HomeMy WebLinkAbout2016 Sep 14 - Singulair Inspection and O&M Report from Bennett Environmental Associates, Inc. ,
� BEI�TNET'�' EI�TVIlZONl�El�TTAL ASSOCIATES, INC.
LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS
1573 Main Street,P.O.Box 1743 (508)896-1706
Brewster,MA 02631 faz(508)896-5109
LETTER �F TR.Al�TSMITTAL
TO: DATE: JOB NUMBER:
Massachusetts Department of Environmental Protection 9/14/16 BEA15-10827
Attention:Title 5 Program
1 Winter Street-6th Floor
Boston,MA 02108 REGARDI1oTG:
Platt Residence REC E�V E�
3 Dove's Wing Road QCT (�3 ?���l
SHIPPING METHOD: 5outh Yaimouth,MA 02664
RegularMail � PickUp � HEALTH DEPT.
Priority Mail ❑ Hand Deliver ❑
Express Mail ❑ Other ❑
Certified Mail � Green Card/RR �
COPIES DATE DESCRII'TION
1 DEP Approved Inspection and O&M Form for Title 5 UA Treatmerrt and Disposal Systems(March,
7une and September 2016)
1 Singulair Service Inspection Checklist(March,June and September 2016) '
1 3/18/16 Alpha Analytical Laboi�atory Report �
1 6/16/16 Alpha Analytical Laboratory Report
1 8/5/16 Alpha Analytical Laboratory Report(resample)
1 9/11/lb Alpha Analytical Laboratory Report
For review and comment: � For approvaL• [� As requested: � For your use: � '
REMARKS:
Please fmd enclosed the DEP Inspection and O&M Forms,Singulair Service Inspection Checklists,and laboratoiy analytical results for
operation and maintenance conducted during the reporting period for the above referenced properiy. If you have any questions or require
� additional information,please contact us at your earliest convenience. Thank you.
cc:Yarmouth Board of Health
Ron Platt,Property Owner
Robin Cassidy-Norweco[via email] .
FROM: Samantha Farrenkopf WWTO#13265
If enclosures aze not as noted,kindly notify us at once
I
. Massachusetts Department of Environmental Protection '
,
Bureau of Resource Protection -Title 5 j
' DEP Approved Inspection and O&M Form for Title 5 1/A �
Treatment and Disposal Systems �
�
A. I nstallation �
Important:When Ron Platt '
filling out forms Owner '
on the computer, . '
use onry the tab 3 Dove's Wing ROad
key to move your Facility Street Address I
cursor-do not South Yarmouth � 02664 i
use the return City Z�P '
key.
� Mailing address of owner, if different:
r� ,
� Street�Address/PO Box.
� City State Z�p ,
(615) 504-4424 ext.
Telephone Number
B. Authorized Service Provider '
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Z�p
(508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265 '
Cert�ed Operator Name Certification Number
C. Facility/System Information '
Singulair 960DN-600
DEP ID Manufacturer ID Model Number
U n known 08/21/2013 '
Installation Date Start of Operation
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No
D. Operating Information
��,�6 12/10/15 System Evaluation
Inspection Date Previous Inspection Date
8"sludge 4"scum" Pumping Recommended � Yes ❑ No
Sludge Depth(to be checked yearly)
t5aiom.doc•rev.0411-13 Page 1 of 3
R
Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5
.
DEP Approved Inspection and O&M Form fo'r 1'itle 51/A
Treatment and Disposal Systems
E, Field Testing .
Field lnspection: .
Color. ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
Effluent Solids: � no ❑ some
pH 7.5 SU p� 2.0 mg/L Turbidity 12.3 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems: ',
8Pd I'
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS�TN� Other(list below) I�
N itrate N itrite TKN
Other 1 Other 2 Other 3 I
G. Inspection and Maintenance
Description of any maintenance pertormed since previous inspection &during this inspection:
On 12/10/15 conduct an initial system e�aluation visit. On 2/26/16 complete repairs to the control
panel and system aerator. Conduct an operation and maintenance event on 3/10/16. Collect effluent
samples for field testin and laborato analysis.
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters. Pumping of the prima portion of the Sin ulair tank is recommended
�
�
�
�
t5aiom.doc•rev.04-11-13 i
Page 2 of 3
Massachusetts Department of Environmental Protection '
; Bureau of Resource Protection -Title 5 �
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems `
�
H. Certification I
I certify: I have inspected the sewage treatment and disposal system at the address above, have �
conducted the required Field Testing and/or sample collection in accordance with Standard Methods, t
have completed this report and the attached technology operation and maintenance checklist, and ;
the information reported is true, accurate, and complete as of the time of the inspection. I am a !
Massachusetts c ' d operator in accordance with 257 CMR 2.00.
� � fi� ��� i
Opera or ignature Date
i
�
System owner must submit this report, technology O&M checklist, and any required sampling results !
to the local board of health as follows for each inspection performed: i
Remedial Use—by January 31�of each year for the previous calendar year i
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31�of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months ;
Send to: �
;
Department of Environmental Protection !
Attention: Title 5 Program
One Winter Street, 5'h Floor
Boston, MA 02108
t5aiom.doc•rev.0411-13 Page 3 of 3
(
Massachu�etts Department of Environmental Protection '
! Bureau of Resource�Protection - Title 5 ;
DEP Approved Inspection and O&M �'orm for Title 5 I/A !
�
�
Treatment and Disposal Systems �
�
A. Installation ;
Important:When Ron Platt
filling out forms Owner �
on the computer, '
use only the tab 3 Dove's Wing Road �
key to move your Facility Street Address !
cursor-do not South Yarmouth 02664 '
use the retum City Z�P �
key.
� Mailing address of owner, if different: �
� �i
Street Address/PO Box: '
tensn �
City State Z�p �
(615) 504-4424 e�.
Telephone Number
B. Authorized Service Provider �
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743 '
Street Address
Bre�nrster MA 02631
City State Z�p
(508) 896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265
Certified Operator Name Certification Number '
C. Facility/System Information �
Singulair 960DN-600
DEP ID Manu#acturer ID Model Number
Unknown 08/21/2013 '!
Installation Date Start of Operation
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial �
Seasonal Residence—used less than 6 mo./year: 0 Yes � No
D. Operating Information
6/10/16 3/10/16
Inspection Date Previous Inspection Date '
10"sludge,4"scum" Pumping Recommended � Yes ❑ No
Sludge Depth(to be checked yearly)
t5aiom.doc•rev.0411-13 Page 1 of 3
f
Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5 ,
DEP Approvecl Inspection and O&M Forrn for �'itle 5 I/A
Treatment and Disposal Systems
E. Field Testing
Field InSpection:
Color: ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
Effluent Solids: � no ❑ some
pH 6.0 SU p� 2.0 mg/L Turbidit 4.32 NTU
6 to 9 2 or greater y 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
9Pd
Parameters sampled: ❑ pH � BOD 0 CBOD � TSS �TN � Other(list below)
N itrate N itrite TKN
Other 1 Other 2 Other 3 �
G. Inspection and Maintenance ,
Description of any maintenance pertormed since previous inspection &during this inspection: I
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis. �
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters. Pumping of the primary tank is recommended.
�
�
�
�
�
t5aiom.doc•rev.04-11-13 Page 2 of 3 '
I
Massachusetts Department of Environmental Protection '
'� Bureau of Resource Protection - Title 5 '
DEP A�aproved Inspection and O&M Form for Title 5 I/A ;
Treatment and �Disposai Systems
�
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have !
conducted the required Field Testing and/or sample collection in accordance with Standard Methods, ;
have completed this report and the attached technology operation and maintenance checklist, and ,
the information reported is true, accurate, and complete as of the time of the inspection. 1 am a ;
Massachusetts ce ' ied operator in accordance with 257 CMR 2.00.
� t�1��° �
Operator Signature Da e �
System owner must submit this report,technology O&M checklist, and any required sampling results
to the local board of health as foAows for each inspection pertormed:
Remedial Use—by January 31�of each year for the previous calendar year '
Piloting Use-within 45 days of inspection date ',
Provisional Use—by March 31th of each year for the previous 12 months ',
General Use—by September 30th of each year for the previous 12 months ',
Send to: '
Department of Environmental Protection '
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108 -
t5aiom.doc•rev.04-11-13 Page 3 of 3
�
Massachusetts Department of Environmental Protection
Bureau of Resource Protection -Title 5 .
DEP Approved Inspection and O&M F'orm for Title 5 I/�►
Treatment and Disposal Systems - - - -
E. Field Testing
_ _ _
Field Inspection:
Color: ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify): .
