HomeMy WebLinkAbout2016 Nov 02 - Bennett Environmental Associates, Inc. �
ENl�TETT E VIRONMENTAL ASSUCIATES, INC.
� LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS
1573 Main Street,P.O.Box 1743 (508)896-1706
Brewster,MA 02631 faz(508)896-5109
LETTER OF TRANSMITTAL
T�: DATE: JOB NUMBER:
Massachusetts Department of Environmental Protection 11/2/16 BEA13-10609
' Attention:Title 5 Progam
1 Winter Street-6th Floor
Boston,MA 02108 REGARDING:
Hughes Residence
_,.,._ �
17 Dove's Wing Road f -
SHIPPING METFIOD: South Yarmouth,MA `
; ��pN 3 0 2011
Regular Mail � Pick Up � � ?
E r!� - i
Priori Mail � �--��_ -� � - �-'
ty ❑ Hand Deliver
Express Mail ❑ Other ❑
Certified Mail 0 Green Card/RR �
COPIES DATE DESCRIPTION
1 DEP Approved Inspection and O&M Form for Title 5 UA Treatment and Disposal Systems(June and
September 2016)
1 AdvanTex Field Maintenance Report(7une and September 2016)
1 3/18/16 Alpha Analytical Laboratory Report
1 9/11/16 Alpha Analytical Laboratory Report .
For review and comment: � For approval: � As requested: � For your use: �
REIVIARKS:
Please fmd enclosed the DEP Inspection and O&M Forms, AdvanTex Field Maintenance Reports,and laboratory analytical results for
operation and maintenance conducted during the reporting period at the above referenced property. If you liave any questions or require
additional information,please contact us at your earliest convenience. Thank you.
cc:Yarmouth Board of Health
Ms.Mazilyn Hughes,Properly Owner
FROM: Samantha Farrenkopf,Wastewater Program Manager
If enclosures are not as noted,kindly notify us at once
Massachusetts Department of Environmental Protection
Bureau of Resource Protection - Title 5
- DEP Approved Inspection and O&M Form for Title 5 I/A �
Treatment and Disposal Systems
A. Installation
Important:When Marilyn Hughes
filling out forms Owner
on the computer,
use only the tab 17 Doves Wing Road
key to move your Facility Street Address
cursor-do not South Yarmouth 02664
use the return City Z�P
key.
� Mailing address of owner, if different:
�
Street Address/PO Box: �
r�rn
City • State Z�p
(508)542-4622 e�.
Telephone Number
B. Authorized Service Provider
Bennett Environmental Associates, Inc.
o&M Firm •
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Zip
(508)896- 1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265
Cert�ed Operator Name Certification Number
C. Facility/System Information
Orenco AdvanTex AX-10
DEP ID Manufacturer ID Model Number
7/26/2008 7/30/2008
Installation Date Start of Operation
. Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial
Seasonal Residence—used less than 6�mo./year: ❑ Yes � No
D. Operating Information
3/10/16 9/14/15
Inspection Date Previous Inspection Date
Sludge Depth(to be checked yearly) PUmplllg R@COt11111e11d2d ❑ Yes � No
t5aiom.doc•rev.04-11-13 Page 1 of 3
Massachusetts Department of Environmental Protection r
Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A - '
Treatment and Disposaf Systems
E. Field Testing
Field Inspection:
Color: ❑ gray ❑ brown � clear ❑turbid
❑ Other(specify):
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid �
Effluent Solids: � no ❑ some
pH 6.5 SU p� 4.0 mg/L Turbidit 1.97 NTU ;�
6 to 9 2 or greater y 40 or less �
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected
per Standard Methods and analyzed for BOD and TSS. !
�
F. Sampling Information ;
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use �
nitrogen reducing systems:
9Pd
Parameters sampled: ❑ pH � BOD � CBOD � TSS ❑TN�Other(list below)
Nitrate Nitrite TKN �
Other 1 Other 2 Other 3 �
G. Inspection and Maintenance '
Description of any maintenance performed since previous inspection &during this inspection:
. Conduct an operation and maintenance event. Coflect effluent samples for field testing and
laboratory analysis.
Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field
testing.
t5aiom.doc•rev.04-11-13 Page 2 of 3
.
i
Massachusetts Department of Environmental Protection
; Bureau of Resource Protection - Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts certified operator in accordance with 257 CMR 2.00.
r
� ��1z�,�
Operator Signature Date
System owner must submit this report, technology O&M checklist, and any required sampling results
to the local board of health as follows for each inspection pertormed: �
Remedial Use—by January 31�of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31th of each year for the previous 12 months
General Use—by September 30�of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5th Floor
Boston, MA 02108
t5aiom.doc•rev.04-11-13 Page 3 of 3
Massachusetts Department of Environmental Protection
; Bureau of Resource Protection -Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A �
Treatment and Disposal Systems
A. Installation
Important:When Marilyn Hughes -
filling out forms Owner
on the computer,
use only the tab 17 Doves Wing Road -
key to move your Facility Street Address
cursor-do not South Yarmouth 02664
use the return City Z�P
key.
