: 06/10i16
Salllpl@ LOC3tio11: SOUTH YARMOUTH,Ma Fieid Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab
Solids,Total Suspended 18. mg/l 5.0 NA 1 - 06l13/16 16:35 121,2540D SG
------_..._—_.__....----------....___- --------------------__-------- -------------------..._....._..------------------......--------
Nitrogen,Nitrite 16. mg/I 025 — 5 - 06/10/16 22:03 44,353.2 MR
--------------.._....---..—._.._..---�----------- ------------------ -----------------_____....._._._._.�..____....�......__-----...--------
Nitrogen,Nitrate 1.1 mg/I 0.50 — 5 - 06/10/16 22:03 44,3532 MR
.--...__.___�_.._______--------— --------._. _—�..---------�—�_��_�_�..----.._. -- --_..�_..--
Nitrogen,Total Kjeldahl 3.94 mg/I 0.300 — 1 06l13/16 20:00 06/15/16 22:14 121,4500N-C AT
....._.._.------..._._...�.__._..........-----------..._._..__�.__._�..--------.._—.._...._...._____._._...---...._—.._-----._.._...--------------- �-----.._.._.__�.�—__...._.._...-----
BOD,5 day 18. mg/l 2.0 NA 1 O6/11l16 04:15 O6/15116 23:10 121,5210B TA
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Page 5 of 15
I
Serial No:06161621:23
Project Name: VOGLER RESIDENCE Lab Number: L1617850 •
i
Project Number: BEA15-10846 Report Date: 06/16/16 ;
Method �lank Analysis
Batch Quality Control
Dilution Date Date Analytical
Parameter IZesult Qualifier Units RL f1ADL Facfior Prepared Analyzed Method Analyst ,
General Chemistry-Westborough Lab for sample(sj: 01 Batch: WG902832-1
Nitrogen,Nitrate ND mg/I 0.10 -- 1 - 06/10/16 20:58 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch` WG902833-1
Nitrogen,NiVite ND mg/l 0.050 — 1 - 06/10/16 21:00 44,353.2 MR
General Chemistry-Westborough Lab for sample(s); 01 Batch: WG902977-1
BOD,5 day ND mg/I 2.0 NA 1 06/11/16 04:15 06115/16 23:10 121,52108 TA
General Chemistry-Westborough Lab for sample(s): Q1 Batch: WG903365-1
Solids,Total Suspended ND mg/I 5.0 NA 1 - 06/13/16 16:35 121,2540D SG
General Chemistry-Westborough Lab for sample(s): 01 Batch; WG903494-1
Nftrogen,Total FCeidahl ND mgfl 0.300 — 1 06/13/16 20:00 06/15/16 22:07 121,4500N-C AT
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Serial No:06161621:23
Project Name: VOGLER RESIDENCE Lab Number: L1617850 � '
Project Number: BEA15-10846 Report Date: 06/16/16 ',
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Sample Receipt and Container Information '
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Were project specific reporting limits specified? YES �
C�oler Information Gustody Sea!
Cooler
q Absent
Container Information Temp
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1617850-01A Plastic 250mi H2SO4 preserved A <2 3.3 Y Absent TKN-4500(28) '
L1617850-01 B Plastic 950m1 unpreserved A 7 3.3 Y Absent NO2-353(2),BOD-5210(2),NO3- '
353{2)
L1617850-01 C Plastic 950m1 unpreserved A 7 3.3 Y Absent TSS-2540(7)
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*Values in parentheses indicate holding time in days _���
Page 10 of 15
Serial No:06161621:23
� Project Name: VOGLER RESIDENCE Lab Number: L1617850
Project Number: BEA15-10846 Report Date: 06/16/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:Tlus value represents the level to which target analyte concentrations are reported as esrimated
values,when those target analyte concentrations aze quantified below the reporting limit(RL).The EAL includes any
adjushnents from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratory Conhol Sample:A sample matrix,free from the analytes of interest,spiked with verified imown amounts of
analytes or a material containing Imown and verified amounts of analytes.
LCSD -Laboratory Conirol Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounu of
analytes or a material containing known and verified amounts of analytes.