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
Effluent Solids: � no ❑ some
pH 7.0 SU D0 2.0 mg/L Turbidity 1.63 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use
nitrogen reducing systems:
9Pd I
Parameters sampled: ❑ pH � BOD 0 CBOD � TSS �TN � Other(list below)
Nitrafe Nitrite TKN
Other 1 Other 2 Other 3
G. Inspection and Maintenance �
Description of any maintenance performed since previous inspection &during this inspection: I
Conduct an operation and maintenance event. Collect effluent samples for field testing and I
labora�ory analysis. I
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field testing
parameters.
�
t5aiom.doc•rev.04-11-13 Page 2 of 3 �
�
Massachuse#ts Department of Environmental Protection
� Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&Ni Form for Titie 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts ce ' d operator in accordance with 257 CMR 2.00.
� ��f�
Operator Signature Date
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection pertormed: .
Remedial Use—by January 31�of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31�of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108
t5aiom.doc•rev.0411-13 Page 3 of 3
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SER..VICE II�TS�"ECTION CHEC�L��T ��'���� -�''��,�
Address: '� `�� '�''1�� �-��.�. Qwner: ��-=`� •
Operator. � �. � � �.n �� - ��;: !�(='i3-i Date: ���'>��t�
This checklist su�vmar�zes the service pracedures to bc performed durin�a ro�tine Singulair 960I�1R inspection.Refer to the
Singulair Manuai for a defaited e�planation of eaoh service procedure and ax�O&M fxoubleshooting guide.
CONTROi, CENTBR SERVICE NdT�S/COMME�TTS
�Check operati.on of control cerner . t-� � Yi c-�- � �t�� U't. v t
C7 Adjust time clock whenrequi.red ./�-i�,��tr� � '�-�.��, �1r�-e �,_
❑Ctteck opezation of reasrculation cantrol panei .
FFLUENT RECIRCULATION SYSTEIVI
��eck operation ofrecircuIation pump t'�-�.y��'Cc.3�� �, �,t e,�
�peot rsciroulation well&fitiangs . t_�r_�„L:�i-- � ,
ly TeS'�dperation � �,,,�,� �-�� j��,� �2��
G7 Set recirculation ra#e rate @ min/hr '
��R SERVICE. . ,
Cheek aer�tor c�peration .�(�y�-c�'-�tr�- ��r�-�'.�-v��t_,�_s,�,�.�.��,-
❑Qb.eck aerator power oox�ssulnpfion �c�n '�>�+�.�t�t G�c�
��laeck aerator air delivery
f9��lean stainless steel aspiratar shaft _ 4'3 f S� . � �� f' ��-�1v►�.
6�dr�esn aspira�,nctip
���'ilean fresh air ve.nt in ec�ncrete cover ,
Oc�`Inspect aeration chamber contents
CLA1tIFICA.TION C'�IAMBER SERVICE
❑Remove the Bia-Kinetic system � �- ���t�(�
❑Scrxpe the clarification c�am.her -2r � u.:� �.�-
C]Iuspect the Bio-Static sludge retzun
❑Inspe�t outlet cou.piing
C1 Install a clean�io-Kinetic system
❑Fill B1ue Crystal feed tube(if inst�Ied) '
0 Fill Bio-Neu�ralizer feed tube(if installed)
G RAL SERVICE
�nspect effl.uentpump ehamber �}csn�.�� c,��3,n�r- r�3.�n� .
�`I�s�cteffluentquaIity ra�rt»n�'t �vr�r,� �,� ��r�a;�Erx,�-
�Inspect outiet line ���- �'
C1 Inspect ground wafi�r reiisf point(if installed} i
Q j�spect effiuerit disposal system _������ , !
t�Complete owner service record j
l�Complete healtli deparlm�nt noi�cation .�' > � �,,r,{��.��S :
CI Cpmplete distributor service record � ��� < <{��,��y. �
❑Mait healii�departmez�notification '
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SERVICE 1NSPECTIa� CHECKLIST .�C�� ��t���t�.�
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Address: '�"��.5'���� • ��:, ��. Owner:� '
Operatar. � � tr- Date: t'D�.�c��tG�
This checklist summari�Pe�e service procedures ta be perfarmed during a routine Singulair 960 NR znspection.Refer to the
Sing�ulair Manua�foz a detailed explanation of each service procedura and an O&M troubleshooting guide.
CONTROL CENTER SERVICE NOTESICOM�i��NTS
�Check operation of control center E'✓��� v`� ' v��.-� '�"��
�Adjust time clock when required 4�,`• � �
�Check operafion of recirculation control panel
E�FLUENT RECI1tCULATI�N SY�TEM
Check operation o#'recirculation pwnp �:�ay-rt�3 �,n �t�futn+� 6�
nspect reciroutatian well&fittirigs I�L i..f i���,c1 �t�-rrr�. �,�,�_c��.�to�
Test Operation ���'/`�C�'�_ � �
�7 Set recirculation rate rate Q minThr
RATOR SERV[CE
,
• heck aerator operation �� M�� F�,—c..�(.�
Checic aerator power consumption
` Check aerator air deliverY f�'j' ���. � �`�€��_
Clean stainless steel aspira#or shaft
Clean aspu�ator tip
leaz�fresh air vent in concrete cover
Inspeet aeratson c�amber contents
CI�AR�'ICATION CHAMBER SERVICE
Q Remove the Bio-Kinetic system: _�z,,��+2��. r:� �{v},r�2'2�
Cl Serape the clarification ehamber
❑Inspect the Bio-Static sludge retum
0 Inspect outl.et coupling � � � � .
❑Iustail a cleau�io-Kinetic system � '
❑Filt Blue Crystal feed tvbe(if ins#alled}
❑Fi7I Bio-Neu#ralizer feed.tube(if installed.)
G NERAL SERVICE .
Inspect effluent}�um�chamber � p,�� ��- ��.
eat effluent qua�ity ��� �,�
inspect ou�.et line �
�I Inspect ground water relief poixrt{if installed) �, �' ,��,,,�� .��
�Inspect effluent disposal sys#em {� � � ,
Complete owner service record � Yt�t � �s�r��
�Compaeie haalth depariment notification : � ��
�Complete disirihutor service recard � � . ��;e � �t
❑Mail heai.fih department notiftcation „�t,� 'r����:�
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�II�GIJL ��O 1�.�I'A�'T��T.r�.'TEI� 'I'�.AT'l��'I` SYST�l�I
�ERVZCE IN�PECTION CHECI�,IST �-�.��.--
Address: :� `.��,/''�� �r � ��- own.er:
����� ���
Operator.����� •� �%�,�' �.'�'r""c-' Date: � � � � ��`�l„��
This checklist swnmar�zes the service procedures to be perFazxned during a ro�.�tine Sitngulai�960 NR inspeotion.�tefer to the
Singulair Manual for a detailed explanatian of each service pracedure and an O&M fronbleshooting guide.
CONTROL CFN'I'�.R S�}.tVICE NOTESIC0114n�ENTS
�Check operation of control center �=�•``�'4 5.��-�. �:; '�. `�"�,.,��rc.., �rs-`'`��.� �`"';'�'
C]Adjust time elock when requ�red Q-�'"�.-�'�`��•� ���r t`f-=�-=�`^�,.�
C�,Check operation of recircuiation confrol panel �.:s,`�"�"vi [ � 5�:.�=\ `� ••�, c,�r�� `t��
I�IR EFFLUENT RECIRCULATIaN SYSTEM �
�.Checkoperationofrecirat�lationpump �.�-�`��f'tE- �uF---,� �.:t�,�c.;���, �;•�J���.
�7nspect rec�rcutation we118s fittfngs f,�
�TestOperation �`�-���`� ,�C.. (.?�' �•..�...'"�,v�'�--�
Q Set rec�culation rate rate @ min/hr\�.,`�-• ��`-� �L�::i�ti---�.� � ��a�,,.,•�t
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AERA.T�R BERVICE
�Check aexator operaiion ��'���,` -� •�«�,c.�� Gv� c�r',f<..�.�•�'t.
❑Check aerator power consumption
�Check aerator air delivery "3`�,r"-`,,,.,,, <-,�'`�
C�Clean stainl$ss steel aspira#or shaft �.��, cJ C.�.h..-�.•�
�Clean aspirator f.ip 9 ��` :i��
C�.Clean fresh air vent in concrete c�ver . �?.�•-�:,..:�.` �.�..r.
l7 Inspect aeration chamber contents `
CLARIFICATION CHAMBBR SERVICE
L
emove f�e Bio-Knzetic system `� .�--�-����. ��, � � �`��r�
❑Scrape�he clarification chan�ber �.L.�.,%�--� ,
❑Inspect tlae Bio-Static sludge retum
CI Inspect outlet coupTing �'j F v�"�M•• L `j�*-�--^'-'`.