Jr��1 Mailing address of owner, if different:
���
� Street Address/PO Box:
renan
City State Z�P
(508) 542-4622 ext.
Telephone Number
B. Authorized Service Provider
Bennett Environmental Associates, Inc.
O&M Firm
1573 Main Street/PO Box 1743
Street Address
Brewster MA 02631
City State Z�p
(508)896-1706 ext. 129
Telephone Number
Samantha Farrenkopf 13265
Certified Operator Name Certification Number
C. Facility/System Information
Orenco AdvanTex AX-10
DEP ID Manufacturer ID Model Number
7/26/2008 7/30/2008
Installation Date Start of Operation
Approval Type: ❑ General � Provisional ❑ Piloting ❑ Remedial
Seasonal Residence—used less than 6 mo./year: ❑ Yes � No
D. Operating Information
9/1/16 3/1/16
Inspection Date Previous Inspection Date
3"sludge, 3"scum Pumping Recommended ❑ Yes � No
Sludge Depth(to be checked yearly)
t5aiom.doc•rev.04-11-13 Page 1 of 3
r
Massachusetts Department of Environmental Protection _
Bureau of Resource Protection - Title 5 � � .
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposai Systems
E. Field Testing
Field inspection:
Color: ❑ gray ❑ brown � clear ❑turbid '
❑ Other(specify): '
Odor: � musty ❑ earthy ❑ moldy ❑ offensive ❑ turbid
Effluent Solids: � no ❑ some
pH 6.5 SU D0 2.0 mg%L Turbidity 5.25 NTU
6 to 9 2 or greater 40 or less
Should a Remedial or General Use system fail the Field Testing, effluent samples shall be collected �
per Standard Methods and analyzed for BOD and TSS.
F. Sampling Information ,
Samples Taken: ❑ Influent � Effluent
Commercial systems or systems with a design flow of 2000 gpd and greater, and General Use '
nitrogen reducing systems: .
gpd
Parameters sampled: ❑ pH � BOD ❑ CBOD � TSS 0 TN � Other(list below)
_Nitcat�- -- Nitrite TKN
Other 1 Other 2 Other 3
G. Inspection and Maintenance
Description of any maintenance performed since previous inspection&during this inspection:
Conduct an operation and maintenance event. Collect effluent samples for field testing and
laboratory analysis. Vent air filter requires replacement.
. Notes and Comments:
All mechanical components of the system are operating correctly. Effluent quality passed field
testing.
_... ._ �
t5aiom.doc•rev.04-11-13 Page 2 of 3
Massachusetts Department ofi Environmental Protection
. Bureau of Resource Protection - Title 5
DEP Approved Inspection and O&M Form for Title 5 I/A
Treatment and Disposal Systems
H. Certification
I certify: I have inspected the sewage treatment and disposal system at the address above, have
conducted the required Field Testing and/or sample collection in accordance with Standard Methods,
have completed this report and the attached technology operation and maintenance checklist, and
the information reported is true, accurate, and complete as of the time of the inspection. I am a
Massachusetts certi ed operator in accordance with 257 CMR 2.00.
�1Z�<t�,
Ope or ,ignature Date
System owner must submit this report, technology Q&M checklist, and any required sampling results
to the local board of health as follows for each inspection performed:
Remedial Use—by January 31�of each year for the previous calendar year
Piloting Use-within 45 days of inspection date
Provisional Use—by March 31�of each year for the previous 12 months
General Use—by September 30th of each year for the previous 12 months
Send to:
Department of Environmental Protection
Attention: Title 5 Program
One Winter Street, 5� Floor
Boston, MA 02108
i
t5aiom.doc•rev.04-11-13 Page 3 of 3
290 914
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Serial No:03181615:07
. � ,., �/'�
.:���.��.�. . :�:��T'1 G:4`L �
ANALYTICAL REPORT
Lab Number: L1607097
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
ATTN: David Bennett
Phone: (508)896-1706
Project Name: HUGHES RES.IDENCE
� Project Number: BEA13-10609
Report Date: 03/18/16
The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its
entirety.Alpha Analytical holds no responsibiliry for results and/or data that are not consistent with the origir�al.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P-330-11-00240).
Eight Walkup Drive,Westborough, MA 01581-1019
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com
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i Serial No:03181615:07
�
Project Name: HUGHES RESIDENCE Lab Number: L1607097
. Project Number: BEA13-10609 Report Date: 03/18/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Rlpha Lab Number and meet NELAP requirements for ali
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list
for each individual sampie,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Ident�ed Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
� even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective
action and'rf both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Spec'�'ic%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool u�rhere it can be reviewed along with any associated usability implications.Soil/sediments,solids an�i tissues are reported on a
dry weight basis unless otherwise noted.Definifions of all data qualifiers and acron�ms used in this report are provided in the Giossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the pertormance criteria for CAM and RCP methods allow for some
quality control failures to occur and stiil be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table.The iriformation is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numericai
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days
from the date the project is compieted.Rfter 21 calendar days,we will dispose of all samples submitted including those put on t�old unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will
be disposed after 3 business days ftom the date the project is compieted.