MDL -Method Detection Limit:This value xepresents the level to which tsrget analyte concentrations aze reported as estimated
values,when those tazget analyte concentrations aze quantified below the reporting limit(RL).The IvIDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.
MS -Matrix Spike Sample:A sample prepazed by adding a]mown mass of target analyte to a specified amount of matrix sample for
wluch an independent estimate of target analyte concentration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicabie.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit
NDPA/DPA -N Nitrosodiphenylamine/Diphenylamine.
NI -Not Ignitable.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil. �
RL -Reporting Limit: The value at wlrich an instrument can accw�ately measure an analyte at a specific concentration.The RL
includes any adjustments from dilutions,conczntrations or mois4ue content,where applicable.
RPD -Relative Percent Difference: The results from mairix and/or mah ix spike duplicates are prnnarily designed to assess the
precision of analytical results in a given matrix and aze expressed as relative percent difference(RPD). Values which are less
thau five times the reporting limit for any individual parameter aze evaluated by utilizing the absolute difference betoveen the
values;although the RPD value will be provided in the report
SRM -Standard Reference Materiat:A reference sample of a]aiown or certified value that is of the same or simi]ar mahix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TTC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound
list(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations.
Foofnotes
1 -The reference for this analyte should be considered modified since this analyte is absent firom the target analyte list of the
original method.
Terms
Total:With respect to Organic analyses,a'Total'result is defined as the summation of results fot individual isomers or.Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which tiie method originates and the analytical reference method(Exunple:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents aze provided in the References section of the Addendum.
Data Qualifiers
A -Spectra iden6fied as"Aldol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox)
the concenh�ation found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable
concentrafions of the anatyte at less than ten times(l Ox)the concen�ation found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting�imit for common lab contaminants)in the associated method blank.For NJ-
Air-related pmjects,flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concenh�ations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the
Report Format. Data Usability Report
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Page 11 of 15
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Serial No:06161621:23
Project Name: VOGLER RESIDENCE Lab Number: L1617850 •
Project Number: BEA15-10846 Report Date: 06/16/16
�
Data Qualifiers _ �
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone). !
C -Co-elution:The tazget analyte co-elutes with a Imown lab standard(i.e,surrogate,intemal standazds,etc.)for co-extracted '
_ _ _ . ._
analyses. '
_ __ __ _ . _
D -Concenfration of analyte was quantified from diluted analysis.Flag oniy applies to field saznples that have detectable concentrations
of the analyte.
E -Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument
G -The concentration may be biased hiah due to malrix interferences(i.e,co-elution)with non-target compound(s).The result should
be considered estimated.
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
I -The lower value for the two columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for dus analyte.
NJ -Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral library search.
P -The RPD between the results for the two columns exceeds the method-specified criteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calbration
Standard exceedences are also qualified on all associated sample results. Note:Tlus flag is not applicable for mahix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations aze less
than Sx the RL.(Metals only.)
R -Analytical results aze from sample re-analysis.
RE -Anatytical results aze from sample re-extracdon.
S -Analytical results are from modified screening analysis.
J -Estimated value.Tlus represents an estimated concentration for Tentatively Identified Compounds(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
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Report Format. Data Usability Report
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Page 12 of 15
' Serial No:06161621:23
: Project Name: VOGLER RESIDENCE Lab Number: L1617850
Project Number: BEA15-10846 Report Date: 06/16/16
REFERENCES
44 Methods for the Determination of Inorganic Substances in Environmentai Samples,
EPA/600/R-93/100, August 1993.
121 Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
LIMITATION OF LIABILITIES '
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. ln no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha AnalyticaL
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling,
containers,sampling procedures, holding time and splitting of samples in the field.
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Page 13 of 15
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Serial No:06161621:23
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 6 • ,
• Department: Quality Assurance Published Date: 2/3/2016 10:23:10 AM �
Title� Certificate/Approval Proqram Summarv Paqe 1 of 1
Gertification Information
The following analytes are nof included in our Primary NELAP Scope of Accreditation:
__ ._ _ _ __
_ _.