❑Install a elean Bio-Kinetic system �y-.�J E..�'� c v�, C� �i.:� ��.. '
❑Fill Blue Czystal feed tube(if installed} ��
❑Fill Bzo-Neutratizer feed tube{if instailed}
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GENERAL SERVICE n� -''�fJ
❑Inspect e�E]uent pum�chamber ��_ ��� 5 �..-•.� �� �..�--�...••,n, C����`�°`��
C�lnspect effluent c�uality ���,��,e:`�.
C�Tnspect outiet line `-�.��`�rj -- \��� r i, rz
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❑Inspect ground water relief point(if ins#alled) ,e.. �n..--� ..� c Y �,s-�
D Inspect e�i�ent disposat syst�n '�=��y _ `�,� cti•�--�:; �3-
Ci Complete owner service record �c�,,,_ � r ,
0 Cpmplefis health department not�catiou , �ti,`- :,. -� �1`�� �`�c���
Cl Complete distnbutor service record ti--' `�'S�� � -�� �.�- � -
t�Mail health depar[rnent no 'tYf"ieation �,�� _ L�,�
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' Serial No:03181615:18
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ANALYTICAL REPORT
Lab Number: L1607091
Client: Bennett Environmental Associates
. 1573 Main Street
Brewster, MA 02631
ATfN: David Bennett
Phone: (508)896-1706
ProjectName: PLATT RESIDENCE�
Project Number. BEA15-10827
Report Date: 03/18/16
The original project report/data package is held by Alpha Analyticai.This report/data package is paginated and should be reproduced oniy in its
entirety.Alpha Analytical holds no responsibility for resufts and/or data that are not consistent with the original.
Certifications 8 Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC{666),TX(T104704476),DOD{L2217),USDA(Permit #P-330-11-00240)..
Eigh#Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com
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• Serial No:03181615:18
Project Name: PLATT RESIDENCE Lab Number: L1607091
� Project Number: BEA15-10827 Report Date: 03/18/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis uniess otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Aipha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required qualiiy control corrective
action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboeatory Batch,Sample Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along with any associated usability implications.Soillsediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qual�ers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance criteria tor CAM and RCP methods allow for some
quality control failures to occur and still be within method�mpliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviswed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days .
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters vuill
be disposed after 3 business days from the date the project is completed.
Please contact Client Senrices at 800-6249220 with any questions.
I,the undersigned, a#test under the pains and penalties of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
�.�-����.� Lu ra L Troy
Authorized Signature: U�
Title: Technical Director/Representative Date: 03/18/16
Page 3 of 15 ��--_ .�-•
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Serial No:03181615:18 -
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Page 4 of 15
• Seriai No:03181615:18
Project Name: PLATT RESIDENCE . Lab Number: L1607091
� Project Number: BEA15-10827 Report Date: 03/18/16
SAMPLE RESULTS
Lab ID: L1607091-01 Date Collected: 03l10/16 11:15
CII2fit ID: EFFLUENT Date Received: 03/11/16
S3111(]I@ LOC8tI0Il: SOUTH YARMOUTH,Ma Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyaed MetMod qnalyst
General Chemistry-Westborou.gh Lab
Solids,Total Suspended 15. mg/l 5.0 NA 1 - 03/17/16 03:12 30,2b40D RT
Nitrogen,Nitrite ND mg/I 0.050 — 1 - 03/11/16 21:40 44,3532 MR
------------------------------------------...._._-- ----—---------------------._..-----�--...-----------------------------_.----• --------...------
Nitrogen,Nitrate ND mgll 0.10 — 1 . - 03l11/1621:40 44,353.2 MR
Nitrogen,Total Kjeldahl 49.4 mg/I 3.00 — 10 03/13/16 20:00 03/16/16 22:41 30,4500N-C AT
BOD,5 day 38. mg/I 2.0 NA 1 03/12/16 04:55 03/16/16 23:10 30,5210B TA
v;.x . e�.
Page 5 of 15
r
Serial No:03181615:18 �
Project Name: PLATT RESIDENCE Lab Nurriber: L1607091
Project Number: BEA15-10827 Report Date: 03/18/16 � �
Method Blank Analysis �
Batch Quality Control '�
�
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i
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Cherriistry=Westborough Lab for sample(s): 01 Batch: WG873113-1 '
Nitrogen,Nitrate ND mg/I 0.10 — 1 - 03/11/16 2130 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873114-1
Nitrogen,Nitrite ND mgll 0.050 -- 1 - 03/11/16 21:32 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873206-1
BOD,5 day ND mgA 2.0 NA 1 03112/16 04:55 03/16/16 23:10 30,5210B TA
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873440-1 _
Nitrogen,Total Kjeldahl ND mg/I 0.300 -- 1 03/13/16 20:00 03/16/16 22:31 30,4500N-C AT
General Chemistry-Westborough Lab for sample(s); 01 Batch_ WG874594-1
Sotids,Total Suspended ND mg/I 5.0 NA 1 - 03/17/16 03:12 30,2540D RT
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Serial No:03181615:18 =
Project Name: PLATT RESIDENCE Lab Number: L1607091
Project Number: BEA15-10827 Report Date: 03/18116 ' '
Sample Receipt and Container Information '
Were project specific reporting limits specified? YES �
Cooler Information Custody Seal ',
Cooler
A Absent '
Container Information Temp
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*) '
L1607091-01A Piastic 250m1 H2SO4 preserved A <2 3.5 Y Absent TKN-4500(28)
L1607091-01B Plastic 950m1 unpreserved A 7 3.5 Y Absent NO2-353(2),BOD-5210(2),NO3-
353(2)
L1607091-01C Plastic 950m1 unpreserved A 7 3.5 Y Absent TSS-2540(7)
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*Values in parentheses indicate holding time in days �a,� .��L
Page 10 of 15
� Serial No:03181615:18
Project Name: PLATT RESIDENCE Lab Number: L1607091
° Project Number: BEA15-10827 Report Date: 03/18/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:Tlris value represents the level to which taz•get analyte concenhgtions are reported as estimated
values,when those taz�get analyte concentrations aze quantified below the reporting 1'vnit(RL).The EDL includes any
adjustments from dilutions,concentrations or moisture conient,where applicable.The use of EDLs is specific to the analysis of
PAHs using Solid-Phase Microextraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratory Conh�ol Sample:A sample matrix,free from the analytes of interest,spiked with verified lmown amounts of anatytes
or a material containino known and verified amounts of analytes.
LCSD -Laboiatory Control Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes
or a material containing known and verified amounts of analytes.
MDL -Method Detection Limit:This value represents the level to which tazget analyte concentrations a�•e reported as estimated values,
when those target analyte concentrations aze quanfified below the reporting limit(RL).The MDL includes any adjustments from
dilutions,concentra6ons or moisture content,where applicable.
MS -Mahix Spike Sample:A sample prepared by adding a lmown mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concentration is available.
MSD -Mahvc Spike Sample Duplicate:Refer to MS.
NA -NotApplicable.
NC -Not Calculated: Texm is utilized when one or more of the results utilized in the calculation are non-detect at the pazameter's
reporfing unit.
NI -NotIgnitable.
NP -Non-Plastia Teim is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limi� The value at wluch an insirument can accurately measure an analyte at a specific concentration.The RL
includes any adjustments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results from mahix and/or matrix spike duplicates aze primarily designed to assess the precision
of analytical res�ilts in a given mahix and are expressed as relative percent difference(RPD). Values wlrich aze less tUan five
times the reporting limit for any individual parameter aze evaluated by utilizing the absolute difference between the values;
although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a laiown or ceatified value that is of the sazne or similar matrix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
1TC -Teatatively Identified Compound:A compound that has been identified to be present and is not part of tl�e target compound list
(TCL)for ihe method and/or program.Ali TICs are qualitatively identified and reported as estimated concentrations.
Foofnotes
1 -The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original
method
Terms
Total:With respect to Organic analyses,a Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from wluch the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Qua/�ers
� A -Spectra identified as"Aldol Condensation Product". '
B -The analyte was detected above the repmting limit in the associated method blank.Flag only applies to associated field samples that
have deteciable concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox)
the concentration found in the blank.For DOD-related projects,fla�only applies to associated field s�ples that have detectable
concenh�ations of the analyte at less than ten times(I Ox)the concenhation found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab contazninants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated feld sampies that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excludina Air),flag only applies to associated field samples that have detectable .
concentrations of the analyte,wlrich was detected above the reporting limit in the assceiated method blank or above five times the
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
Report Format: Data Usability Report '
��;: he�
Page 11 of 15
Serial No:03181615:18 f
Project Name: PLATT RESIDENCE Lab Number: L1607091
Project Number: BEA15-10827 Report Date: 03/18/16 ' �
E
Data Qualifiers
C -Co-elution:The tazget analyte co-elutes with a lmown lab standard(i.e.surrogate,intemal standards,etc.)for co-ex�acted i
analyses. �
, D •Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations ;
of the analyte. _ `
E -Concenhation of analyte exceeds the range of the calibration cuxve and/or linear range of the inshvment
G -The concentration may be biased high due to mahix interferences(i.e,co-elution)with non-tazget compound(s).The result should
be considered estimated.
