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I � k . r GRDUNDWATER ANAI.YTICAI. Inorganic Cherriistry Field ID: FE Matrix: Aqueous Project: Singulair/64 Melville Rd S.Yarmouth Received: 05-28-04 14:20 Client: Siegmund Environmenta)Services Lab ID: 73147-01 Sampled: 05-27-04 18:00 conta�ner: 250 mL PldStiC Preservation: H2SO4/Cool ' Analyte ftesult llrli�s , kt.".'bF-volume; A�r�lyzed" ; QC.Bat�ch. Method inst a�W3� Nitro en,Total K eldahl TKN "`""'"'°'�'o„P^ � $_ )__ ( _ ) _ �¢ � f11g/� �3 S 4ml �06-07-0477:46 TKN-7357-W J5131 1 AV6 Lab ID: 73147-02 Sampled: 05-27-04 18:00 Container: 1 L Plastic Preservation: Cool _Analyte Result Unifs RL DF volume ° Analyzed Q�Batch Methoil Inst �aiYs� _ -- Biochemical Oxygen Demand 28 mg/L �� 60 5mL 06-01-041823 60D-767&W SM52106 3 DDW Lab ID: 73147-03 Sampled: 05-27-04 18:00 Conta�ne�: 1 L PldStiC Preservation: Coo) _ {�tnalyte �--- Result IJn�Cs .. RI. �F' dalume Analyzed I�C Bateh Mcthod lnst �rys� Solids,Total Suspended BRL ff1glL lO 1 100mL 06-01-0410:% TSSA961-W SM2540D 4 MW pH 7.5 pH NA 1 50 mL OS-28-04 18:00 PH-1691-W SM 9500-H+B 2 DDW Lab ID: 73147-04 Sampled: 05-27-04 18:00 Comatnec 1 L Plastic Preservation: Cool �Anal}tte� Result Unif� " RL t�� vnlume An�lyzed QCBatch` Method Inst ���v�� _ __ — _ . —_-- --._�� Nitrate(as Nitrogen) BRL fllg/� 0.�2 1 5 mL OS-28-0416:15 NI-2189-W �"�"'o-�o'-04�t��"' 1 DDW �500-NO3 il . Lacha110.1o)A41{�5�q Nitrite(as Nitrogen) 0.62 mg/L 0.02 1 5 mL os-za-oa ie:�s NI-2189-W ��No,� i oow ' Method Reference: Methods for Chemical Analysis of Water and Wastes,US EPA,EPA-600/4-790-020(Revised 1983),and Methods for the Determination of Inorganic Substances in Environmental Samples,US EPA,EPA/600/R-93/100(1993),and Standard Methods for the Examination of Water and Wastewater,APHA,Twentieth Edition(1998),and Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update 111(1996). Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. RL Reporting Limit DF Dilution Factor. ' 1 Instrument ID: Lachat 8000 Autoanalyzer 2 Instrument ID: Accumet AR50 3 Instrument ID: Y51 5100 � 4 Instrument ID: Metder AT 200 Balance ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 -:s,. a j . � . i . 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