__ __ __ __. _ . _ __. ._ .
Westborough Facility _
EPA524.2:1,2-Dibromo-3-chloropropane,1,2-Dibromoethane,m!p-xylene,o-xylene
EPA 624:2-Butanone(ME{�,1,4-Dioxane,tert-Amylmethyl Ether,tert-Butyl Alcohol,m/p-xylene,o-xylene
EPA 625: Aniline,Benzoic Acid,Benryl Aicohol,4-Chioroaniline,3-Methylphenol,4-Methylphenol.
EPA 1010A: NPW: Ignitability
EPA 6010C: NPW:Strontium;SCM: Strontium
EPA 8151A: NPW:2,4-DB,Dicamba,Dichloroprop,MCPA,MCPP;SCM: 2,4-DB,Dichloroprop,MCPA,MCPP
EPA 8260C:NPW:1,2,4;5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene,Isopropanol;SCM:lodomethane(methyl iodide),Methyl methacrylate
(soil);1,2,4,5-Tetramethylbenzene;4-Ethyltoluene.
EPA 8270D: NPW:Pentachloronitrobenzene,1-Methylnaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Pentachloronitrobenzene,1-
Methylnaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 9010: NPW: Amenable Cyanide Distillation,Total Cyanide Distillation
EPA 9038: NPW: Suffate
EPA 9050A: NPW:Specific Conductance
EPA9056:NPW:Chloride,Nitrate,Sulfate
EPA 9065: NPW:Phenols
EPA9251: NPW:Chloride
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved organic Carbon
Mansfield Facility
EPA 8270D:NPW: Biphenyl;SCM: Biphenyl,Caprolactam
EPA 8270DSIM Isotope Dilution: SCM: 1,4-Dioxane
SM 2540D: TSS .
SM2540G: SCM:Percent Solids
EPA 1631E:SCM: Mercury
EPA 7474: SCM: Mercury
EPA 8081 B:NPW and SCM:Mirex,Hexachlorobenzene.
EPA8082A:NPW: PCB:1,5,31,87,1�1,110,141,151,153,180,183,187.
EPA 8270-SIM: NPW and SCM: Alkylated PAHs.
EPATO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4-Trimethyl-l-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene,2-Ethylthiophene, 1,2,3-Trimethylbenzene,Indan, Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene,n-
Butyibenzene,n-Propylbenzene,sec-Butylbenzene,tert-Butylbenzene. `
Biological Tissue Matrix: 8270D-S/M;30508;3051A;74718;8089B;8082A;&020A:Lead;8270D:bis(2-ethylhexyl)phthalate,Butylbenrylphthalate, (
Diethyl phthalate,Dimethyl phthalate,Di-n-butyl phthalate,Di-n-octyl phthalate,Fluoranthene,Pentachlorophenol. �
i
t
The following analytes are inciuded in our Massachusetts DEP Scope of Accreditation,Westborough Facility:
Drinking Water ;
EPA200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7:Ba,Be,Ca,Cd,Cr,Cu,Na;EPA 245.1:Mercury;
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1, !
SM2130B,SM4500C1-D,SM23206,SM2540C,SM4500H-B
EPA 332:Perchlorate. '
Microbiology.SM9215B;SM9223-P/A,SM9223B-Colilert-QT,Enterolert-QT.
Non-Potable Water
EPA200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; ,
EPA 245.1,5M45DOH,B,EPA 120.1,SM25106,SM2540C,SM2340B,SM2320B,SM4500CL-E,SM4500E-BC,SM426C,SM450DNH3-BH,EPA
350.1:Ammonia-N,LACHAT 10-107-06-1-8:Ammonia-N,SM4500NO3-F,
EPA 353.2:Nitrate-N,SM4500NH3-BC-NES,EPA 351.1,SM4500P-E,SM4500P-B,E,SM5220D,EPA 490.4,SM5210B,SM5310C,SM4500CL-D,
EPA 7664,SM14 510AC,EPA420,1,SAA4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-6HC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan I,Endosutfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC(Acid/Base/Neutral Extractables),EPA 600i4-81-045:PCB-Oil.