Please contact Client Services at 800-6249220 with any questions.
I,the undersigned,attest under the pains and penaities of perjury that,to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report, such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
�...�-� �� Lu ra L 7roy
Authorized Signature: �� (/
Title: Technical Director/Representative Date: 03/18/16
Page 3 of 15 ����
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Serial No:03181615:07
I������ ���
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IlIIISCELLANEOUS
_.:._.. e..
Page 4 of 15
, Serial_No:03181615:07
Project Name: HUGHES RESIDENCE Lab Number: L1607097
• Project Number: BEA13-10609 Report Date: 03/18/16
SAMPLE RESULTS
Lab ID: L1607097-01 Date Collected: 03/10/16 14:30
Client ID: EFF�uEtvT Date Received: 03/11/16
Sample Location: sourH YaRnnotrrH,nna, Fieid Prep: Not Specified
Matrix: Water
� Dilution Date Date Analytical
Parameter Result Quali£er Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-VVestborough Lab ; '
$olids,Total Suspended ND mg/I 5A NA 1 - 03117l16 03:12 30,2540D RT
Nitrogen,Nitrite 0.26 mgll 0.050 __ _ 1 ___;__ _03/11/1621�41� 44,353.2 _ MR
Nitrogen,Nftrate 19. � mgti 0.50 — 5 - 03111116 23:37 44,353.2 MR
Nitrogen,Total Kjeldahl 1.98 mg/I 1.50 — 5 03/13/16 20:00 03/16116 22:36 30,4500N-C AT
BOD,5 day 10. mg/i 2.0 NA 1 03/12/16 04:55 03/16/16 23:10 30,52106 TA
Page 5 of 15
r
Serial No:03181615:07 �
Project Name: HUGHES RESIDENCE Lab Number: L1607097 '
Project Number: BEA13-10609 Report Date: 03/18/16 '
� Method Blank Analysis ;
Batch Quality Control '
r
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
G,eneral Ghemistry-1Nestborough Lab for.sample(s): 01 Batch: WG873113-1
Nitrogen,Nitrate ND mg/I 0.10 — 1 - 03/11/16 21:30 44,353.2 MR
General Ghemisfry-Westfiorough Lab for sample(s): 01 Batch: WG873114-1 ' .
NiVogen,Nitrite ND mg/l 0,050 - 1 - 03/11/16 21:32 44,353.2 MR ;
General Chemi"stry-V1%estborough Lab for sample(s): 01 Batch: WG873206-1 ;
BOD,5 day ND mg/I 2.0 NA 1 03/12/16 04:55 03/16/16 23:10 30,5210B TA
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG873440-1
Nitrogen,Total lCeldahl ND mg/I 0.300 — 1 03/13l16 20:00 03/16/16 22:31 30,4500N-C AT
General Chemisfry-Westborough Lab for sample(s): 01 Batch: WG874594-1
Solids,Total Suspended ND mg/i 5.0 NA 1 - 03/17/16 03:12 30,2540D RT
............................... _.......... - .........._..............................................................._........._........ ..........- -...._.......................__..._..
'
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Page 6 of 15
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Serial No:03181615:07 '
Project Name: HUGHES RESIDENCE Lab Number: L1607097
Project Number: BEA13-10609 Report Date: 03/18/16 -
� Sample Receipt and Container Information
Were project specific reporting limits specified? YES
�
Cooler Information Custody Seal '
Cooler
A Absent
Container Information Temp
Container ID Container Type Cooler pH deg C Pres Seal Analysis(*) �
L1607097-01A Plastic 250m1 H2SO4 preserved A <2 3.5 Y Absent TKN-4500(28)
L1607097-01 B Plastic 950m1 unpreserved A 7 3.5 Y Absent NO2-353(2),BOD-5210(2),NO3- �
353(2)
L1607097-01C Plastic 950m1 unpreserved A 7 3.5 Y Absent TSS-2540(7)
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*Values in parentheses indicate holding time in days -
-.�.;..r,a.�
Page 10 of 15
Serial No:03181615:07
Project Name: HUGHES RESIDENCE Lab Number: L1607097
• Project Number: BEA13-10609 Report Date: 03/18/16
GLOSSARY "
Acronyms
EDL -Estimated Detection Limit:This value represents the level to which target analyte concentradons aze reported as estimated
values,when those target analyte concentrations aze quantified below the repozting limit(RL).The EDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDIs is specific to the analysis of
PAFis using Solid-Phase Microextraction(SPME).
EPA -Environmentat Protection Agency.
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified imown amounts of analytes
or a material containing known and verified amounts of analytes.
LCSD -Laboratory Control Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free&om the analytes of interest,spiked with verified known amounts of analytes
or a material containino lmown and verified amounts of analytes.