H -The analysis of pH was peiformed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. • .
I -The lower value for the two columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for tlus analyte.
N7 -Presumptive evidence of c4mpound.This represents an estimated concenhation for Tentatively Identified Compounds(TICs),where ,
the identificarion is based on a mass spectral library search.
P -The RPD between the results for the two columns exceeds the mefliod-specified criteiia.
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration
Standard exceedences aze also qualified on all associated sample results. Note:llris flag is not applicable for matrix spike recoveries
when the saznple concentration is greates than 4x the spike added or for batch duplicate RPD wben the sample concentrafions are less
than Sx the RL.(Metals only.)
R -Analytical results aze from saznple re-analysis.
RE -Aualytical results are from sample re-eashacrion.
S -Analytical results aze from modified screening analysis.
J •Estimated value.This represents an estimated concentration for Tentafively Identified Compounds(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
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Repor!Format: Data Usability Report
�3, ��`
Page 12 of 15
` Serial No:03181615:18
Project Name: PLATT REStDENCE Lab Number: L1607091
Project Number: BEA15-10827 Report Date: 03/18/16
REFERENCES
30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-
WPCF. 18th Edition. 1992. .
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100,August 1993.
LIMITATION OF LIABILITIES
Alpha Analytical performs senrices with reasonable care and diligence normal to the analytical testing
laboraiory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analy#ical be held liable
for any incidentaf, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. '
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling,
containers,sampling procedures, holding time and splitting of samples in the field. '
-�.: e�.
Page 13 of 15
f
Serial No:03181615:18 '
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 6
Department: Quality Assurance Published Date:2/3/2016 10:23:10 AM
Title• Certificate/Approval Proqram Summarv Paqe 1 of 1 .
Certification information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA524.2:1,2-Dibromo-3-chloropropane,1,2-Dibromoethane,m/p-xylene,o-xylene
EPA 624:2-Butanone(MEK),1,4-Dioxane,tert-Amyimethyl Ether,tert-Butyl Alcohol,m/p-xylene,o-xylene
EPA 625: Aniline,Benzoic Acid,Benryl Alcohol,4-Chioroaniline,3-Methylphenol,4-Methylphenol.
EPA 1010A: NPW: Ignitability
EPA 6010C: NPW:Strontium;SCM: Strontium
EPA8151A: NPW:2,4-DB,Dicamba,Dichloroprop,MCPA,MCPP;SCM: 2,4-DB,Dichloroprop,MCPA,MCPP �
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene,Isopropanol;SCM:lodomethane(methyl iodide),Methyl methacrylate
(soil);1,2,4,5-Tetramethylbenzene;4-Ethyftoluene.
EPA8270D: NPW:Pentachloronitrobenzene,1-Methylnaphthalene,Dimethylnaphthalene,l,4-Diphenylhydrazine;SCM:Pentachloronitrobenzene,1-
Methylnaphthalene,.Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 9010: NPW: Amenable Cyanide Distillation,Total Cyanide Distillation
EPA9038: NPW: Sulfate
EPA 9050A: NPW:Specific Conductance '
EPA 9056:NPW:Chioride,Nitrate,Sulfate
EPA 9065: NPW:Phenols
EPA 9251: NPW:Chloride
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved O�cygen;SCM:Totai Phosphorus,TKN,NO2,NO3.
SM5390C:DW:Dissolved Organic Carbon
Mansfield Facility '
EPA 8270D:NPW: Biphenyl;SCM: Biphenyl,Caprolactam
EPA 8270D-SfM Isotope Dilution: SCM: 1,4-Dioxane
SM 2540D: TSS
SM2540G: SCM:Percent Solids
EPA 1631E:SCM: Mercury '
EPA 7474: SCM: Mercury i
EPA8081B:NPW and SCM:Mirex,Hexachlorobenzene.
EPA8082A:NPW: PCB:1,5,31,87,101,110,141,151,1b3,180,183,187. E
EPA 8270-SIM: NPW and SCM: Alkylated PAHs. '
i
EPATO-75:Halothane,2,4,4-Trimethyi-2-pentene,2,4,4Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methyfthiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene,n- k
Butylbenzene,n-Propylbenzene,sec-Butylbenzene,tert-Butylbenzene. �
Biological Tissue Matrhc: 8270D-SIM;30506;3051A;7471B;8081B;8082A;6020A:Lead;8270D:bis(2-ethylhexyl)phthalate,Butylbenrylphfhalate, !
Diethyl phthalate,Dimethyl phthalate,Di-n-butyl phthalate,Di-n-ociyi phthalate,Fluoranthene,Pentachlorophenol. �
The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: I
Drinking Water
EPA200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA30U.7:Ba,Be,Ca,Cd,Cr,Cu,Na;EPA245.1:Mercury;
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:NiVate-N,Nifite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1, �;
SM2130B,SM4500CI-D,SM2320B,SM2540C,SAA4500H-B
EPA332:Perchlorate.
Microbiology:SM9215B;SM9223-P/A,SM9223B-Colilert-QT,Enterolert-QT.
Non-Pota6le Water
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;.
EPA200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn;
EPA 245,1,SM4500H,6,EPA 120.1,SM2510B,SM2540C,SM2340B,SM23206;SM4500CL-E,SM4500E-BC,SM426C,SM4500NH3-BH,EPA
350.1:Ammonia-N,LACHAT 10-107-06-1-B:Ammonia-N,SM4500NO3-F,
EPA 353.2:Nitrate-N,SM4500NH3-BC-NES,EPA 351.1,SM4500P-E,SM4500P-B,E,SM5220D,EPA 410.4,SM5210B,SM5310C,SM4500CLA,
EPA 1664,SM14 510AC,EPA420.1,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-6HC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan I,Endosulfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs !
EPA 625:SVOC(Acid/Base/Neutral Extractabies),EPA 600/4-81-045:PCB-Oil.
Microbioiogy.SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: 08-113
Page 14 of 15
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• Serial No:06161621:24
Project Name: PLATf RESIDENCE Lab Number: L1617848
` Project Number: BEA15-10827 Report Date: 06/16/16
Case Narrative
, The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless othervvise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even"rf only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corcective
action and'rf both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sampie Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
in reference to questions H(CAM)or 4(RCP)when"NO"is checked,the perFormance criteria for CAM and RCP methods allow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
ftnm the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters wi►1
be disposed after 3 business days from the date the project is completed. '
Please contact Client Services at 800-6249220 with any questions.
I,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
Authorized Signature:
G;��� Cristin Walker � '
Title: Technical Director/Representative Date: 06116/16
Page 3 of 15 S
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Page 4 of 15
. Serial No:06161621:24
Project Name: PLATT RESIDENCE Lab Number: L1617848
' Project Number: BEA15-10827 Report Date: 06/16/16
SAMPLE RESULTS
Lab ID: L1617848-01 Date Collected: 06/10/16 09:30
Cli0llt 1D: EFFLUENT Date Received: 06/10/16
S3CTipI@ LOCat1011: SOUTH YARMOUTH,Ma Field Prep: Not Specifled
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method qnalyst
_ _.
General Chemistry-Westborough Lab
_ , _ _
Solids,Total Suspended 16. mgfl 5.0 NA 1 - 06/13/16 16:35 121,2540D SG
-------��.�----...._—.__._.._...------_..__. _�_._._.___.....-----._._.._._._...-----..._..--....�__..__...__...---�-�-------._..._._.....�____-_-------._.._..-----...---..._...----
Nitragen,Nitrite 5.3 mg/I 0.25 — 5 - 06/10/16 22:00 44,353.2 MR
_.____.—____ __.._....--------- ---------- -------.._._..__...__.._.._..._._.....------------...---.....----._...— -----------..—..----...____..---._..
Nitrogen,Nitrate 20. mgil 0.50 — 5 - 06/10/16 22:00 44,353.2 MR
�.--------------------------------____--------�..—.�....._.�---- ------ ----.__..---.�._
Nitrogen,Total Kjeldahl 2.09 mg/I 1.50 -- 5 06/13116 20:00 O6/15/16 22:15 121,4500N-C AT
-�--------_._._.—__`.__.....__._......._..____---------..____.._— ---------__-----__�_._____..._....._......-----.._..___._...___------------_....-----------._.._._.....---
60D,5 day 28. mgA 2.0 NA 1 06/11/16 04:15 06/15I16 23:10 127,52106 TA
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Page 5 of 15 '
F
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Serial No:06161621:24 .