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: 08-113
Page 14 of 15
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Serial No:09111619:52
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A`:1V}► l.:Y,�T 1 G A L
ANALYTICAL REPORT
Lab Number: L1627747
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631 ,
ATTN: David Bennett '
Phone: (508)896-1706 ;
Project Name: VOGLER RESIDENCE ',
Project Number: BEA15-10846
Report Date: 09/11/16
The original project repott/data package is held by Alpha Analyticai.This repottldata package is paginated and should be reproduced only in its
entirety.Alpha Analytical holds no responsibility for results andlor data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com �
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Serial No:09111619:52
' Project Name: VOGLER RESIDENCE Lab Number: L1627747
Project Number: BEA15-10846 Report Date: 09/11/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Aipha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sampie specific Quality Controi data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Ident�ed Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even'rf only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective
action and if both sets of data are reported.,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g,more than one LCS},the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific°/a recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along with any associated usability implications.Soii/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qual"fiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance criteria for CAM and RCP methods allow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed ',
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical ',
Standards requested on the Chain of Custody. '
HOLD POLICY ',
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days ',
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those puY on hoid unless '
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will
be disposed after 3 business days from the date the project is completed. .
Please contact Ciient Senrices at 800-624-9220 with any questions.
I,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and
beliefi and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This cert�cate of analysis is not
complete unless this page accompanies any and all pages of this report.
�����(�� Kefly Stenstrom
Authorized Signature:
Title: Technical Director/Representative Date: 09/11/16 �
'�'��;a
Page 3 of 15 �
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Serial No:09111619:52
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_ _ __ _ _ _ _
INORGANICS
&
MI�C�LLi4NE0U�
.��� �
Page 4 of 15
, . ,
Serial No:09111619:52
• Project Name: VOGLER RESIDENCE Lab Number: L1627747
Project Number: BEA15-10846 Report Date: 09/11/16
SAMPLE RESULTS
Lab ID: L1627747-01 Date Collected: 09/01/16 13:00
Client ID: EFFLUENT Date Received: 09/02/16
Sa171p1e LOCat1011: SOUTH YARMOUTH,nnA Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method qnalyst
General Chemistry-Westborough Lab
Solids,Total Suspended ND mg/I 5.0 NA 1 - 09/04/16 14:25 121,2540D SG
N iirogen,Nitrite 0.41 mg/I 0.050 - 1 - 09/02/16 23:53 44,353.2 MR
-----...__..___.._....--.....__-------------------------------- -- ------ --------—.....__..._.._._.__..__...---------------._....__.^._._-------._._
Nitrogen,Nitrate 2.6 mgA 0.10 - 1 - 09103/1600:08 44,353.2 MR
N itrogen,Total Kjeldahl 30.2 mg/l 3.00 -- 10 09/07/16 09:07 09l09/16 00:13 121,4500N-C AT
BOD,5 day 13. mg/I 2.0 NA 1 09/03/16 00:30 09/07/16 23:15 121,52106 JC
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Page 5 of 15
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4
Serial No:09119619:52
Project Name: VOGLER RESIDENCE Lab Number: L1627747 � '
' i
Project Number: BEA15-10846 Report Date: 09/11/16 �
Me#hod �lank Analysis �
Batch Quality Control
�
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared .4nalyzed Method Analyst
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928643-1
Nitrogen,Nitrate ND mg/I 0.10 -- 1 - 09/02/16 22:39 44,3532 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928645-1
Nitrogen,Nitrite ND mg/I 0.050 -- 1 - 09l02/16 22:42 44,3532 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928708-1
BOD,5 day ND mg/l 2.0 NA 1 09/03/16 00:30 09/07/16 23:15 121,5210B JC
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928894-1
Solids,Total Suspended ND mg/I 5.0 NA 'I - 09/04/i6'14:25 121,2540D SG
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG929421-1
Nitrogen,Total Kjeldahl ND mg/l 0.300 -- 1 09/07/16 09:07 09l08116 23:49 121,4500N-C AT
.. . ..... . ...._ .. ......_... . ...... ............. ... . ................. . _......._ ..... . ...... ..... .... .... ........ . .... .... ...... .. ............_. . .... .. ...