MDL -Method Detection Limit:This value tepresents the level to which target analyte concentrations aze reported as estimated values,
when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjusiments from
dilutions,concentrafions or moisture content,where applicable.
MS -Matrix Spike Sampie:A sample prepazed by adding a l�own mass of target analyte to a specified amount of matrix sample for
wluch an independent estimate of target anatyte concentration is available.
MSD -Matrix Spike Sample Duplicate:Refer to MS.
NA -NotApplicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation aze non-detect at the parameter's
reporting unit.
IVI -NotIgnitable.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL -Reporting Limit: The value at which an inshvment can accurately measure an analyte at a specific concentradon.The RL
includes any adjushnents from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results&om matrix and/or matrix spike duplicates are primarily designed to assess the precision
of analykical resulis in a given matrix and aze eacpressed as relative percent difference(RPD). Values which are less than five
times the reporking limit for any individual parameter are evatuated by utilizing the absolute difference between the values; �
although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a lmown or certified value that is of the same or similar matrix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA Method 1315.
TIC -Tentatively Ideatified Compound:A compound that has been identified to be present and is not part of the target compound list
(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations.
Footnotes .
1 -The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original
method
Terms
Total:With respect to Organie anatyses,a"Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.Tlus is applicable to'Tatal'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and the analytical reference method(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided�in the References section of the Addendum.
Data Qualifrers
A -Spectra identified as"Aidol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times(lUx)the concentration found in the blank.For MCP-related
projects,flag only applies w associated field samples that have detectable concentrations of the analyte at less than ten times(10�c)
the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times(lOx)the concentration found in the blank ANIS the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab eontaminants)in the associated method blank.For NJ-
Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
Report Format: Data Usability Report '
�'�A;. .�'�
Page 11 of 15
, Serial No:03181615:07 =
Project Name: HUGHES RESIDENCE Lab Number: L1607097
Project Number: BEA13-10609 Report Date: 03/18/16 " i
Data Quali�ers
C -Co-elution:The target analyte co-elutes with a Irnown lab standazd(i.e.surrogate,internal standards,etc.)for co-e�ctracted
analyses.
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrafions
of the analyte.
E -Concentration of analyte e�cceeds the range of the calibration curve and/or lineaz range of the instrument
G -The concentration may be biased high due to mahix interferences(i.e,co-elution)with non-tazget compound(s).The result should
be considered estimated.
H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
I -The lower value for the iwo columns has been reported due to obvious interference.
M -Reporting Lixnit(RL)exceeds the MCP CAM Reporting Limit for tlus analyte.
NJ -Presumprive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(1'ICs),where
the identification is based on a mass spectral library search.
P -The RPD between the results for the two columns exceeds the method-specified criteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DODxelated projects,LCS and/or Continuing Cah'bration '
Standard exceedences a��e also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries '
wHen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less '
than Sx the RL.(Metals only.) ',
R -Analylical results are from sample re-analysis.
RE -Analytical results are from sample re�xtraction. '
3 •Analytical results are from modified screenin�analysis.
J -Estimated vatue.Thcs represents an estimated concentration for Tentatively Identified Compounds(TICs).
ND -Not detected at the reporting limit(RL)for the sample.
�i
f
Report Format: Data Usability Report �
'�.� FiA
Page 12 of 15
aenai i�o:u.s�i u�i n-i�:u i
Project Name: HUGHES RESIDENCE Lab Number: L1607097
• Project Number: BEA13-10609 Report Date: 03/18/16
REFERENCES
30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-
WPCF. 18th Edition. 1992.
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100, August 1993.
LIMITATION OF LIABILITIES
Alpha Analytical performs services with reasonable care and diligence normai to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental,consequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,
containers, sampling procedures, holding time and splitting of samples in the field.
aa �..
Page 13 of 15
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Serial No:03181615:07 . ;
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 6
Department:Quality Assurance Published Date:2/3/2016 10:23:10 AM _
Title: Certificate/Approval Proqram Summarv PaQe 1 of 1
Certification Information
The following analytes are not included in our Primary NELAP Scope of Accreditation:
Westborough Facility
EPA 524.2:1,2-Dibromo-3-chloropropane,1,2-Dibromoethane,m/p xylene,o-xylene
EPA 624:2-Butanone(MEK),1,4-Dioxane,tert-Amylmethyl Ether,tert-Butyl Alcohol,m/p-xylene,o-xylene
EPA 625: Aniline,Benzoic Acid,Benryl Alcohol,4-Chloroaniline,3-Methylphenol,4-Methylphenol.
EPA 1010A: NPW: Ignitability
EPA 6010C: NPW:Strontium;SCM: Strontium
EPA 8151A: NPW:2,4-DB,Dicamba,Dichloroprop,MCPA,MCPP;SCM: 2,4D6,Dichloroprop,MCPA,MCPP
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4-Ethyltoluene,Azobenzene,Isopropanol;SCM:lodomethane(methyi iodide),Methyl methacrylate
(soil);1,2,4,5-Tetramethylbenzene;4Ethyltoluene.