Project Name: PLATT RESIDENCE Lab Number: L1617848 '
Project Number: BEA15-10827 Report Date: 06/16/16 -
Method Blank Analysis �
Batch Quality Gontrol �
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_ ;
Dilution Date Date Analytical
Parameter Resuit Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Cherrii,stry-Westborough Lab for sample(s): 01 Batch: WG902832-1
Nitrogen,Nitrate ND mg/I 0.10 -- 1 - O6/10/1620:58 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG902833-1
NiYrogen,Nifite ND mg/1 0.050 -- 1 - 06/10/16 21:00 44,353.2 MR '
Genera]Chemistry-Westborough Lab for sample(s): 01 Batch: WG902977-1
BOD,5day ND mg/l 2.0 NA 1 06/11/1604:15 06/15/1623:10 121,5210B TA
General Chemistry-Westborowgh Lab for sample(s): 01 Batch: WG903365-1
Solids,Total Suspended ND mg/I 5.0 NA 1 - 06113/1616:35 121,2540D SG '
General Ghemistry-Westborough Lab for sample(s): 01 Batch: WG903494-1 ',
Nitrogen,Total Kjeldahl ND mg/I 0.300 — 1 06/13/16 20:00 06/15/16 22:07 121,4500N-C AT '
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Serial No:06161621:24 '
Project Name: PLATT RESIDENCE Lab Number: L1617848
Project Number: BEA15-10827 Report Date: 06/16/16 '
Sample Receipt and Container Information `
C
Were project specific reporting limits specified? YES �
Gooler Information Custody Seal
Cooler
A Absent
Container Information Temp
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1617848-01A Plastic 250m1 H2SO4 preserved A <2 3.3 Y Absent TKN-4500(28)
L1617848-01 B Plastic 950m1 unpresenred A 7 3.3 Y Absent NO2-353(2),BOD-5210(2),NO3-
353(2)
L161784&01C Plastic 950m1 unpreserved A 7 3.3 Y Absent TSS-2540(7)
�
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*Values in parentheses indicate holding time in days ,���� r.�L f
Page 10 of 15
• Serial No:06161621:24
Project Name: PLATT RESIDENCE Lab Number: L1617848
� Project Number: BEA15-10827 Report Date: 06/16/16
GLOSSARY
Acronyms
EDL -Estimated Detection L'unit:Tlus value reptesents the level to wluch target analyte concentrations are reported as estimated
values,when those tazget analyte concentrations aze quantified below the reporting limit(RL).The EDL includes any
adjusiments from dilutions,concentrations ox moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Micrce�ctraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified lmown amounts of
analytes or a material containing known and verified amounts of analytes.
LCSD -Laboratory Contrnl Sample Duplicate:Refer to I,CS.
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified Imown amounts of
analytes or a material containing known and verified amounfs of analytes.
1�IDL -Method Detection Limit:Tlus value represents the level to which target analyte concentrations are reported as estimated
values,when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.
MS -Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample far
which an independent estimate of target analyte concentration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reporting unit
NDPA/DPA -N Nitrosodiphenylamine/Diphenylamine.
NI -Not Ignitable.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit: The value at wluch an instrument can accurately measure an analyte at a specific concentration.The RL
inclucles any adjusiments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results from matrix and/or mahix spike duplicates aze primarily designed to assess the
precision of analytical results in a�ven matrix and are expressed as relative percent difference(RPD). Values wlrich are less
than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the
values;although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a lmown or certifieti value that is of the same or similaz matrix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TTC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound
list(TCI.)for the method and/or program.All TICs are qualitatively identified and reported as estimated concenttations.
Foofnotes
1 -The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the
original method
Terms
Total:VJith respect to Organic analyses,a'Total'result is defined as the sL*+�+nption of resutts for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and the analytical reference meihod.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Qua/ifiers
A -Spech-a identified as"Aldol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times(lOx)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox)
the concentration found in the blank.For DOD-related pmjects,flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times(lOx)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting]imit for common lab contaminants)in the associated method blank.For N7-
Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,wluch was detected above the reporting limit in the associated method blank or above five times the
Report Format: Data Usability Report
��-. .��,,.
Page 11 of 15
f
�
Serial No:06161621:24 =
Project Name: PLATT RESIDENCE Lab Number: L1617848 I,
Project Number: BEA15-10827 Report Date: 06/16/16 �
Dafa Qualifiers �
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
C -Co-elution:The target analyte co-elutes with a known lab standard(i.e.surrogate,intemal standazds,etc,)for co-extracted
analyses.
D -Concentrarion of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations �
of the analyte. �
E -Concentration of analyte exceeds the range of the calibration curve and/or lineaz range of the instrument
G -The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should
be considered estimated.
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
I -The lower value for the tcvo columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for this analyte.
NJ -Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral librazy search.
P -The RPD between the results for the two columns exceeds the method-specified criteria.
Q -The qualiry control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than Sx the RL.(Metals only.)
R -Analytical results are from sample re-analysis.
RE -Analytical results are from sample re�xtraction.
S -Analytical results are from modified screening analysis.
J -Estimated value.Tlus represents an estimated concentration for Tentatively Identified Compounds(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
Report Format: Data Usability Report
�F'A•
Page 12 of 15 �
I
�
. Serial No:06161621:24
Project Name: PLATf RESIDENCE Lab Number: L1617848
� Project Number: BEA15-10827 Report Date: 06/16/16
REFERENCES
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
121 Standard Methods for the Examination of Wafer and Wastewater.APHA-AWWA-WEF.
Standard Methods Oniine.
LIMITATION OF LIABILITIES ,
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers,sampling procedures, holding time and splitting of samples in the field.
,�
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Page 13 of 15
Serial No:06161621:24 ,
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 6
Department: Quality Assurance Published Date: 2/3/2016 10:23:10 AM . '
Title• Certificate/Approvaf Proqram Summarv Paqe 1 of 1
Gertification Information �
The following analytes are not included in our Primary NELAP Scope of Accreditation:
_ . _ _ _ . _. _ _ _ _ __ __ _ . ._ _ ;
Westborough Facility
EPA524.2; 1,2-Dibromo-3-chloropropane,1,2-Dibromoethane,m/p-xylene,o-xylene ;
EPA 624:2-Butanone(MEK),1,4-Dioxane,tert-Amylmethyl Ether,tert-Butyl Alcohol,m/p-xylene,o-xylene
EPA 625: Aniline,Benzoic Acid,Benzyl Alcohol,4-Chloroaniline,3-Methylphenol,4-Methylphenol.
EPA 1010A: NPW: Ignitability
EPA 6010C: NPW:Strontium;SCM: Strantium
EPA 8151A: NPW:2,4-DB,Dicamba,Dichloroprop,MCPA,MCPP;SCM: 2,4-DB,Dichloroprop,MCPA,MCPP
EPA 8260C:NPW:1,2,4;5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene,Isopropanol;SCM:lodomethane(methyl iodide),Methyl methacrylate '
(soiQ;1,2,4,5-Tetramethylbenzene;4-Ethyltoluene.
EPA8270D: NPW:Pentachloronitrobenzene,1-Methylnaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Pentachloronitrobenzene,1-
Methylnaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine. ,
EPA 9U10: NPW: Amenable Cyanide Distillation,Total Cyanide Distillation
EPA 9038: NPW: Sulfate
EPA 9050A: NPW:Specific Conductance
EPA 9056:NPW:Chloride,Nitrate,Sulfate
EPA 9065: NPW:Phenols
EPA 9257: NPW:Chloride
SM3500: NPW:Ferrous Iron '
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved Organic Carbon
Mansfield Facility
EPA 8270D:NPW: Biphenyl;SCM: Biphenyl,Caprolactam
EPA8270DSIM Isotope Dilution: SCM: 1,4-Dioxane
SM 2540D: TSS
SM2540G: SCM:Percent Solids
EPA1631E:SCM: Mercury
EPA 7474; SCM: Mercury
EPA8081B:NPW and SCM:Mirex,Hexachlorobenzene.
EPA 8082A:NPW: PCB:1,5,31,87,101,110,441,151,153,180,183, 187.
EPA 8270�SIM: NPW and SCM: Alkylated PAHs.
EPA TO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4-Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methyfthiophene,2-Ethylthiophene, 1,2,3-Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene,n-
Butylbenzene,n-Propylbenzene,sec-Butylbenzene,tert-Butylbenzene.