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Serial No:09111619:52 . -
Project Name: VOGLER RESIDENCE Lab Number: L1627747 �
Project Number: BEA15-10846 Report Date: 09/11/16 '
Sample Receipt and Container Information
Were project specific reporting limits specified? YES
Gooler Information Custocly Seal :
Cooler
A Absent
Container Information Temp '
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1627747-01A Plastic 250m1 H2SO4 preserved A Q 2.3 Y Absent TKN-4500(28)
L1627747-01 B Plastic 950m1 unpreserved A 7 2.3 Y Absent NO2-353(2),BOD-5210(2),NO3-
353(2)
L1627747-01 C Plastic 950m1 unpreserved A 7 2.3 Y Absent TSS-2540(7)
*Values in parentheses indicafe holding time in days ;''�tli�;�
Page 10 of 15
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- Serial No:09111619:52
• Project Name: VOGLER RESIDENCE Lab Number: L1627747
Project Number: BEA15-10846 Report Date: 09/11/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:This value represents the level to which tazget analyte concentrations aze reported as estimated
values,when those tazget analyte concentrations are quantified below the reporting limit(RL).The EDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction(SPME).
EPA -Envuonmental Protection Agency.
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified lmown amaunts of
analytes or a material containing known and verified amounts of analytes.
LCSD -Laboratory Contr�ol Saznple Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of
analytes or a material containing Imown and verified amounts of analytes.
MDL -Method Detection Limit:Tlus value represents the level to which target analyte concentralions aze reported as estimated
values,when those taz•get analyte concentrations are quantified below the reporting limit(RL).The MDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.
MS -Matrix Spike Sample:A sample prepazed by adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available. .
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parametei's
reporting unit
NDPA/DPA -N Nitrosodiphenylamine/Diphenylamine.
NI -Not Ignitable.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Lixnit The value at which an instrument can accurately measure an analyte at a specific concentration.The RL
includes any adjustments&om dilutions,concentrations or moishse content,where applicable.
RPD -Relative Percent Difference: The results from matrix and/or mah-ix spike duplicates aze priuiarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values wluch are less
than five times tlie reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values;althongh the RPD value will be pmvided in the report.
SRM -Siandaz•d Reference Material:A reference sample of a lmown or certified value that is of the same or similaz matrix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TIC -Tentatively Idenrified Compound:A compound that has been identified to be present and is not part of the target compound
list(T'CL)for the method and/or program.All TICs aze qualitatively identified and reported as estimated concentcations.
Footnotes
1 -The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method.
Terms
Total:With respect to Organic analyses,a'Total'result is defined as the summarion of results for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from wluch the method originates and the analytical reference method.(Fxample:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents aze pmvided in the References section of the Addendum.
Data Quali�ers
A -Specha identified as"Aldol Condensation Product". .
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations ofthe analyte at less ihan ten times(lOx)the concenhation found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(I Ox)
the concenh�ation found in the blank For DOArelated projects,flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting]imit for common lab contaminants)in the associated method blank.For NJ-
Air-related projects,f(ag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flaa only applies to associated field samples that have detectable
concentrations of the analyte,wluch was detected above the reporting limit in the associated method blank or above five times the
Report Format.• Data Usabitity Report
_ ,�, ti�`
��.��,
Page 11 of 15
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M
Serial No:09111619:52 =
Project Name: VOGLER RESIDENCE Lab Number: L1627747 � '
Project Number: BEA15-10846 Report Date: 09/'11/16 ;
Data Qualifiers
repoxting liinit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
C -Co-elution:The tazget anal}rte co-elutes with a known lab standard(i.e.surrogate,inteinal standards,etc.)for co-exh�acted
analyses. _ _
_. ... __. _. _ _
D -Concentration of analyte was quantified fi•oin diluted analysis.Flaa only applies to field samples that have detectabie concentrations '
of the analyte.
E -Concentration of anal}rte eacceeds the range of the calibration curve andlor linear range of the insirument.
G -The concenh�ation may be biased high due to matrix interferences(i.e,co-elurion)with non-taz-get compound(s).The result should
be considered estimated. :
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the tiuie of sample collection
I -The lower value for the two columns has been reported due to obvious interference.