EPA 8270D: NPW:Pentachloronitrobenzene,1-Methylnaphthalene,Dimethylnaphthalene,l,4-Diphenylhydrazine;SCM:Pentachloronitrobenzene,1-
Methyinaphthalene,Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 9010: NPW: Amenable Cyanide Distillation,Total Cyanide Distillation
EPA 9038: NPW: Sulfate .
EPA 9050A: NPW:Specific Conductance
EPA 9056:NPW:Chloride,Nitrate,Sulfate
EPA 9065: NPW:Phenols
EPA 9251: NPW:Chloride
SM3500: NPW:Ferrous Iron
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Totai Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved Organic Carbon
Mansfleld Facility �
EPA 8270D:NPW: Biphenyi;SCM: Biphenyl,Caprolactam
EPA 8270DSIM Isotope Dilution: SCM: 1,4-Dioxane
SM 2540D: TSS
SM2540G: SCM:Percent Solids
EPA 1631 E:SCM: Mercury
EPA 7474: SCM: Mercury
EPA 8081B:NPW and SCM:Mirex,Hexachlorobenzene.
EPA8082A:NPW: PCB:1,5,31,87,101,110,141,151,153,180,183,187.
EPA 8270SIM: NPW and SCM: Alkylated PAHs.
EPA TO-15:Halothane,2,4,4Trimethyl-2-pentene,2,4,4Trimethyi-1-pentene,Thiophene,2-Methylthiophene,
3-Methylthiophene,2-Ethylthiophene,1,2,3 Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene,n-
Butylbenzene,n-Propylbenzene,sec-Butylbenzene,tert-Butylbenzene. '
Biological Tissue Matrix: 8270D-SIM;30508;3051A;7479B;8081B;8082A;6020A:Lead;8270D:bis(2-ethylhexyi)phthalate,Butylbenrylphthalate, i
Diethyi phthalate,Dimethyl phthalate,Di-n-butyl phthalate,Di-n-octyl phthalate,Fluoranthene,Pentachlorophenol:
The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: '
Drinking Water
EPA200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA200.7:Ba,Be,Ca,Cd,Cr,Cu,Na;EPA245.1:Mercury;
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4SOOCN-CE,EPA 180.1,
SM2130B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate.
Microbiology:SM9215B;SM9223-P/A,SM9223B-Colilert-QT,Enterolert-QT.
Non-Pofa6fe Wafer
EPA200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn;
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn;
EPA 245.7,SM4500H,B,EPA 120.1,SM2510B,SM2540C,SM2340B,SM2320B,SM4500CL-E,SM4500E-BC,SM426C,SM4500NH3-BH,EPA
350.1:Ammonia-N,LACHAT 10-107-06-7-B:Ammonia-N,SM4500NO3-F,
EPA 353.2:Nitrate-N,SM4500NH3-BC-NES,EPA 351.1,SM4500P-E,SM4500P-B,E,SM5220D,EPA 410.4,SM5210B,SM5370C,SM4500CL-D,
EPA 1664,SM14 570AC,EPA420.7,SM4500-CN-CE,SM2540D.
EPA 624:Volatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,detta-BHC,Dieldrin,DDD,DDE,DDT,Endosulfan 1,Endosulfan 11,
Endosuffan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epoxide,PCBs
EPA 625:SVOC(AcidBase/Neutral Extractables),EPA 600/4-81-045:PCB-Oil.
Microbiology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF.
i
For a complete lisfing of analytes a�d methods,please contact your Alpha Project Manager.
Document Type: Form Pre-Qualtrax Document ID:08-113
Page 14 of 15
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, Serial_No:09111619:53
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.4=N;H t-Y�.T 1 C A L ,
ANALYTICAL REPORT
Lab Number: L1627746
Client: Bennett Environmental Associates
1573 Main Street
Brewster, MA 02631
ATTN: David Bennett
Phone: (508)896-1706
Project Name: HUGHES RESIDENCE
Project Number: BEA13-10609
Report Date: 09/11/16
The original project report/data package is held by Aipha Analytical.This report/data package is paginated and should be reproduced only in its
entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH{2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086),
PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(L2217),USDA(Permit #P�30-11-00240).
Eight Walkup Drive,Westborough, MA 01581-9019 ;
508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com
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Page 1 of 15
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. Serial No:09111619:53
Project Name: HUGHES RESIDENCE Lab Number: L1627746
' Project Number: BEA13-10609 Report Date: 09/11/16
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis uniess otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all
NELAP accredited parameters unless otherwise noted in the following narrative.The data presented in this report is organized by parameter
(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Sunogate Spike Recovery)is reported at the end of the target analyte list
for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter.Tentatively Identified Compounds
(TICs),if requested,are reported for compounds identified to be present and are not part of the method/program Target Compound List,
even if only a subset of the TCL are being reported.If a sample was re-analyzed or re-extracted due to a required quality control corrective
action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",
respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element
are noted in the grey shaded header line of each data table.Any LaboraEory Batch,Sample Specific%recovery or RPD value that is outside
the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data
Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments,solids and tissues are reported on a
dry weight basis unless otherwise noted.Definitions of ali data qualifiers and acronyms used in this report are provided in the Glossary
located at the back of the report.