Biological Tissue Matrix: 8270D-S/M;30508;3051A;7471B;80818;8082A;6020A:Lead;8270D:bis(2-ethylhexyl)phthalate,Butylbenzylphthalate,
Diethyl phthalate,Dimethyl phthalate,Di-n-butyl phthalate,Di-n-octyl phthalate,Fluoranthene,Pentachlorophenol.
The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility:
Drinkfng Water '
EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7:Ba,Be,Ca,Cd,Cr,Cu,Na;EPA 245.1:Mercury; ;
EPA 300.0:Nitrate-N,Fluoride,5ulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 980.1, I
SM2130B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate.
Microbiology:SM9215B;SM9223-P/A,SM9223B-Colilert-QT,Enterolert-QT.
Non-Pota6le Water
EPA200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;
EPA200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn;
EPA 245.1,SM4500H,B,EPA 120.1,SM2510B,SM2540C,SM2340B,SM2320B,SM4500CL-E,SM4500E-BC,SM426C,SM4500NH3-BH,EPA
350.1:Ammonia-N,LACHAT 10-107-06-1-B:Ammonia-N,SM4500NO3-F,
EPA 353.2:Nitrate-N,SM4500NH3-BC-NES,EPA 351,1,SM4500P-E,SM4500P-B,E,SM522DD,EPA 410.4,SM5210B,SM5310C,SM4500CL-D,
EPA 1664,SM14 590AC,EPA 420,7,SM4500-CN-CE,SM25400.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endasulfan I,Endosulfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC{AcidBase/Neutral E�dractables),EPA 600/4-81-045:PCB-Oil.
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: 08-113 'i
Page 14 of 15 '
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.. �
I
David Bennett
.
From: Kevin Aguiar <KAguiar@BETA-Inc.com>
Sent: Thursday,June 23, 2016 9:28 AM '
To: David Bennett
Subject: Proposal �
Morning Dave,
Are you able to forward over a proposal for the Westport project?Architect has a meeting with client tomorrow
and were hoping to have a complete fee ready.
Please advise.
Sent fi�om my T�erizon Wi�eless 4G LTE DROID
Confidentiality Notice: '
This emaii message(and any attachments)contains information trom BETA Group,Inc.
that is confidential.If you are not the intended recipient(s),you may not disclose,
copy,distribute,rely upon,or use its contents.Please reply to the sender
immediately and delete this message.Thank you for your cooperation.
i
�
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; Serial No:08051620:42
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ANALYTICAL REPORT
Lab Number: L1624103
Ciient: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
ATTN: David Bennett
Phone: � (508)896-1706 ,
Project Name: PLATf RESIDENCE �'
Project Number: BEA15-10827 '
Report Date: 08/05/16
The original project reporUdata package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its '
entirety:Alpha Analytical holds no responsibility for results and/or data that are not consisterrt with the original.
Gertifications&Approvals: MA(M-MA086j,NY (11148),CT(PH-057d),NH(2003),NJ NELAP{MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com ;
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, Serial_No:08051620:42
Project Name: PLATT RESIDENCE Lab Number: L1624103
! Project Number: BEA'15-10827 Report Date: 08/05/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipf,Container Information,and the Chain of Custody are located at the back of the report.
Resuits contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requiremenfs for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample spec�c Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end ofi the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective
action and'rf both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samp�es for each element
are noted in the grey shaded header line of each data tabie.Any Laboratory Batch,Sampie Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can he reviewed along with any associated usability implications,Soil/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the perFormance criteria for CAM and RCP methods allow for some
quality control failures to occur and stiil be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical ',
Standards requested on the Chain of Custody. '
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hoid samples(with the exception of Air canisters)free of charge for 21 calendar days i
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters wiil
be disposed after 3 business days from the date the project is completed.
Please contact Client Services at 800-624-9220 with any questions. ,
I,the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This cerfificate of analysis is nbt
complete unless this page accompanies any and all pages of this report. ;
�'� A,mita IVaik
Authorized Signature:
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Title: Technical Director/Representative Date: 08/05/16 �
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Page 4 of 15
� Serial No:08051620:42
Project Name: PLATT RESIDENCE Lab Number: L1624103
' Project Number: BEA15-10827 Report Date: 08/05/16
SAMPLE RESULTS
Lab ID: L1624103-01 Date Collected: 08/02I16 09:15
Ciient ID: EFF�uENT Date Received: 08/03/16
S3t71p1@ LOCBtIOn: SOUTH YARMOUTH,Ma Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab
Nitrogen,Nitrite 3.4 mgll 0.050 — 1 - 08/03/1621:19 44,353.2 MR
----- ------...----.�.__......_--- _._--- --------._------------------- ------ ----
Nitrogen,Nitrate 3.9 mg/I 0.10 — 1 - 08/03/1621:19 44,353.2 MR
_....-- ___.._._....._ .... ..._. _....__..._..__.......------- ----- ---- -----._....--------- -._.... ...._. .---._..---.. ... __ . ._....__ ...._....__—--_.........,._...._ ....._.._ .---....._..._._._._.._ ....
N itrogen,Total Kjeldahl 16.7 mg/I 0.600 — 2 08/03/16 20:30 08/04/16 20:37 129,4500N-C AT
,t� :
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Page5of15
�
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Serial No:08051620:42 •
Project Name: PLATT RESIDENCE Lab Number: L1624103 '
Project Number: BEA15-10827 Report Date: 08/05/16 �
�
Method Blank Analysis ;
Batch Quality Control
;
;
_ . _ _ �
Dilution Date Date Analyticai ��!
Parameter Result Qualifier Units RL MDL Factor Prepared Anatyzed Method Analyst
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG919733-1 -
Nitrogen,Nitrafe ND mg/l 0.10 -- 1 - 08/03/16 21:08 44,353.2 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG919735-1
Nitrogen,Nitrite ND mg/I 0.050 — 1 - 08/03/16 21:11 44,3532 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG919747-1
Nitrogen,Total Kjeldahl ND mg/I 0.300 -- 1 OSl03/16 20:30 08l04/16 20:33 121,4500N-C AT
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Page 6 of 15
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Serial No:08051620:42 -
Project Name: PLATT RESIDENCE Lab Number: L1624103
Project Number: BEA15-10827 Report Date: 08/05/16 '
Sample Receipt and Container Information
Were project specific reporting limits specified? YES i
Gooler Information -Custody Seal - ;
Cooler ,�
A Absent `
�
;
(
C
Container Information Temp
Container ID Container Type Cooler pH deg C pres Seal Analysis(*)
L1624103-01 A Plastic 250m1 H2SO4 preserved A <2 22 Y Absent TKN-4500(28)
L1624103-01B Plastic 120m1 unpreserved A 7 2.2 Y Absent NO2-353(2),NO3-353(2)
I
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�� *Values in parentheses indicate holding time in days ,'�[�i�t;�
�i Page 10 of 15
l
• Serial No:08051620:42
Project Name: PLATT RESIDENCE Lab Number: L1624103
' Project Number: BEA15-10827 Report Date: 08/05/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:Tlus value represents the level to which target analyte concentrations are reported as estimated
values,when those target analyte concenhations are quantified below the reporting limit(RL).The EDL includes any
' adjustments&om dilutions,concenirations or moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microextraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratoiy Control Saznple:A sample mahix,free from the analytes of interest,spiked with verified Irnown amounts of
analytes or a material containing known and verified amounts of analytes.
LCSD -I,aboratory Control Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample mah•ix,free from the analytes of interest,spiked with verified l�own amounts of
analytes or a material containing known and verified amounts of analytes.
MDL -Method Detection Limit:Tlus value represents the level to which target analyte concentrations are reported as estimated
values,when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any
adjustments&om dilutions,concentrations or moisture content,where applicable.
MS . -Matrix Spike Sample:A sample prepazed by adding a known mass of tazget analyte to a specified amount of matrix sample for
whicl�an independent estimate of target analyte concenhation is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calcularion are non-detect at the parameter's
reporting unit
NDPA/DPA -N Nitrosodiphenylamine/Diphenylamine.
N! -Not Ignitable. �
NP -Non-Plastic:Teim is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit: Tlie value at wlrich an instrument can accurately measure an analyte at a specific concentration.The RL
includes any adjustments from dilutions,concentrations ar moishu•e content,wliere applicable.
RPD -Relarive Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less
than five times the reportino]imit for any individual paruneter are evaluated by utilizing the absolute difference between the
values;although the RPD value will be provided in the report.
SRM -Standard Reference Materiat:A reference sample of a laiown or certified value that is of the same or similar matrix as the ',
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TIC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound �
list(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations. ;
Footnotes '
1 -The reference for this analyte should be considered modified since tlris analyte is absent from the target analyte list of the
original method.