� M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for this analyte.
NJ -Preswnptive evidence of compound.This represents an estimated concenhation for Tentatively Identified Compounds(TICs},where
the identification is based on a mass spectral library search. ;
P -The RPD between the results for the two columns exceeds the method-specified ciYteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration
Standard exceedences aze also qualified on all associated sample results. Note:This flag is not applicable for mat�-u�spike recoveries
when the sample concentradon is greater than 4x the spike added or for batch duplicate RPD when the sampie concentra6ons are less
than Sx the RL.(Metals only.)
R -Analytical results az•e fi•om sample re-analysis.
RE -Analytical results are from sample re-extraction.
S -Analytical results are from modified screening analysis.
J -Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(T'ICs).
ND •Not detected at the reporting limit(RL)for the sample. �
t
Report Format. Data Usability Report
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= Serial No:09111619:52
� Project Name: VOGLER RESIDENCE � Lab Number: L1627747
Project Number: BEA15-10846 Report Date: 09/11/16
REFERENCES
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100,August 1993.
121 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WEF.
Standard Methods Online.
LIMITATION OF LIABILITIES
Alpha Analytical perForms services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way '
connected with the use of, interpretation of, information or analysis provided by Alpha AnalyticaL
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
�ti�
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Serial No:09111619:52 -
Alpha Analytical, Inc. ID No.:'17873
Facility: Company-wide Revision 7 '
Department: Quality Assurance Published Date: 8/5/2016 11:25:56 AM
Title: Certificate/Approval Proqram Summarv Paqe 1 of 1 �
Gertification Information �
�
The foilowing analytes are not inciuded in our Primary NELAP Scope of Accreditation: !
_ _ _. .__ _ _
_ _._ . _ _ _ -_ . _. _.. . _. _ _ _ _
Westborough Facility
EPA 624:m/p-xylene,o-xylene
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene;SCM:lodomethane(methyl iodide),Methyl methacrylate,1,2,4,5-
Tetramethylbenzene;4-Ethyltoluene.
EPA8270D: NPW:Dimethyinaphthalene,1,4-Diphenylhydrazine;SCM:Dimethylnaphthalene,l,4-Diphenylhydrazine.
EPA 300: DW:Bromide
EPA 6860: NPW and SCM:Perchlorate
EPA 9010: NPW and SCM: Amenable Cyanide Distillation
EPA 90128: NPW:Total Cyanide
EPA 9050A: NPW:Specific Conductance
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved Organic Carbon
Mansfield Facility
SM 2540D: TSS
EPA 3005A NPW
EPA 8082A:NPW: PCB:1,5,31,87,101,110,141,151,153,180,183,187.
EPATO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4-Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene.
Biological Tissue Matrix: EPA 3050B
The foliowing analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SAA4500E-C,SM4500CN-CE,EPA 180.1,
SM2130B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate;EPA 524.2: THMs and VOCs;EPA 504.1:EDB,DBCP.
Microbiology:SM9215B;SM9223-P/A,SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B,EPA 120.1,SM2510B,SM2540C,SM2320B,SM4500CL-E,SM4500E-BC,SMA50ONH3-BH,EPA 35D.1:Ammonia-N,LACHAT 10-107- '
06-1-B:Ammonia-N,SM4500NO3-F,EPA 353.2:Nitrate-N,EPA 351.1,SM4500P-E,SM4500P-B,E,SM4500SO4-E,SM5220D,EPA 410.4,
SM5210B,SM5310C,SM4500CL-D,EPA 1664,EPA 420.1,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics, '
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan I,Endosulfan Ii,
Endosutfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs ;
EPA 625:SVOC(AcidBase/Neutral Extractables),EPA 600I4-81-045:PCB-OiL
Microbiology.SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
;
Mansfield Facility:
Drinking Water �I
EPA 200.7:Ba,Be,Cd,Cr,Cu,Ni,Na,Ca.EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TL.EPA 245.1 Hg.
Non-Pota6le Wafer
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Gr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,TL,Ti,V,Zn.
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TL,Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID:08-113
Page 14 of 15
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