In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the perFormance criteria for CAM and RCP methods aliow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
a�sociated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hoid,Alpha's policy is to hold samples(with the exception of Air qnisters)free of charge for 21 calendar days
ftom the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless
you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters wili
be disposed after 3 business days from the date the project is completed.
Please contact Client Services at 800-6249220 with any questions.
I,the undersigned,attest under the pains and penalties of perjury that, to the best of my knowledge and
belief and based upon my personal inquiry of those responsible for providing the information contained
in this analytical report,such information is accurate and complete. This certificate of analysis is not
complete unless this page accompanies any and all pages of this report.
�����(�7 Kerly Stenstrom
Authorized Signature:
Title: Technical Director/Representative Date: 09/11/16
._�
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Page 3 of 15 - •
Serial No:09111619:53 `
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Page 4 of 15
Serial No:09111619:53
Project Name: HUGHES RESIDENCE Lab Number: L1627746
` Project Number: BEA13-10609 Report Date: 09/11/16
SAMPLE RESULTS
Lab ID: L1627746-01 Date Collected: 09/01/16 15:10
Client ID: EFFLUENT Date Received: 09/02/16
SaI7lple LOCatIOn: SOUTH YARMOUTH,nna Field Prep: Not Specified
Matrix: Water
Dilution Date Date Analytical
Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab
Solids,Total Suspended 6.0 mgfl 5A NA 1 - _ 09/06/16 16:20 121,2540D SG
Nitrogen,Nitrite 0.14 mgfl 0.050 - 1 - 09/02/16 23:51 44,353.2 MR
--.._...__.._.__.-----....---._..._---
---------------- -—---------------..-------------------_..._- -----�---------------------�---
Nitrogen,Nitrate 35. mgA 0.50 - 5 - 09/03/16 00:07 44,353.2 R
Nitrogen,Total Kjeldahi 9.04 mg/i 3.00 - 10 09/07/16 09:07 09/09/16 00:14 121,4500N-C AT
BOD,5 day _____ 8.0 _ __,__m9� _ 2•0 __NA __ 1_ „09/03/16 00:30 09/07/16 23:15 121,5210B JC
`..'{
LZI:�b'A
Page 5 of 15
Serial No:09111619:53 '
Project Name: HUGHES RESIDENCE Lab Number: L1627746
Project Number: BEA13-10609 Report Date: 09/11/16
Method Blank Analysis
Batch Quality Control
Dilution Date Date Analytical
Parameter Result Quali�er Units RL MDL Factor Prepared Analyzed Method Analyst
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG928643-1-
Nitrogen,Nitrate ND mg/I 0.10 – 1 - 09/02ft6 22:39 44,353.2 MR
---- -- —--- — —
General Chemistry-Westborough Lab for sample(s): 09 Batch: WG928645-1 :
Nitrogen,Nitrite ND mg/l 0.050 – 1 - 09/02/16 22:42 44,3532 MR
--- --�--- -- – ._.---------- -...- -------- .. ..__.
General Chemistry-Westborough Lab for sample(s); 01 Batch: WG928708-1 '
BOD,5 day ND mg/I 2.0 NA 1 09/03/16 00:30 09/07l16 23:15 721,52108 JC
General Chemistry=Westborough Lab for sample(s): 01 Batch: WG929134-1
Solids,Total Suspended ND__ � ^ __ mg/� 5.0 NA 1 - 09/O6/1616:20 121,2540D SG
General Chemistry-Westborough Lab for sample(s): 01 Batch: WG929421-1
Nitrogen,Total Kjeldahl ND mg/I 0.300 – 1 09/07/16 09:07 09/08l16 23:49 121,4500N-C AT
.. _ . ...... . ._ ..... .......... ....... _ .. ... ... . ...... ..... ... .. ..... .... .... ....
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Seriai No:09111619:53 '
Project Name: HUGHES RESIDENCE Lab Number: L1627746 '
Project Number: BEA13-10609 Report Date: 09/11/16 �
Sample Receipt and Container Information
Were project specific reporting limits specified? YES
Cooler Information Custody Seal .
Cooler
A Absent
Container Information Temp
Container ID Container Type Cooler pH deg C pres Seal Analysis(*)
L1627746-01A Plastic 250m1 H2SO4 preserved A <2 2.3 Y A6sent TKN-4500(28)
L1627746-01 B Plastic 950m1 unpreserved A 7 2.3 Y Absent NO2-353(2),BOD-5210(2),NO3-
353(2)
L1627746-01C Plastic 950m1 unpreserved A 7 2.3 Y Absent TSS-2540(7)
I
�I� . . . . . .. _._ _ .