Terms
Total:VJith respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors.If a'TotaP
result is requested,the results of its individual components will also be reported.This is applicable to"Total'results for methods 8260,8081
and 8082. �
Analytical Method:Both t1�e document from which the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addeudum.
Data Qual�ers
A -Specha iden6fied as"Aldol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times(lOx)fl�e concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(l Ox)
the concentration found in the blank For DOD-related projects,flag only applies to associated field saznples that have detectable
concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common]ab contaminants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated field samples that have detectable concentrations of ffie analyte above the k
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the �
�
Report Format. Data Usability Report
I
I
�._�tiJ�.. �
Page 11 of 15
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Serial No:08051620:42 �
Project Name: PLATT RESIDENCE Lab I�umber: L1624103
Project Number: BEA15-10827 Report Date: 08/05/16 �
Data Qualifiers
reporting limit for common lab contaminanis(Phflialates,Acetone,Methylene Chloride,2-Butanone). ,
C -Co-elution:The tazget analyte co-elutes wiNi a known lab sfandard(i.e.surrogate,intemal standards,etc.)for co-exh�acted '
analyses. �
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples tUat have detectable concentrations �
of the analyte. �
E -Concentration of analyte exceeds the range of the calibration curve and/or lineaz range of the instrument.
G -The concenh-ation may be biased hi�due to matrix intei�erences(i.e,co-elution)with non-tazget compound(s).The result should !
be considered estimated. �
H -The analysis of pH was performed beyond the regulatory-required holding tune of 15 minutes from the tune of sample collection.
i
I -The lower value for the two columns has been reported due to obvious interference. y
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for tius analyte.
NJ -Presumptive evidence of compound.This represents an estunated concentration for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral library seazch.
P -The RPD between the results for the two columns exceeds the method-specified criteria.
Q -The quality control sample exceeds the assoczated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration
Standard exceedences aze also qualified on all associated sample results. Note:Tlus flag is not applicable for mah•ix spike recoveries
when the sample concenhation is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations aze less
than Sx the RL.(Metals only.)
R -Analytical iesults are fiom sample re-analysis.
RE -Analytical results aze from sample re-extraction.
S -Analytical results are from modified screening analysis.
J •Estimated value.This represenis an esdmated concentration for Tentatively Identified Compounds(TTCs). �
ND -Not detected at the reporting limit(RL)for the sample.
Report Format. Data Usability Report
;�kR
_ ��a �,.�
Page 12 ofi 15
�
� Serial No:08051620:42
Project Name: PLATT RESIDENCE Lab Number: L1624103
r Project Number: BEA15-10827 Report Date: 08/05/16
REFERENCES
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100,August 1993.
121 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WEF.
Standard Methods Online.
LIMITATION OF LIABILITIES
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
�,
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Page 13 of 15
�
5erial No:08051620:42 •
Alpha Analytical, Inc. ID No.:'17873
Facility: Company-wide Revision 7
Department: Quality Assurance Pubiished Date: 8/5/2016 11:25:56 AM '
Title:Certificate/Approval Program SummarV Paqe 1 of 1
Certifi�ation Information
F
�
j
The following analytes are not included in our Primary NELAP Scope of Accreditation: !
_..._ _ _.. __ _ _._ . . _ _ _ . ;
Westborough Facility _ ',.
EPA 624:m/p-xylene,o-xylene
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene;SCM:lodomethane(methyl iodide),Methyl methacrylate,1,2,4,5- '
Tetramethylbenzene;4-Ethyltoluene. '
EPA8270D: NPW:Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 300: DW:Bromide
EPA 6860: NPW and SCM:Perchlorate
EPA901U: NPW and SGM: Amenable Cyanide Distillation '
EPA 9012B: NPW:Total Cyanide
EPA 9050A: NPW:Specific Conductance �
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Totai Phosphorus,TKN,NO2,NO3.
SM53'IOC:DW:Dissolved Organic Carbon
Mansfield Facility
SM 2540D: TSS
EPA 3005A NPW
EPA 8082A:NPW: PCB:1,5,31,87,101,110, 141,151,153, 180,183,187.
EPATO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene,2-Ethylthiophene, 1,2,3-Trimethylbenzene,Indan,indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene.
Biological Tissue Matrix: EPA 3a50B
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1,
SM2130B,SM4500C1-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate;EPA 524.2: THMs and VOCs;EPA 504.1:EDB,DBCP.
Microbiology:SM9215B;SM9223-P/A,SM9223B-Colilert-QT,SM9222D.
Non-Potable Water
SM4500H,B,EPA 120.1,SM25106,SM2540C,SM2320B,SM4500CL-E,SM4500E-BC,SM4500NH3-BH,EPA 350.1:Ammonia-N,LACHAT 10-107-
06-1-B:Ammonia-N,SM4500NO3-F,EPA 353,2:Nitrate-N,EPA 351.1,SM4500P-E,SM4500P-B,E,SM4500SO4-E,SM5220D,EPA 410.4,
SM5210B,SM5310C,SM4500CL-D,EPA 1664,EPA420.1,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,aipha-BHC,beta-BHC,gamma-BHC,detta-BHC,Dieidrin,DDD,DDE,DDT,Endasulfan I,Endosulfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC(AcidBase/Neutral Extractables),EPA B00/4-81-045:PCB-OiL
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
Mansfield Facility: '
Drinking Water
EPA 200.7:Ba,Be,Cd,Cr,Cu,Ni,Na,Ca.EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TL.EPA 245.7 Hg.
Non-Pota6le Water
EPA 200J:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,TL,Ti,V,Zn.
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TL,Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: 08-113
Page 14 of 15
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ANALYTICAL REPORT
Lab Number: L1627750
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
A7TN: David Bennett
Phone: (508)896-'1706
Projeot Name: PLATT RESIDENCE
Project Number: BEA15-10827
Report Date: 09/11/16
The originai project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its
entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T'104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Waikup Drive, Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com ,
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� Serial No:09111619:53
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Project Name: PLATT RESIDENCE Lab Number: L1627750
Project Number: BEA15-10827 Report Date: 09/11/16
Case Narrative
The sampies were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the sampies submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter:Tentatively Identified Compounds
(flCs),'rf requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective
action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sampie Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along vvith any associated usability implications.Soil/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of ail data qualifiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance criteria for CAM and RCP methods allow for some
quality controi failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Aipha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Aipha to continue to hoid the samples.Air canisters will
be disposed after 3 business days from the date the project is completed.
Please contact Client Services at 800-624-9220 with any questions.
I,the undersigned, attest under the pains and penalties of perjury fhat,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not '
complete unless this page accompanies any and all pages of this report.
Authorized Si nature: ����� Kelly Stenstrom j
9
Title: Technical Director/Representative Date: 09/11/16
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Page 3 of 15 �_:��"�.
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Serial No:09111619:53 � '
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Page 4 of 15
• Serial No:09111619:53
Project Name: PLATT RESIDENCE Lab Idumber: L1627750
� Project Number: BEA15-10827 Report Date: 09/11/16
SAMPLE RESULTS
Lab ID: L1627750-01 Date Collected: 09/01/16 13:40
Client ID: EFF�uENT Date Received: 09/02/16
Sa11lpIB LOCBtIOCI: SOUTH YARMOUTH,MA Field Prep: Not Specified
Matrix: Vllater
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method pnalyst
Generai Chemistry-Westborough Lab
Solids,Total Suspended ND mg/I 5.0 NA 1 - 09/06/16 16:20 121,2540D SG
Nitrogen,Nitrite ND mg/I 0.050 — 1 - 09/02/1623:55 44,353.2^ MR
_._.._._--...._.._..__..__.._.......__._.... ..---._._. . . .__ ._......-------_.._ _ _ __ _ __----.._._..-- - _._._.....__....----..___... _.._.._._ ..__....._-----.._.�_....___......---------.....__._..-----
Nitrogen,Nitrate 5.2 mg/l 0.10 — 1 - 09/02/1623:55 44,3532 MR
Nitrogen,Total Kjeldahl 2.85 mg/l 0.300 — 1 09l07/16 09:07 09/09/16 00:16 121,4500N-C AT
BOD,5 day 4.0 mg/I 2.0 NA 1 09/03/16 00:30 09/07/16 23:15 121,52108 JC
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Page 5 of 15
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Serial No:09111619:53 ` '
Project Name: PLATT RESIDENCE Lab Number: L1627750
Project Number: BEA15-10827 Report Date: 09/11/16 � '
Method Blank.4nalysi� '
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�atch Quality Control ;
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Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928643-1
Nitrogen,Nitrate ND mg/I 0.10 — 1 - 09/02/16 22:39 44,353.2 MR
General Chemistry-Westborough Lab for sample{s): 01 Batch: WG928645-1 '
Nitrogen,Nitrite ND mgll OA50 — 1 - 09/02/16 22:42 44,3532 MR
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928708-1
BOD,5 day ND mgA 2.0 NA 1 09l03/16 00:30 09/07/16 23:15 121,5210B JC '
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG929134-1
Solids,Total Suspended ND mgll 5.0 NA 1 - 09/06/16 96:20 121,2540D SG
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG929421-1
Nitrogen,Total Kjeldahl ND mgA 0.300 — 1 09/07/16 09:07 09/08/16 23:49 121,4500N-C AT
_. _ .. . . . . .. . . ._............. .._ .... _ _. .. . .... _ ... .. .. .__ .. _.. .... .. ._ .