*Values in parentheses indicate holding time in days '��a
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� Serial_No:Uy 1'I'I ti'I y:5�
Project Name: HUGHES RESIDENCE Lab Number: L1627746
` Project Number: BEA13-10609 Report Date: 09/11/16
GLOSSARY
Acronyms
EDL -Estimated Detection Limit:This�Value represents the level to which target analyte concentrations are reported as estimated
values,when those target analyte concentrations are quantified below the reporting limit(RL).The EDL includes any
adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis
of PAHs using Solid-Phase Microe�rtraction(SPME).
EPA -Environmental Protection Agency.
LCS -Laboratory Control Sample:A sample matrix,free from the analytes of interest,spilced with verified laiown amounts of
analytes or a material containing known and verified amounts of analytes.
LCSD -Laboratory Control Sample Duplicate:Refer to LCS.
LFB -Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of
analytes or a material containing lalown and verified amounts of analytes.
MDL -Method Detection Limit:Tlus value represents the level to which tazget analyte concentrations aze reported as estixnated
values,when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any
adjustments&om dilutions,concentrations or moisture content,where applicable.
MS -Matrix Spike Sample:A sample prepazed by adding a known mass of target analyte to a specified amount of matriarsample for
wluch an independent estimate of target analyte concentration is available.
MSD -Matrix Sp�ce Sample Duplicate:Refer to MS.
NA -Not Applicable.
NC -Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parazneter's
reporting unit.
NDPA/DPA -N NitrosodiphenylaminelDiphenylamine.
NI -Not Ignitable.
NP -Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil.
RL •Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RL
includes any adjustments from dilutions,concentrations or moisture content,where applicable.
RPD -Relative Percent Difference: The results from matrix and/or matrix spike duplicates ue piimarily desi�ed to assess the
precision of analytical results in a given matrix and are e�cpressed as relative percent difference(RPD). Values which aze less
than five times the reporting limit for any individual parameter aze evaluated by utilizing the absolute difference between the
values;although the RPD value will be provided in the report.
SRM -Standard Reference Material:A reference sample of a lmown or certified value that is of the same or similaz matrix as the
associated field samples.
STLP -Semi-dynamic Tank Leaching Procedure per EPA 1vlethod 1315.
TIC -Tentatively Identified Compound:A compound that has been identified to be present and is not part of the target compound
list(TCL)for the method and/or program.All TICs are qualitatively identified and reported as estimated concentrations.
Footnotes
1 _q'he reference for ttus analyte should be considered modified since this analyte is absent&om the tazget analyte list of the
original method.
Terms
Total:With respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total'
result is requested,the results of its individual components will also be reported.This is applicable to"Total'results for methods 8260,8081
and 8082.
Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 8260B is
shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum.
Data Quali�ers
A -Spectra identified as"Aldol Condensation Product".
B -The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that
have detectable concentrations of the analyte at less than ten times(101c)the concentradon found in the blank.For MCP-related
projects,flag only applies to associated field sampies that have detectable concenirations of the analyte at less than ten times(l Ox)
the concentration found in the blanlc.For DOD-related projects,fla�only applies to associated field samples that have detectable
concentrations of the analyte at less than ten times(l Ox)the concentration found in the blank AND the analyte was detected above
one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For N7-
Air-related projects,flag oniy applies to associated field samples that have detectable concenhations of the analyte above the
reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable
concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the
Report Format: Data Usability Report
wr .\, 1ir�
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Serial No:09111619:53 `
Project Name: HUGHES RESIDENCE Lab Number: L1627746
Project Number: BEA13-10609 Report Date: 09111/16 i
Dafa Qualifiers
reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone).
C -Co-elution:The target analyte co-elutes with a l�own lab standaz•d(i.e.sturogate,intemal standazds,etc.)for co-extracted
analyses.
D -Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations
of the analyte.
E -Concentration of analyte exceeds the range of the calibration curve and/or linear range of the inshwnent
G -The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-tareet compound(s).The result should
be considered estimated
� -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample coilection.
I -The lower value for the two columns has been reported due to obvious interference.
M -Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for Uus analyte.
NJ -Presumprive evidence of compound.Tlus represents an estimated concenhation for Tentatively Identified Compounds(TICs),where
the identification is based on a mass spectral library search.
P -The RPD between the results for the two columns exceeds the method-specified criteria.
Q -The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Cah`braHon
Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries '
when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less
than Sx the RL.(Metals only.)
It -Analytical results are from sample re-analysis.
RE -Analytical results aze from sampie re-extracrion.
S -Analytical results aze from modified screen�na analysis.
J -Fsrimated value.This represents an estimated concentr�ation for Tentatively Identified Compounds(TICs).
ND •Not detected at the reporting limit(RL)for the sample.
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Report Format. Data Usability Report
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� Jerlal_IVo:U�J-119 t�l y:bS
Project Name: HUGHES RESIDENCE Lab Number: L1627746
Project Number: BEA13-10609 Report Date: 09/11/16
REFERENCES
44 Methods for the Determination of Inorganic Substances in Environmental Samples,
EPA/600/R-93/100,August 1993.