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Serial No:09111619:53 ' ,
Project Name: PLATT RESIDENCE Lab Numher: L1627750 ,
Project Number: BEA15-10827 Report Date: 09/11l16 � ,
Sample Receipt and Container Information '
I
Were project specific reporting limits specified? YES
Cooler information Custody Sea!
Cooler
A Absent
Container Information Temp
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*)
L1627750-01A Piastic 250m1 H2SO4 preserved A <2 2.3 Y Absent TKN-4500(28) '
L1627750-01 B Plastic 950m1 unpreserved A 7 2.3 Y Absent NO2�53(2),BOD-5210(2),NO3-
353(2)
L1627750-01C Plastic 950m1 unpreserved A 7 2.3 Y Absent TSS-2540(7)
'�
*Values in parentheses indicate holding time in days ;'_vt�a
Page 10 of 15
` Serial No:09111619:53
�
Project Name: PLATT RESIDENCE Lab Number: L1627750
Project Number: BEA15-10827 Report Date: 09/11/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:Tlus value represents the level to which tazget analyte concentrations az•e reported as estunated
values,when those target analyte concenLations are quantified below the reporting limit(RL).The EDL includes any
adjustrnents fi�om dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microexfi�action(SPME).
EPA -Envu•onmental Protection Agency.
LCS -LaUoratoiy Control Sample:A sample mahY�c,free fiom the analytes of interest,spiked with verified known amounts of
analytes or a material containing l�own and verified amounts of analytes.
LCSD -Laboratory Conh•ol Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample mafrix,free from flie analytes of interest,spiked with verified I�own amounts of
analytes or a material containing known and verified amounts of analytes.
MDL -Method Detection Limit:This value represents the level to wluch target analyte concentrafions are reported as estimated
values,when those tazget analyte concentrations aze quantified below the reporting limit(RL).The MDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.
MS -Matrix Spike Sample:A sample prepared�y adding a known mass of target analyte to a specified amount of matrix sample for
which an independent estimate of target analyte concenhation is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Teim is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's
reportin�unit
NDPA/DPA -N-Nitrosodiphenylamine/Diphenylamine.
NI -Not Ignitabie.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RL
includes any adjustments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the
precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less
than five times the reporting limit for any individual pazameter are evaluated by utilizing the absolute difference between the
values;although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a]�own or certified value that is of the same or simi]ar matrix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TIC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound
list(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations.
Footnotes
1 -The reference for ttus analyte should be considered modified since tlus analyte is absent from Yhe target analyte list of the
original method.
Terms
Total:4Jith respect to Organic analyses,a'Total'result is defined as the sunvnation of results for individuai isomers or Aroclors.If a'Total'
result is requested,the results of its mdividual components will also be reported.Tlus is applicable to'Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Qualifiers
A -Spectra identified as"Aldol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentratIons of the analyte at less than ten times(l0at)the concentration found in the blank.For MCP-related
projects,flag only applies to associated field samples that have detectabie concentrations of the analyte at less than ten times(l Ox)
the concenlration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable
concenirations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated field sampies that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(eaccluding Air),flaa only applies to associated field samples that have detectable
concentrations of the analyte,which was detected above the repoiting limit in the associated method blank or above frve times the
Repo�t Format: Data Usability Report '
L�+la?HA
Page 11 of 15
�
Serial No:09111619:53 ' �
Project Name: PLATT RESIDENCE Lab Number: L1627750
:
Projecf Number: BEA15-10827 Report Date: 09/11/16 '
Data Qualifiers
---.
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone). �
C -Co-elution:The tazget analyte co-elutes with a Imown lab standud(i.e.surrogate,internal standards,etc.}for co-exh-acted ;
analyses. '
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations
of the analyte.
E -Concentration of analyte eacceeds the range of the calibrarion curve and/or lineaz range of the instrument.
G -The concentration may be biased lugh due to mah-ix interferences(i.e,co-elution)witli non-target compound(s).T'he result should
be considered estimated.
H -The analysis of pH was performed beyond the regulatory-required holding rime of I S minutes from Nie time of sample collection.
I -The lower value for the two colwnns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds flie MCP CAM Reporting Limit for diis analyte.
NJ -Presumptive evidence of compourid.This represents an estimated concenhalion for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral libraiy search.
P -Tl�e RPD between the results for the two columns exceeds the method-specified criteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration
Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for maUvc spike recoveries
when the sample concentration is greater than 4x the spike added or for Uatch duplicate RPD when the sample concentrations aze less
than Sx the RL.(Metals only.j
R -Anal}rtical results aze from sample re-analysis.
RE -Analytical results are fi•om sample re-exteaction.
S -Analytical results aze from modified screening analysis.
J -Estimated value.This represents an esUmated concentration for Tentatively Identified Compowids(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
f
Report Format: Data Usabifity Report
.lSf:?F;A
__Y"rrew•
Page 12 of 15
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' Serial No:09111619:53
Project Name: PLATT RESIDENCE Lab Number: L1627750
Project Number: BEA15-10827 Report Date: 09/11/16
REFEEtENCES
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
121 Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WEF.
Standard Methods Online.
LIMITATION OF LIABILITIES
Alpha Analytical perForms services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at iYs own expense. In no event shall Alpha Analytical be held liable
fior any incidental, consequential or special damages,including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation,cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
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Page 13 of 15
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Serial_No:o9111619:53 ' ;
Alpha Analytical, Inc. ID No.:'17873 ' �
Facility: Company-wide Revision 7 ;
Department: Quality Assurance Published Date: 8/5/2016 11:25:56 AM
Title� Certificate/Approval Proqram Summarv Paqe 1 of 1
Certification Information �
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The following analytes are not included in our Primary NELAP Scope of Accreditation: '
_.. _ __. _ _ _ _ __
11Vestborough Facility
EPA 624:m/p-xylene,o-xylene
EPA8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene;SCM:lodomethane(methyl iodide),Methyl methacrylate,1,2,4,5-
Tetramethylbenzene;4-Ethyltoluene.
EPA8270D: NPW:Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 300: DW:Bromide '
EPA 6860: NPW and SCM:Perohlorate '
EPA 9090: NPW and SCM: Amenable Cyanide Distillation
EPA 9012B: NPW:Total Cyanide
EPA 9050A: NPW:Specific Conductance
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved Organic Carbon
Mansfield Facility
SM 2540D: TSS
EPA 3d05A NPW
EPA 8082A:NPW: PCB:1,5,31,87,101,110, 141,151,153,180,183,187.
EPATO-15:Halothane,2,4,4-Trimethyl-2-pentene,2,4,4Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene.
Biological Tissue Matrix: EPA 305a6
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SAA4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.9,
SM2930B,SM4500C1-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate;EPA 524.2: THMs and VOCs;EPA 504.1:EDB,DBCP.
Microbiology.SM9215B;SM9223-P/A,SM9223B-Colilert-QT,SM9222D.
Non-Pofable Wafer
SM4500H,B,EPA 120.1,SM2510B,SM2540C,SM23206,SM4500CL-E,SM4500E-BC,SM4500NH3-BH,EPA 350.1:Ammonia-N,LACHAT 10-907-
06-1-B:Ammonia-N,SM4500NO3-F,EPA 353.2:Nitrate-N,EPA 351.1,SM4500P-E,SM4500P-B,E,SM4500SO4-E,SM5220D,EPA 410.4, ',
SM5210B,SM5310C,SM4500CL-D,EPA 1664,EPA 420.1,SM4500-CN-CE,SM25400. ;
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan 1,Endosulfan 11,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC(AcidBaselNeutral Extractables),EPA 600/4-87-045:PCB-OiL
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
Mansfield Facility:
Drinking Water
EPA 200.7:Ba,Be,Cd, Cr,Cu,Ni,Na,Ca.EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TL.EPA 245.1 Hg. _
Non-Potable Water
EPA200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,TL,Ti,V,Zn.
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TL,Zn.
EPA 245.1 Hg.
SM2340B
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID: 08-113
Page 14 of 15
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