121 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WEF.
Standard Methods Online. �
LIMITATION OF LIABILITIES
Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing
laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical
shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable
for any incidental, cQnsequential or special damages, including but not limited to, damages in any way
connected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, presenration, cooling, ,�
containers,sampling procedures, holding time and splitting of samples in the field.
�t�a
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Seriai No:o9111619:53 = '
Alpha Analytical, Inc. ID No.:17873
Facility: Company-wide Revision 7
Department:Quality Assurance Published Date: 8/5/2016 11:25:56 AM •
Title: Certificate/Approval Propram Summarv Paqe 1 of 1
Certification Information
�
�
The following analytes are not included in our Primary NELAP Scope of Accreditation: �
Westborough Facility '
EPA 624:m/p-xylene,axylene
EPA 8260C:NPW:1,2,4,5-Tetramethylbenzene;4Ethyltoluene,Azobenzene;SCM:lodomethane(methyi iodide),Methyl methacrylate,1,2,4,5-
Tetramethylbenzene;4-Ethyltoluene.
EPA8270D: NPW:Dimethylnaphthalene,1,4-Diphenylhydrazine;SCM:Dimethylnaphthalene,1,4-Diphenylhydrazine.
EPA 300: DW:Bromide
EPA 6860: NPW and SCM:Perchlorate
EPA 9010: NPW and SCM: Amenable Cyanide Distillation
EPA 9012B: NPW:Total Cyanide
EPA 9050A: NPW:Specific Conductance
SM3500: NPW:Ferrous Iron .
SM4500:NPW: Amenable Cyanide,Dissolved Oxygen;SCM:Total Phosphorus,TKN,NO2,NO3.
SM5310C:DW:Dissolved Organic Carbon
Mansfield Facility
SM 2540D: TSS '
EPA 3005A NPW
EPA8082A:NPW: PCB:1,5,31,87,101,11Q 141,151,153,180,183, 187.
EPATO-15:Halothane,2,4,4Trimethyl-2-pentene,2,4,4Trimethyl-1-pentene,Thiophene,2-Methylthiophene,
3-Methyfthiophene,2-Ethylthiophene,1,2,3-Trimethylbenzene,Indan,Indene,1,2,4,5-Tetramethylbenzene,Benzothiophene,1-Methylnaphthalene.
Biological Tissue Matrix: EPA 30508
The following analytes are included in our Massachusetts DEP Scope of Accreditation
Westborough Facility:
Drinking Water
EPA 300.0:Nitrate-N,Fluoride,Sulfate;EPA 353.2:Nitrate-N,Nitrite-N;SM4500NO3-F:Nitrate-N,Nitrite-N;SM4500E-C,SM4500CN-CE,EPA 180.1,
SM213�B,SM4500CI-D,SM2320B,SM2540C,SM4500H-B
EPA 332:Perchlorate;EPA 524.2: THMs and VOCs;EPA 504.1:EDB,DBCP.
Microbiology;SM92156;SM9223-P/A,SM9223B-Colilert-QT,SM92220.
Non-Potable Water
SM4500H,B,EPA 120.9,SM25106,SM2540C,SM2320B,SM4500CL-E,SM4500E-BC,SM4500NH3-BH,EPA 350.1:Ammonia-N,LACHAT 10-707-
06-1-8:Ammonia-N,SM4500NO3-F,EPA 353.2:Nitrate-N,EPA 351.1,SM4500P-E,SM4500P-B,E,SM4500SO4-E,SM5220D,EPA 410.4,
SM5210B,SM5370C,SM4500CL-D,EPA 1664,EPA 420.7,SM4500-CN-CE,SM2540D.
EPA 624:Valatile Halocarbons&Aromatics,
EPA 608:Chlordane,Toxaphene,Aldrin,alpha-BHC,beta-BHC,gamma-BHC,delta-BHC,Dieldrin,DDD,DDE,DDT,Endasulfan I,Endosulfan II,
Endosulfan sulfate,Endrin,Endrin Aldehyde,Heptachlor,Heptachlor Epo�ade,PCBs
EPA 625:SVOC(Acid/Base/Neutral Extractables),EPA 600/4-81-045:PCB-Oil.
Microblology:SM9223B-Colilert-QT;Enterolert-QT,SM9222D-MF. ',
Mansfield Facility: I
Drinking Water
EPA 200.7:Ba,Be,Cd,Cr,Cu,Ni,Na,Ca.EPA 200.8:Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TL.EPA 245.1 Hg.
Non-Potable Water
EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,TL,Ti,V,Zn.
EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TL,Zn.
EPA 245.1 Hg.
SM2340B .
For a complete listing of analytes and methods,please contact your Alpha Project Manager.
_ . __ . _.. ..._ _ . _ __ __ _
Document Type: Form Pre-Qualtrax Document ID: 08-113
Page 14 of 15
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